METHYL 2-METHOXYNICOTINATE
- Product Name
- METHYL 2-METHOXYNICOTINATE
- CAS No.
- 67367-26-4
- Chemical Name
- METHYL 2-METHOXYNICOTINATE
- Synonyms
- 2-Methoxy-nicotinic acid Methyl ester;2-methoxynicotinate;METHYL 2-METHOXYNICOTITE;2-methoxy-, methyl ester;METHYL 2-METHOXYNICOTINATE;[METHYL 2-METHOXYNICOTITE];Methyl 2-methoxypyridine-3-carboxylate;3-Pyridinecarboxylic acid, 2-methoxy-, methyl ester
- CBNumber
- CB2138619
- Molecular Formula
- C8H9NO3
- Formula Weight
- 167.16
- MOL File
- Mol file
METHYL 2-METHOXYNICOTINATE Property
- Boiling point:
- 114-115 °C(Press: 12 Torr)
- Density
- 1.156±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 1.36±0.10(Predicted)
- Appearance
- Colorless to light yellow Liquid
Safety
- Hazard Codes
- Xi
- HazardClass
- IRRITANT
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H225Highly Flammable liquid and vapour
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.
P233Keep container tightly closed.
P240Ground/bond container and receiving equipment.
P241Use explosion-proof electrical/ventilating/lighting/…/equipment.
P242Use only non-sparking tools.
P243Take precautionary measures against static discharge.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P370+P378In case of fire: Use … for extinction.
P403+P235Store in a well-ventilated place. Keep cool.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B451475
- Product name
- Methyl2-Methoxynicotinate
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 018136
- Product name
- Methyl 2-methoxynicotinate
- Purity
- 95+%
- Packaging
- 5g
- Price
- $19
- Updated
- 2021/12/16
- Product number
- X5985
- Product name
- Methyl2-methoxynicotinate
- Packaging
- 5g
- Price
- $27
- Updated
- 2021/12/16
- Product number
- 018136
- Product name
- Methyl 2-methoxynicotinate
- Purity
- 95+%
- Packaging
- 25g
- Price
- $47
- Updated
- 2021/12/16
- Product number
- 4H58-1-602
- Product name
- Methyl 2-methoxynicotinate
- Packaging
- 5G
- Price
- $68
- Updated
- 2021/12/16
METHYL 2-METHOXYNICOTINATE Chemical Properties,Usage,Production
Synthesis
67-56-1
16498-81-0
67367-26-4
General procedure for the synthesis of methyl 2-methoxynicotinate from methanol and 2-methoxynicotinic acid: a) Synthesis of methyl 2-methoxynicotinate: a concentrated aqueous sulfuric acid solution (0.1 mL) was slowly added to a solution of methanol (20 mL) containing 2-methoxynicotinic acid (2.00 g, 13.1 mmol), stirred to mix well and then heated to reflux. After the reaction was carried out for 6 hours, saturated aqueous sodium bicarbonate solution was added to the reaction mixture for neutralization, followed by extraction with ethyl acetate. The organic layer was separated, dried with anhydrous magnesium sulfate and concentrated under reduced pressure to afford the target product methyl 2-methoxynicotinate (1.85 g, 85% yield) as a colorless oil. Low resolution mass spectrometry (LRMS) showed m/z: 168 ([M + 1]+).1H NMR (300 MHz, DMSO-d6) δ ppm: 3.81 (s, 3H), 3.92 (s, 3H), 7.11 (dd, 1H), 8.13 (dd, 1H), 8.38 (dd, 1H).
References
[1] Patent: EP2397482, 2011, A1. Location in patent: Page/Page column 64
[2] Patent: WO2011/157397, 2011, A1. Location in patent: Page/Page column 119
METHYL 2-METHOXYNICOTINATE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from METHYL 2-METHOXYNICOTINATE manufacturers
- Product
- METHYL 2-METHOXYNICOTINATE 67367-26-4
- Price
- US $16.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1kg, 10kg, 50kg
- Release date
- 2020-03-09