DODECANEDIOIC ACID MONOMETHYL ESTER
- Product Name
- DODECANEDIOIC ACID MONOMETHYL ESTER
- CAS No.
- 3903-40-0
- Chemical Name
- DODECANEDIOIC ACID MONOMETHYL ESTER
- Synonyms
- NSC 29000;MONOMETHYL-DODECANEDIOATE;Methyl 11-Carboxyundecanoate;MonoMethyl 1,12-Dodecanedioate;12-keto-12-methoxy-lauric acid;11-CarboMethoxyundecanoic Acid;MONOMETHYL DODECANE-1,12-DIOATE;12-methoxy-12-oxododecanoic acid;Dodecanedioic Acid 1-Methyl Ester;12-methoxy-12-oxo-dodecanoic acid
- CBNumber
- CB2157375
- Molecular Formula
- C13H24O4
- Formula Weight
- 244.33
- MOL File
- 3903-40-0.mol
DODECANEDIOIC ACID MONOMETHYL ESTER Property
- Melting point:
- 51.5-52 °C
- Boiling point:
- 170 °C(Press: 3 Torr)
- Density
- 1.012±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- DMSO (Slightly, Heated), Methanol (Slightly)
- form
- Solid
- pka
- 4.78±0.10(Predicted)
- color
- White
- InChI
- InChI=1S/C13H24O4/c1-17-13(16)11-9-7-5-3-2-4-6-8-10-12(14)15/h2-11H2,1H3,(H,14,15)
- InChIKey
- REGGDLIBDASKGE-UHFFFAOYSA-N
- SMILES
- C(OC)(=O)CCCCCCCCCCC(O)=O
Safety
- HS Code
- 2917198090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D494535
- Product name
- DodecanedioicAcid1-MethylEster
- Packaging
- 2g
- Price
- $250
- Updated
- 2021/12/16
- Product number
- 010920
- Product name
- Dodecanedioic Acid 1-Methyl Ester
- Packaging
- 1g
- Price
- $403
- Updated
- 2021/12/16
- Product number
- FD22587
- Product name
- Dodecanedioic acid 1-methyl ester
- Packaging
- 100g
- Price
- $300
- Updated
- 2021/12/16
- Product number
- FD22587
- Product name
- Dodecanedioic acid 1-methyl ester
- Packaging
- 250g
- Price
- $500
- Updated
- 2021/12/16
- Product number
- CHM0029391
- Product name
- DODECANEDIOIC ACID MONOMETHYL ESTER
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $704.55
- Updated
- 2021/12/16
DODECANEDIOIC ACID MONOMETHYL ESTER Chemical Properties,Usage,Production
Chemical Properties
White Solid
Uses
Used in cosmetic compositions.
Uses
Dodecanedioic Acid 1-Methyl Ester is used in cosmetic composition.
Synthesis
1731-79-9
3903-40-0
Synthesis of compound 2: To a stirred solution of dimethyl dodecanedioate 1 (200 g, 774.65 mmol) in a mixed solvent of diethyl ether and acetonitrile, potassium hydroxide (891.4 mmol) dissolved in methanol was slowly added, keeping the reaction temperature between 0-5°C for 1 hour. Subsequently, the reaction mixture was continued to be stirred at the same temperature for 48 hours. Upon completion of the reaction, the white solid in the reaction mixture was filtered using a sintered funnel and washed with diethyl ether (100 mL) followed by suction drying for 3 hours. The resulting white solid was dissolved in water (500 mL), acidified to pH 3-4 with 1N hydrochloric acid solution, filtered to collect the precipitated white solid and washed with water (50 mL x 2). Finally, the product was air-dried in air for 1 day and then dried in the presence of phosphorus pentoxide to give monomethyl dodecanedioate 2 (166 g, 88% yield) as a white powder.
References
[1] Patent: WO2014/25805, 2014, A1. Location in patent: Page/Page column 33
[2] Bioorganic and Medicinal Chemistry Letters, 2004, vol. 14, # 16, p. 4253 - 4256
[3] Chemische Berichte, 1983, vol. 116, # 2, p. 761 - 776
[4] Helvetica Chimica Acta, 2005, vol. 88, # 9, p. 2470 - 2478
[5] Synthesis, 2010, # 7, p. 1150 - 1158
DODECANEDIOIC ACID MONOMETHYL ESTER Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from DODECANEDIOIC ACID MONOMETHYL ESTER manufacturers
- Product
- Dodecanedioic acid monomethyl ester 3903-40-0
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-09-28
- Product
- DODECANEDIOIC ACID MONOMETHYL ESTER 3903-40-0
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20T
- Release date
- 2024-08-15
- Product
- DODECANEDIOIC ACID MONOMETHYL ESTER 3903-40-0
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 200kg
- Release date
- 2019-08-30