1-Methyl-1H-indazol-4-ylamine
- Product Name
- 1-Methyl-1H-indazol-4-ylamine
- CAS No.
- 77894-69-0
- Chemical Name
- 1-Methyl-1H-indazol-4-ylamine
- Synonyms
- 1-methylindazol-4-amine;4-AMino-1-Methylindazole;1-Methyl-1H-indazol-4-amine;1-Methyl-4-aMino-1h-indazole;1H-Indazol-4-aMine,1-Methyl-;1-Methyl-1H-indazole-4-amine;1-Methyl-1H-indazol-4-ylamine;1-Methyl-1H-indazol-4-amine, CAS 77894-69-0
- CBNumber
- CB21501203
- Molecular Formula
- C8H9N3
- Formula Weight
- 147.18
- MOL File
- 77894-69-0.mol
1-Methyl-1H-indazol-4-ylamine Property
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- form
- solid
- color
- Light yellow to brown
Safety
- HS Code
- 2933998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M782560
- Product name
- 1-methyl-1H-indazol-4-amine
- Packaging
- 25mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- W8430
- Product name
- 1-Methyl-1H-indazol-4-amine
- Packaging
- 250mg
- Price
- $144
- Updated
- 2021/12/16
- Product number
- 3H30-1-K7
- Product name
- 4-Amino-1-methyl-1H-indazole
- Packaging
- 1g
- Price
- $223
- Updated
- 2021/12/16
- Product number
- 069652
- Product name
- 1-Methyl-1H-indazol-4-ylamine
- Purity
- 98%
- Packaging
- 5g
- Price
- $650
- Updated
- 2021/12/16
- Product number
- W8430
- Product name
- 1-Methyl-1H-indazol-4-amine
- Packaging
- 5g
- Price
- $651
- Updated
- 2021/12/16
1-Methyl-1H-indazol-4-ylamine Chemical Properties,Usage,Production
Synthesis
26120-43-4
77894-69-0
General procedure for the synthesis of 1-methyl-1H-indazol-4-amine from 1-methyl-4-nitro-1H-indazole: A catalytic amount of 10% palladium carbon was added to a solution of 1-methyl-4-nitro-1H-indazole (0.97 g, 5.5 mmol) in ethanol (50 ml). The resulting mixture was stirred under hydrogen atmosphere for 2 hours. Upon completion of the reaction, the catalyst was removed by filtration followed by evaporation of the solvent. The product was dried by azeotropy with toluene to give 1-methyl-1H-indazol-4-amine as a light brown solid (0.78 g, 96% yield). Mass spectrum (electrospray positive ion mode) m/z: 148 ([M+H]+).
References
[1] Patent: WO2004/46133, 2004, A1. Location in patent: Page 28
[2] Patent: WO2005/28445, 2005, A2. Location in patent: Page/Page column 36
[3] Heterocycles, 2006, vol. 68, # 12, p. 2595 - 2605
[4] Bioorganic and Medicinal Chemistry, 2006, vol. 14, # 14, p. 4740 - 4749
[5] Bioorganic and Medicinal Chemistry, 2015, vol. 23, # 17, p. 6025 - 6035
1-Methyl-1H-indazol-4-ylamine Preparation Products And Raw materials
Raw materials
Preparation Products
1-Methyl-1H-indazol-4-ylamine Suppliers
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View Lastest Price from 1-Methyl-1H-indazol-4-ylamine manufacturers
- Product
- 1-Methyl-1H-indazol-4-ylamine 77894-69-0
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 150KG
- Release date
- 2019-07-09