ChemicalBook > CAS DataBase List > 2-METHYL-6-HYDRAZINOPYRIDINE

2-METHYL-6-HYDRAZINOPYRIDINE

Product Name
2-METHYL-6-HYDRAZINOPYRIDINE
CAS No.
5315-24-2
Chemical Name
2-METHYL-6-HYDRAZINOPYRIDINE
Synonyms
5-Methoxypyrazin-2-amin;2-METHYL-6-HYDRAZINOPYRIDIN;2-METHYL-6-HYDRAZINOPYRIDINE;2-Hydrazinyl-6-methylpyridine;Pyridine, 2-hydrazinyl-6-methyl-;2-Hydrazinyl-6-Methylpyridine(WXC01942);2-hydrazino-6-methylpyridine(SALTDATA: 1.3HCl 0.7H2O)
CBNumber
CB21482472
Molecular Formula
C6H9N3
Formula Weight
123.16
MOL File
5315-24-2.mol
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2-METHYL-6-HYDRAZINOPYRIDINE Property

Melting point:
54-56 °C
Boiling point:
80-85 °C(Press: 0.5 Torr)
Density 
1.16±0.1 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Store in freezer, under -20°C
pka
9.73±0.70(Predicted)
Appearance
Off-white to yellow Solid
InChI
InChI=1S/C6H9N3/c1-5-3-2-4-6(8-5)9-7/h2-4H,7H2,1H3,(H,8,9)
InChIKey
RDVGWJKUYXVTSO-UHFFFAOYSA-N
SMILES
C1(NN)=NC(C)=CC=C1
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H317May cause an allergic skin reaction

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P272Contaminated work clothing should not be allowed out of the workplace.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P333+P313IF SKIN irritation or rash occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P363Wash contaminated clothing before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
H716515
Product name
2-Hydrazinyl-6-methylpyridine
Packaging
100mg
Price
$45
Updated
2021/12/16
ChemScene
Product number
CS-W021701
Product name
2-Hydrazinyl-6-methylpyridine
Purity
>97.0%
Packaging
1g
Price
$60
Updated
2021/12/16
ChemScene
Product number
CS-W021701
Product name
2-Hydrazinyl-6-methylpyridine
Purity
>97.0%
Packaging
5g
Price
$180
Updated
2021/12/16
AK Scientific
Product number
W6763
Product name
2-Hydrazinyl-6-methylpyridine
Packaging
1g
Price
$275
Updated
2021/12/16
ChemScene
Product number
CS-W021701
Product name
2-Hydrazinyl-6-methylpyridine
Purity
>97.0%
Packaging
10g
Price
$300
Updated
2021/12/16
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2-METHYL-6-HYDRAZINOPYRIDINE Chemical Properties,Usage,Production

Synthesis

18368-63-3

5315-24-2

General procedure for the synthesis of 2-methyl-6-hydrazinopyridine from 2-chloro-6-methylpyridine: [0719] A mixture of 2-chloro-6-methylpyridine (5 g, 39.19 mmol) with an excess of hydrazine hydrate (20 g, 391.94 mmol) was reacted by refluxing the reaction for 36 hours at 119°C. Upon completion of the reaction, unreacted hydrazine hydrate was removed by concentration under reduced pressure. The residue was diluted with deionized water (30 ml) and extracted with dichloromethane (30 ml x 3). The organic layers were combined, washed with saturated saline (30 ml), dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give the crude product. The crude product was purified by recrystallization from petroleum ether (15 ml) at -10 °C to afford 2-methyl-6-hydrazinopyridine (2.40 g, yield: 49.35%) as a black-brown solid.1H NMR (400 MHz, DMSO-d6) δ 7.39-7.29 (m, 1H), 7.25 (s, 1H), 6.51 (d, J = 8.4 Hz. 1H), 6.39 (d, J = 7.3 Hz, 1H), 4.06 (s, 2H), 2.26 (s, 3H).MS (ESI) m/z (M + H) + 127.8.

References

[1] Patent: US2003/187014, 2003, A1
[2] Patent: WO2018/64119, 2018, A1. Location in patent: Paragraph 0719
[3] Patent: US4622401, 1986, A
[4] Bioorganic and Medicinal Chemistry Letters, 2013, vol. 23, # 6, p. 1743 - 1747

2-METHYL-6-HYDRAZINOPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-METHYL-6-HYDRAZINOPYRIDINE manufacturers

Career Henan Chemical Co
Product
2-METHYL-6-HYDRAZINOPYRIDINE 5315-24-2
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100KG
Release date
2020-01-08

5315-24-2, 2-METHYL-6-HYDRAZINOPYRIDINERelated Search:

6-METHYL-4-(TRIFLUOROMETHYL)PYRID-2-YL HYDRAZINE 1-(6-METHYL-4-(TRIFLUOROMETHYL)PYRID-2-YL)-1-METHYLHYDRAZINE 2-HYDRAZINO-6-(TRIFLUOROMETHYL)PYRIDINE N'-METHYL-N'-[4-METHYL-3-(METHYLSULFONYL)-6-PHENYL-2-PYRIDINYL]CYCLOPROPANECARBOHYDRAZIDE 2-hydrazino-4,6-bis(trifluoromethyl)pyridine 4-METHYL-2-(1-METHYLHYDRAZINO)-3-(METHYLSULFONYL)-6-PHENYLPYRIDINE 3,4-DICHLORO-N'-[4,6-DIMETHYL-3-(METHYLSULFONYL)-2-PYRIDINYL]-N'-METHYLBENZENECARBOHYDRAZIDE 1-(6-(trifluoromethyl)pyridin-2-yl)-1-methylhydrazine N'-[4,6-DIMETHYL-3-(METHYLSULFONYL)-2-PYRIDINYL]-2,6-DIFLUORO-N'-METHYLBENZENECARBOHYDRAZIDE N'-[4,6-DIMETHYL-3-(METHYLSULFONYL)-2-PYRIDINYL]-3-METHOXY-N'-METHYLBENZENECARBOHYDRAZIDE 4-METHYL-2-(1-METHYLHYDRAZINO)-3-[(4-METHYLPHENYL)SULFONYL]-6-PHENYLPYRIDINE N',2,2-TRIMETHYL-N'-[4-METHYL-3-(METHYLSULFONYL)-6-PHENYL-2-PYRIDINYL]PROPANOHYDRAZIDE 2-HYDRAZINO-4,6-DIMETHYL-3-(METHYLSULFONYL)PYRIDINE 2,6-DIFLUORO-N'-METHYL-N'-[4-METHYL-3-(METHYLSULFONYL)-6-PHENYL-2-PYRIDINYL]BENZENECARBOHYDRAZIDE 2-HYDRAZINO-4,6-DIMETHYLNICOTINONITRILE 4-METHOXY-N'-METHYL-N'-[4-METHYL-3-(METHYLSULFONYL)-6-PHENYL-2-PYRIDINYL]BENZENECARBOHYDRAZIDE 4-CHLORO-N'-METHYL-N'-[4-METHYL-3-(METHYLSULFONYL)-6-PHENYL-2-PYRIDINYL]BENZENECARBOHYDRAZIDE N'3-[6-METHYL-4-(TRIFLUOROMETHYL)-2-PYRIDYL]-5-CHLORO-1-METHYL-1H-PYRAZOLE-3-CARBOHYDRAZIDE

  • 2-METHYL-6-HYDRAZINOPYRIDINE
  • 2-Hydrazinyl-6-methylpyridine
  • 2-hydrazino-6-methylpyridine(SALTDATA: 1.3HCl 0.7H2O)
  • Pyridine, 2-hydrazinyl-6-methyl-
  • 2-Hydrazinyl-6-Methylpyridine(WXC01942)
  • 5-Methoxypyrazin-2-amin
  • 2-METHYL-6-HYDRAZINOPYRIDIN
  • 5315-24-2
  • Heterocycle-Pyridine series
  • amine