3,5-DIBROMO-1H-1,2,4-TRIAZOLE
Uses- Product Name
- 3,5-DIBROMO-1H-1,2,4-TRIAZOLE
- CAS No.
- 7411-23-6
- Chemical Name
- 3,5-DIBROMO-1H-1,2,4-TRIAZOLE
- Synonyms
- 5-DIBROMO-1H-1;sO|DEbLQxbSKfsSP@;3,5-dibromo-s-triazol;3,5-DIBROMO-S-TRIAZOLE;s-Triazole, 3,5-dibromo-;3,5-DIBROMO-1,2,4-TRIAZOLE;3,5-DIBROMO-1H-1,2,4-TRIAZOLE;3,5-DIBROMO-4H-1,2,4-TRIAZOLE;1H-1,2,4-Triazole, 3,5-dibroMo-;3,5-Dibromo-1H-1,2,4-triazole 97%
- CBNumber
- CB2116341
- Molecular Formula
- C2HBr2N3
- Formula Weight
- 226.86
- MOL File
- 7411-23-6.mol
3,5-DIBROMO-1H-1,2,4-TRIAZOLE Property
- Melting point:
- 201 °C
- Boiling point:
- 364.8±25.0 °C(Predicted)
- Density
- 2.620
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- powder to crystal
- pka
- 5.50±0.40(Predicted)
- color
- White to Light yellow
- InChI
- InChI=1S/C2HBr2N3/c3-1-5-2(4)7-6-1/h(H,5,6,7)
- InChIKey
- FRAKFBWDPXYIQO-UHFFFAOYSA-N
- SMILES
- N1C(Br)=NC(Br)=N1
- CAS DataBase Reference
- 7411-23-6(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi,Xn
- Risk Statements
- 36/37/38-20/21/22-22
- Safety Statements
- 26-36/37/39-22
- RTECS
- XZ4570000
- HazardClass
- IRRITANT
- HS Code
- 2933998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- CDS002983
- Product name
- 3,5-Dibromo-1H-1,2,4-triazole
- Purity
- AldrichCPR
- Packaging
- 250mg
- Price
- $73.1
- Updated
- 2025/07/31
- Product number
- D5030
- Product name
- 3,5-Dibromo-1,2,4-triazole
- Purity
- >97.0%(GC)
- Packaging
- 5g
- Price
- $83
- Updated
- 2025/07/31
- Product number
- D5030
- Product name
- 3,5-Dibromo-1,2,4-triazole
- Purity
- >97.0%(GC)
- Packaging
- 25g
- Price
- $329
- Updated
- 2025/07/31
- Product number
- D426145
- Product name
- 3,5-Dibromo-1h-1,2,4-triazole
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- FD124892
- Product name
- 3,5-Dibromo-1H-1,2,4-triazole
- Packaging
- 100g
- Price
- $280
- Updated
- 2021/12/16
3,5-DIBROMO-1H-1,2,4-TRIAZOLE Chemical Properties,Usage,Production
Uses
3,5-Dibromo-1H-1,2,4-triazole is used in organic synthesis.
Chemical Properties
Pale yellow or white powder
Synthesis
288-88-0
7411-23-6
General procedure for the synthesis of 3,5-dibromo-1H-1,2,4-triazole from 1H-1,2,4-triazole: a solution of bromine (6.1 mL, 119 mmol) in dichloromethane (DCM, 15 mL) and sodium hydroxide (6.78 g, 169 mmol) in water (20 mL) were added simultaneously and slowly dropwise to the stirred 1H-1,2,4- triazole (3.9 g, 56 mmol), water (50 mL) and DCM (15 mL) mixture at 0°C. The reaction temperature was controlled to be below 20°C during the dropwise addition. The reaction mixture was stirred at room temperature overnight. Subsequently, concentrated hydrochloric acid (2.0 mL, 66 mmol) was added to the reaction solution. The solid product was isolated by filtration, washed with water and dried under vacuum to afford the title compound 3,5-dibromo-1H-1,2,4-triazole as a solid (8.3 g, 65% yield). Mass spectrum (ESI) m/z 224 [M-H]-.
References
[1] Synthesis, 1998, # 9, p. 1357 - 1361
[2] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2014, vol. 53, # 5, p. 610 - 618
[3] Patent: WO2014/195321, 2014, A1. Location in patent: Page/Page column 15; 16
[4] Patent: WO2014/195322, 2014, A1. Location in patent: Page/Page column 15
[5] Patent: US2010/240619, 2010, A1. Location in patent: Page/Page column 68
3,5-DIBROMO-1H-1,2,4-TRIAZOLE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3,5-DIBROMO-1H-1,2,4-TRIAZOLE manufacturers
- Product
- 3,5-DIBROMO-1H-1,2,4-TRIAZOLE 7411-23-6
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 10000KGS
- Release date
- 2020-01-09