3,6-dichloropyridazin-4-amine
- Product Name
- 3,6-dichloropyridazin-4-amine
- CAS No.
- 823-58-5
- Chemical Name
- 3,6-dichloropyridazin-4-amine
- Synonyms
- NSC 170664;4-Amino-3,6-dichL;3,6-Dichloro-4-Pyridazinamine;4-Amino-3,6-dihydropyridazine;3,6-dichloropyridazin-4-amine;3,6-Dichloro-4-aMinopyridazine;4-AMino-3,6-dicholropyridazine;4-AMino-3,6-dichloropyridazine;4-PyridazinaMine, 3,6-dichloro-;4-Amino-3,6-dichloropyridazine 98%
- CBNumber
- CB21457726
- Molecular Formula
- C4H3Cl2N3
- Formula Weight
- 163.99
- MOL File
- 823-58-5.mol
3,6-dichloropyridazin-4-amine Property
- Melting point:
- 203 °C
- Boiling point:
- 363.0±37.0 °C(Predicted)
- Density
- 1.606±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- form
- solid
- pka
- 2.08±0.10(Predicted)
- color
- Yellow-brown
- InChI
- InChI=1S/C4H3Cl2N3/c5-3-1-2(7)4(6)9-8-3/h1H,(H2,7,8)
- InChIKey
- HODYDVHWWMTUEL-UHFFFAOYSA-N
- SMILES
- C1(Cl)=NN=C(Cl)C=C1N
Safety
- HS Code
- 2933998090
N-Bromosuccinimide Price
- Product number
- D438165
- Product name
- 3,6-Dichloropyridazin-4-amine
- Packaging
- 1g
- Price
- $55
- Updated
- 2021/12/16
- Product number
- 074414
- Product name
- 4-Amino-3,6-dichloropyridazine
- Purity
- 95+%
- Packaging
- 1g
- Price
- $13
- Updated
- 2021/12/16
- Product number
- OR304307
- Product name
- 4-Amino-3,6-dichloropyridazine
- Purity
- 98%
- Packaging
- 1g
- Price
- $29
- Updated
- 2021/12/16
- Product number
- 3H30-5-1B
- Product name
- 4-Amino-3,6-dichloropyridazine
- Packaging
- 1g
- Price
- $32
- Updated
- 2021/12/16
- Product number
- 074414
- Product name
- 4-Amino-3,6-dichloropyridazine
- Purity
- 95+%
- Packaging
- 5g
- Price
- $41
- Updated
- 2021/12/16
3,6-dichloropyridazin-4-amine Chemical Properties,Usage,Production
Synthesis
6082-66-2
823-58-5
General procedure for the synthesis of 3,6-dichloropyridazin-4-amine from 3,4,6-trichloropyridazine: Example 24A: 3,4,6-Trichloropyridazine (25 g, 136 mmol) was added to a 500 mL stainless steel pressure flask containing 14.8 N ammonium hydroxide solution (200 mL). The reaction mixture was stirred at 75°C for 16 hours. Upon completion of the reaction, the mixture was cooled to room temperature and the solid product was collected by filtration to afford 17 g (76% yield) of the target compound 3,6-dichloropyridazin-4-amine. The product characterization data were as follows: 1H NMR (400 MHz, DMSO-d6) δ ppm 7.16 (s, 2H), 6.82 (s, 1H); MS (ESI+) m/z 164 (M+H)+.
References
[1] Journal of Organic Chemistry, 2014, vol. 79, # 21, p. 10311 - 10322
[2] Patent: US2017/15675, 2017, A1. Location in patent: Paragraph 1001
[3] Patent: US2009/163489, 2009, A1. Location in patent: Page/Page column 51
[4] Patent: US2014/349990, 2014, A1. Location in patent: Paragraph 1051; 1052
[5] Patent: WO2014/191896, 2014, A1. Location in patent: Page/Page column 217; 218
3,6-dichloropyridazin-4-amine Preparation Products And Raw materials
Raw materials
Preparation Products
3,6-dichloropyridazin-4-amine Suppliers
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- sales@ajchem.in
- Country
- India
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View Lastest Price from 3,6-dichloropyridazin-4-amine manufacturers
- Product
- 3,6-dichloropyridazin-4-amine 823-58-5
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-10-18
- Product
- 3,6-dichloropyridazin-4-amine 823-58-5
- Price
- US $0.00-0.00/KG
- Min. Order
- 1g
- Purity
- 99%minHPLC
- Supply Ability
- 50kgs/month
- Release date
- 2021-11-05
- Product
- 3,6-Dichloropyridazin-4-amine 823-58-5
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98.8%
- Supply Ability
- 100 tons
- Release date
- 2022-02-18