3-CYANO-5-NITRO-BENZOIC ACID METHYL ESTER
- Product Name
- 3-CYANO-5-NITRO-BENZOIC ACID METHYL ESTER
- CAS No.
- 99066-80-5
- Chemical Name
- 3-CYANO-5-NITRO-BENZOIC ACID METHYL ESTER
- Synonyms
- 3-Cyano-5-nitro-benzoic acid meth;3-CYANO-5-NITRO-BENZOIC ACID METHYL ESTER;Benzoic acid, 3-cyano-5-nitro-, methyl ester;3-CYANO-5-NITRO-BENZOIC ACID METHYL ESTER >98%
- CBNumber
- CB2127866
- Molecular Formula
- C9H6N2O4
- Formula Weight
- 206.15
- MOL File
- 99066-80-5.mol
3-CYANO-5-NITRO-BENZOIC ACID METHYL ESTER Property
- Melting point:
- 137-138 °C
- Boiling point:
- 334.8±32.0 °C(Predicted)
- Density
- 1.39±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- crystals
- color
- Colourless
Safety
- HS Code
- 2916399090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- M338870
- Product name
- Methyl3-Cyano-5-nitrobenzoate
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 4654-1-21
- Product name
- Methyl 3-cyano-5-nitrobenzoate
- Purity
- 98.0%
- Packaging
- 250mg
- Price
- $50
- Updated
- 2021/12/16
- Product number
- 6940AC
- Product name
- Methyl3-cyano-5-nitrobenzoate
- Packaging
- 1g
- Price
- $158
- Updated
- 2021/12/16
- Product number
- 4654-1-21
- Product name
- Methyl 3-cyano-5-nitrobenzoate
- Purity
- 98.0%
- Packaging
- 1g
- Price
- $159
- Updated
- 2021/12/16
- Product number
- 6940AC
- Product name
- Methyl3-cyano-5-nitrobenzoate
- Packaging
- 5g
- Price
- $482
- Updated
- 2021/12/16
3-CYANO-5-NITRO-BENZOIC ACID METHYL ESTER Chemical Properties,Usage,Production
Synthesis
50826-00-1
99066-80-5
Methyl 3-methyl-3-carbamoyl-5-nitrobenzoate (30 mmol) was used as a starting material and dissolved in 1,2-dichloroethane (100 mL). POCl3 (33 mmol) was added to this solution and the reaction mixture was subsequently heated to reflux for 3 hours. After completion of the reaction, it was cooled to room temperature and the reaction solution was slowly poured into water. The organic layer was separated and washed sequentially with saturated NaHCO3 solution and brine. The organic layer was dried over anhydrous Na2SO4 and concentrated under reduced pressure to afford the target product methyl 3-cyano-5-nitrobenzoate in 90% yield.
References
[1] Patent: US2009/118292, 2009, A1. Location in patent: Page/Page column 29
[2] Patent: WO2011/137587, 2011, A1. Location in patent: Page/Page column 55
3-CYANO-5-NITRO-BENZOIC ACID METHYL ESTER Preparation Products And Raw materials
Raw materials
Preparation Products
3-CYANO-5-NITRO-BENZOIC ACID METHYL ESTER Suppliers
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- Country
- India
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