2-methylsulfonylbenzaldehyde
- Product Name
- 2-methylsulfonylbenzaldehyde
- CAS No.
- 5395-89-1
- Chemical Name
- 2-methylsulfonylbenzaldehyde
- Synonyms
- 2-mesylbenzaldehyde;2-methylsulfonylbenzaldehyde;2-Methanesulfonylbenzaldehyde;2-(Methylsulphonyl)benzaldehyde;Benzaldehyde,2-(Methylsulfonyl)-;2-(Methylsulfonyl)-Benzaldehyde 97%
- CBNumber
- CB21456916
- Molecular Formula
- C8H8O3S
- Formula Weight
- 184.21
- MOL File
- 5395-89-1.mol
2-methylsulfonylbenzaldehyde Property
- Melting point:
- 98-99 °C(Solv: water (7732-18-5))
- Boiling point:
- 385.7±34.0 °C(Predicted)
- Density
- 1.289±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C, stored under nitrogen
- form
- solid
- Appearance
- White to off-white Solid
Safety
- HS Code
- 2913000090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M339158
- Product name
- 2-(Methylsulfonyl)benzaldehyde
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- CHM0299956
- Product name
- 2-(METHYLSULFONYL)BENZALDEHYDE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $498.47
- Updated
- 2021/12/16
- Product number
- W6824
- Product name
- 2-(Methylsulfonyl)benzaldehyde
- Packaging
- 100g
- Price
- $1651
- Updated
- 2021/12/16
- Product number
- 5395891
- Product name
- 2-Methylsulfonylbenzaldehyde
- Packaging
- 25g
- Price
- $749
- Updated
- 2021/12/16
- Product number
- 61-5278
- Product name
- 2-(methylsulfonyl)benzaldehyde
- Purity
- 97+%
- Packaging
- 1g
- Price
- $135
- Updated
- 2021/12/16
2-methylsulfonylbenzaldehyde Chemical Properties,Usage,Production
Synthesis
17696-73-0
446-52-6
5395-89-1
2-Fluorobenzaldehyde (12.4 g, 0.1 mol, 1 eq.) and methanesulfonic acid (11.2 g, 0.11 mol, 1.1 eq.) were dissolved in DMSO (75 ml) and heated to 100 °C for 16 hours. After completion of the reaction, the mixture was cooled to room temperature and poured into crushed ice (100 g). The resulting 2-(methylsulfonyl)benzaldehyde was collected by filtration and dried under vacuum at 45 °C for 16 h to give a yellow solid product (9.2 g, 50% yield). The product was characterized as follows: 1H NMR (300 MHz, CDCl3) δ 10.77 (1H, s, CHO), 8.18-8.16 (1H, m, ArH), 8.10-8.08 (1H, m, ArH), 7.83-7.80 (2H, m, ArH), 3.28 (3H, s, SO2CH3); LCMS (6 min) Rt = 1.93 min, (M++1) = 185.1.
References
[1] Patent: WO2004/52858, 2004, A2. Location in patent: Page 109
2-methylsulfonylbenzaldehyde Preparation Products And Raw materials
Raw materials
Preparation Products
2-methylsulfonylbenzaldehyde Suppliers
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- Country
- India
- ProdList
- 6100
- Advantage
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View Lastest Price from 2-methylsulfonylbenzaldehyde manufacturers
- Product
- 2-methylsulfonylbenzaldehyde 5395-89-1
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2019-12-25