4-BROMO-2-IODOTOLUENE

Product Name: 4-BROMO-2-IODOTOLUENE
CAS No.: 260558-15-4
Chemical Name: 4-BROMO-2-IODOTOLUENE
Synonyms: 4-Bromo-2-iodo-1-methylbenzene;4-BROMO-2-IODOTOLUENE;2-Iodo-4-bromotoluene;4-Bromo-2-iodotoluene 98%;Benzene,4-bromo-2-iodo-1-methyl-;4-bromo-2-iodo-1-methylbenzene98%
CBNumber: CB2126793
Molecular Formula: C7H6BrI
Formula Weight: 296.93
MOL File: 260558-15-4.mol

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4-BROMO-2-IODOTOLUENE Property

Melting point:: 262-267℃
Boiling point:: 268℃
Density: 2.062
Flash point:: 116℃
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
Appearance: Colorless to light yellow Liquid

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Safety

HS Code: 2903998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: B693578
Product name: 4-Bromo-2-iodo-1-methylbenzene
Packaging: 250mg
Price: $55
Updated: 2021/12/16

TRC

Product number: B693578
Product name: 4-Bromo-2-iodo-1-methylbenzene
Packaging: 1g
Price: $75
Updated: 2021/12/16

Matrix Scientific

Product number: 115214
Product name: 4-Bromo-2-iodo-1-methylbenzene
Purity: >97%
Packaging: 500mg
Price: $49
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3730-S-07
Product name: 4-Bromo-2-iodotoluene
Packaging: 5G
Price: $200
Updated: 2021/12/16

AK Scientific

Product number: J96640
Product name: 4-Bromo-2-iodo-1-methylbenzene
Packaging: 10g
Price: $120
Updated: 2021/12/16

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4-BROMO-2-IODOTOLUENE Chemical Properties,Usage,Production

Synthesis

39478-78-9

260558-15-4

The general procedure for the synthesis of 4-bromo-2-iodo-1-methylbenzene from 2-amino-4-bromotoluene was as follows: intermediate 6 (4-bromo-2-iodo-1-methylbenzene) was synthesized in the scheme shown in Scheme 4, with the following experimental details. Step 1: 2-Methyl-5-bromoaniline (1.5 g, 8.06 mmol) was dissolved in diiodomethane (3.4 ml) at 0°C and tert-butyl nitrite (1.6 ml, 12.1 mmol) was slowly added. After removal of the ice bath, the reaction mixture was stirred at room temperature and subsequently heated at 80 °C for 30 min. Upon completion of the reaction, the solvent was removed by distillation under reduced pressure and the residue was purified by column chromatography (eluent: EtOAc/heptane) to afford the target compound 4-bromo-2-iodo-1-methylbenzene (1.6 g, 67% yield).LCMS analysis showed m/z 297 [M + H]+.1H NMR (300 MHz, CDCl3) δ: 7.96 (1H, s) 7.42-7.35 (1H, m), 7.12 (1H, d, J = 8.1 Hz), 2.40 (3H, s).

References

[1] Patent: US2011/39920, 2011, A1. Location in patent: Page/Page column 10
[2] Patent: WO2009/130434, 2009, A1. Location in patent: Page/Page column 21
[3] Patent: TW2016/9616, 2016, A. Location in patent: Paragraph 0161

4-BROMO-2-IODOTOLUENE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-BROMO-2-IODOTOLUENE Suppliers

China 108 India 3 United Kingdom 2 United States 10 Global 123

J & K SCIENTIFIC LTD.

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View Lastest Price from 4-BROMO-2-IODOTOLUENE manufacturers

Henan Fengda Chemical Co., Ltd

Product: 4-BROMO-2-IODOTOLUENE 260558-15-4
Price: US $101.00-1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2023-12-28

Career Henan Chemical Co

Product: 4-BROMO-2-IODOTOLUENE 260558-15-4
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2020-01-08

260558-15-4, 4-BROMO-2-IODOTOLUENERelated Search:

2-Bromo-4-chlorotoluene 2-Iodotoluene 4-BROMO-2-IODOTOLUENE 4-BROMO-2-IODOBENZONITRILE 4-BROMO-2-IODO-6-NITROTOLUENE 4-Bromo-2-iodo-6-methyl-benzamide 4-BROMO-5-FLUORO-2-IODOTOLUENE

4-BROMO-2-IODOTOLUENE

4-Bromo-2-iodo-1-methylbenzene

4-Bromo-2-iodotoluene 98%

Benzene,4-bromo-2-iodo-1-methyl-

2-Iodo-4-bromotoluene

4-bromo-2-iodo-1-methylbenzene98%

260558-15-4

Bromine Compounds

Iodine Compounds