1-Benzhydryl-3-iodoazetidine

Product Name: 1-Benzhydryl-3-iodoazetidine
CAS No.: 125735-40-2
Chemical Name: 1-Benzhydryl-3-iodoazetidine
Synonyms: N-Benzhydryl-3-iodoazetidine;1-Benzhydryl-3-iodoazetidine;3-Iodo-N-benzhydrylazetidine;Azetidine, 1-(diphenylMethyl)-3-iodo-;1-diphenylmethyl-3-iodoazacyclobutane;1-Diphenylmethyl-3-iodazo heterocyclic butane
CBNumber: CB21570540
Molecular Formula: C16H16IN
Formula Weight: 349.21
MOL File: 125735-40-2.mol

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1-Benzhydryl-3-iodoazetidine Property

Melting point:: 101～102℃
Boiling point:: 377℃
Density: 1.55
Flash point:: 182℃
storage temp.: 2-8°C(protect from light)
pka: 6.16±0.10(Predicted)
Appearance: White to yellow Solid
InChI: InChI=1S/C16H16IN/c17-15-11-18(12-15)16(13-7-3-1-4-8-13)14-9-5-2-6-10-14/h1-10,15-16H,11-12H2
InChIKey: IBCVAYQWXMWFLD-UHFFFAOYSA-N
SMILES: N1(C(C2=CC=CC=C2)C2=CC=CC=C2)CC(I)C1

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Safety

HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC

Product number: B279173
Product name: 1-Benzhydryl-3-iodoazetidine
Packaging: 50mg
Price: $45
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-H-0E
Product name: 1-Benzhydryl-3-iodoazetidine
Purity: 98%
Packaging: 1g
Price: $175
Updated: 2021/12/16

Matrix Scientific

Product number: 093254
Product name: 1-Benzhydryl-3-iodoazetidine
Purity: 95+%
Packaging: 250mg
Price: $454
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-H-0E
Product name: 1-Benzhydryl-3-iodoazetidine
Purity: 98%
Packaging: 5G
Price: $496
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0354661
Product name: 1-BENZHYDRYL-3-IODOAZETIDINE
Purity: 95.00%
Packaging: 5MG
Price: $504.45
Updated: 2021/12/16

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1-Benzhydryl-3-iodoazetidine Chemical Properties,Usage,Production

Uses

1-Benzhydryl-3-iodoazetidine is a useful research reagent used in the synthetic preparation of other pharmacologically active molecules.

Synthesis

33301-41-6

125735-40-2

Step 1: Potassium iodide (530 mg, 3.14 mmol) was added to a mixed solution of 1-diphenylmethyl-3-methanesulfonic acid azetidine (500 mg, 1.57 mmol) in water (2.5 mL) and 1,2-dimethoxyethane (2.5 mL). The reaction mixture was stirred at room temperature and then heated to reflux and stirred continuously for 3 hours. After the reaction was completed, it was cooled to room temperature and diluted with water (50 mL) and ethyl acetate (50 mL). The aqueous phase was separated and extracted with ethyl acetate (2 x 70 mL). The organic phases were combined, washed with saturated sodium chloride solution (40 mL), dried over anhydrous sodium sulfate, filtered and concentrated to dryness to give 1-diphenylmethyl-3-iodoazetidine as a yellow solid (550 mg, 100% yield).LCMS (ESI-APCI) m/z 350.0 (M + H)+.

References

[1] Patent: WO2011/61214, 2011, A1. Location in patent: Page/Page column 159-160
[2] Patent: EP992493, 2000, A1
[3] Patent: EP962457, 1999, A1

1-Benzhydryl-3-iodoazetidine Preparation Products And Raw materials

Raw materials

Preparation Products

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1-Benzhydryl-3-iodoazetidine Suppliers

China 72 India 1 Switzerland 1 United States 7 Global 81

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View Lastest Price from 1-Benzhydryl-3-iodoazetidine manufacturers

Career Henan Chemical Co

Product: 1-Benzhydryl-3-iodoazetidine 125735-40-2
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2020-01-02

125735-40-2, 1-Benzhydryl-3-iodoazetidineRelated Search:

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1-Benzhydryl-3-iodoazetidine

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1-Diphenylmethyl-3-iodazo heterocyclic butane

1-diphenylmethyl-3-iodoazacyclobutane

125735-40-2

C16H16IN