ChemicalBook > CAS DataBase List > 3-Amino-2-iodo-6-(trifluoromethyl)-pyridine

3-Amino-2-iodo-6-(trifluoromethyl)-pyridine

Product Name: 3-Amino-2-iodo-6-(trifluoromethyl)-pyridine
CAS No.: 920979-04-0
Chemical Name: 3-Amino-2-iodo-6-(trifluoromethyl)-pyridine
Synonyms: 124947;3-Amino-6-iodo-2-trifluoromethylpyridine;5-Amino-6-iodo-2-(trifluoromethyl)pyridine;2-IODO-6-TRIFLUOROMETHYL-PYRIDIN-3-YLAMINE;3-Amino-2-iodo-6-(trifluoromethyl)-pyridine;3-Pyridinamine, 2-iodo-6-(trifluoromethyl)-;2-IODO-6-( TRIFLUOROMETHYL) PYRIDINE-3- AMINE
CBNumber: CB21471179
Molecular Formula: C6H4F3IN2
Formula Weight: 288.01
MOL File: 920979-04-0.mol

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3-Amino-2-iodo-6-(trifluoromethyl)-pyridine Property

storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
Appearance: White to off-white Solid

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Apolloscientific

Product number: PC446152
Product name: 2-Iodo-6-(trifluoromethyl)pyridin-3-ylamine
Purity: 95+%
Packaging: 1g
Price: $356
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0363905
Product name: 2-IODO-6-(TRIFLUOROMETHYL)PYRIDIN-3-AMINE
Purity: 95.00%
Packaging: 5MG
Price: $500.76
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H30-K-02
Product name: 2-Iodo-6-(trifluoromethyl)pyridin-3-ylamine
Purity: 95.0%
Packaging: 1g
Price: $570
Updated: 2021/12/16

AK Scientific

Product number: 5557AC
Product name: 2-Iodo-6-(trifluoromethyl)pyridin-3-amine
Packaging: 10g
Price: $1339
Updated: 2021/12/16

Alichem

Product number: 920979040
Product name: 3-Amino-2-iodo-6-(trifluoromethyl)pyridine
Packaging: 5g
Price: $1594.73
Updated: 2021/12/16

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3-Amino-2-iodo-6-(trifluoromethyl)-pyridine Chemical Properties,Usage,Production

Synthesis

106877-33-2

920979-04-0

General procedure for the preparation of Example IV 3-amino-2-iodo-6-(trifluoromethyl)pyridine: 3.85 g (12.3 mmol) of silver sulfate was added to a 100 mL ethanol solution containing 2 g (12.3 mmol) of 5-amino-2-(trifluoromethyl)pyridine under stirring and room temperature conditions. Subsequently, 3.13 g of iodine was added to the reaction system and stirred continuously for 24 hours at room temperature. Upon completion of the reaction, the suspended solids in the reaction medium were removed by filtration and the filtrate was concentrated under reduced pressure. The concentrated residue was dissolved in 200 mL of dichloromethane, washed sequentially with 5% sodium hydroxide solution and water, and the organic phase was dried with magnesium sulfate. Finally, the dried organic phase was concentrated under reduced pressure to afford 3.42 g of the target product 3-amino-2-iodo-6-(trifluoromethyl)pyridine as a pink solid in 96% yield and with a melting point of 127 °C.

References

[1] Patent: US2008/200495, 2008, A1. Location in patent: Page/Page column 6
[2] Patent: US2008/125459, 2008, A1. Location in patent: Page/Page column 16
[3] Patent: US2009/42873, 2009, A1. Location in patent: Page/Page column 25
[4] Patent: US2010/41634, 2010, A1. Location in patent: Page/Page column 19-20
[5] Patent: WO2010/91310, 2010, A1. Location in patent: Page/Page column 142

3-Amino-2-iodo-6-(trifluoromethyl)-pyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Amino-2-iodo-6-(trifluoromethyl)-pyridine Suppliers

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920979-04-0, 3-Amino-2-iodo-6-(trifluoromethyl)-pyridineRelated Search:

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