N-(3-Bromophenyl)methansulfonamide

Product Name: N-(3-Bromophenyl)methansulfonamide
CAS No.: 83922-51-4
Chemical Name: N-(3-Bromophenyl)methansulfonamide
Synonyms: N-(3-Bromophenyl)methansulfonamide;3-BROMO PHENYL METHANE SULPHONAMIDE;3-(methylsulfonyl)amino-1-bromo-benzene
CBNumber: CB22130976
Molecular Formula: C7H8BrNO2S
Formula Weight: 250.11
MOL File: 83922-51-4.mol

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N-(3-Bromophenyl)methansulfonamide Property

Boiling point:: 330.7±44.0 °C(Predicted)
Density: 1.711±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 7.47±0.10(Predicted)
Appearance: White to gray Solid

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Safety

HS Code: 2935909099

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC

Product number: B698330
Product name: N-(3-Bromophenyl)methanesulfonamide
Packaging: 1g
Price: $75
Updated: 2021/12/16

BroadPharm

Product number: BP-21291
Product name: N-(3-BROMOPHENYL)METHANESULFONAMIDE
Packaging: 1g
Price: $106
Updated: 2021/12/16

AK Scientific

Product number: X5390
Product name: N-(3-Bromophenyl)methansulfonamide
Packaging: 5g
Price: $192
Updated: 2021/12/16

SynQuest Laboratories

Product number: 8669-9-57
Product name: N-(3-Bromophenyl)methanesulfonamide
Packaging: 1g
Price: $245
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0137515
Product name: METHANESULFONAMIDE, N-(3-BROMOPHENYL)-
Purity: 95.00%
Packaging: 1G
Price: $721.57
Updated: 2021/12/16

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N-(3-Bromophenyl)methansulfonamide Chemical Properties,Usage,Production

Synthesis

124-63-0

591-19-5

83922-51-4

Step i: To a stirred solution of anhydrous dichloromethane (200 ml) of m-bromoaniline (6 g, 34.87 mmol) was sequentially added pyridine (4.13 mg, 52.31 mmol) and methanesulfonyl chloride (5.194 g, 45.34 mmol) at 10 °C. The reaction mixture was stirred at room temperature for 15 h. The progress of the reaction was monitored by thin layer chromatography (TLC, the unfolding agent was a hexane solution of 35% ethyl acetate). After completion of the reaction, the reaction mixture was diluted with dichloromethane (50 ml) and washed with 1N hydrochloric acid (25 ml). The organic layer was dried with anhydrous sodium sulfate and concentrated under reduced pressure to give N-(3-bromophenyl)methane sulfonamide 8.45 g in 96.3% yield. The product was structurally confirmed by 1H NMR (DMSO-d6, 300 MHz) and mass spectrometry (MS: m/z = 251.8 [M + 1]).

References

[1] Patent: WO2014/6554, 2014, A1. Location in patent: Page/Page column 28
[2] Synthetic Communications, 2004, vol. 34, # 20, p. 3807 - 3819
[3] Patent: WO2017/18803, 2017, A1. Location in patent: Paragraph 791; 792; 793
[4] Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, 1982, vol. 38, # 7, p. 791 - 796
[5] Heterocycles, 2001, vol. 54, # 1, p. 105 - 108

N-(3-Bromophenyl)methansulfonamide Preparation Products And Raw materials

Raw materials

Preparation Products

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N-(3-Bromophenyl)methansulfonamide Suppliers

China 42 India 3 United Kingdom 1 United States 5 Global 51

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83922-51-4, N-(3-Bromophenyl)methansulfonamideRelated Search:

N-(3-Bromophenyl)methansulfonamide 4-amino-N-(3-bromophenyl)benzenesulfonamide 3-AMINO-N-(3-BROMO-4-ETHOXY-PHENYL)-4-CHLORO-BENZENESULFONAMIDE N-(3-bromophenyl)-4-methylbenzenesulfonamide 4-bromo-N-(3-bromophenyl)benzene-1-sulfonamide (3-BROMOPHENYL)((2,4,6-TRIMETHYLPHENYL)SULFONYL)AMINE 5-AMINO-N-(3-BROMO-4-METHOXY-PHENYL)-2-METHOXY-BENZENESULFONAMIDE N-(3-BROMOPHENYL)-4-[(2-CHLORO-1,3-THIAZOL-5-YL)METHOXY]BENZENESULFONAMIDE 3-AMINO-N-(3-BROMO-4-ETHOXY-PHENYL)-4-METHOXY-BENZENESULFONAMIDE 5-AMINO-N-(3-BROMO-4-ETHOXY-PHENYL)-2-CHLORO-BENZENESULFONAMIDE 5-AMINO-N-(3-BROMO-4-ETHOXY-PHENYL)-2-METHOXY-BENZENESULFONAMIDE 3-(3-BROMO-4-ETHOXY-PHENYLSULFAMOYL)-BENZOIC ACID N-(3-bromophenyl)-4-chlorobenzene-1-sulfonamide N-(3-bromophenyl)-1-phenylmethanesulfonamide N-(3-bromophenyl)-4-fluorobenzenesulfonamide N-(3-bromophenyl)ethanesulfonamide N-(3-bromophenyl)benzenesulfonamide N-(3-bromophenyl)thiophene-2-sulfonamide

N-(3-Bromophenyl)methansulfonamide

3-(methylsulfonyl)amino-1-bromo-benzene

3-BROMO PHENYL METHANE SULPHONAMIDE

83922-51-4

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