4-METHOXY-1H-PYRAZOLO[3,4-D]PYRIMIDIN-6-AMINE
- Product Name
- 4-METHOXY-1H-PYRAZOLO[3,4-D]PYRIMIDIN-6-AMINE
- CAS No.
- 100644-67-5
- Chemical Name
- 4-METHOXY-1H-PYRAZOLO[3,4-D]PYRIMIDIN-6-AMINE
- Synonyms
- 6-Amino-4-methoxypyrazolo[3,4-d]pyrimidine;4-METHOXY-1H-PYRAZOLO[3,4-D]PYRIMIDIN-6-AMINE;6-AMINO-4-METHOXY-1H-PYRAZOLO[3,4-D]PYRIMIDINE;4-Methoxy-1H-pyrazolo[3,4-d]pyrimidin-6-ylamine;1H-Pyrazolo[3,4-d]pyrimidin-6-amine, 4-methoxy-
- CBNumber
- CB22449500
- Molecular Formula
- C6H7N5O
- Formula Weight
- 165.15
- MOL File
- 100644-67-5.mol
4-METHOXY-1H-PYRAZOLO[3,4-D]PYRIMIDIN-6-AMINE Property
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
N-Bromosuccinimide Price
- Product number
- FA145048
- Product name
- 6-Amino-4-methoxypyrazolo[3,4-d]pyrimidine
- Packaging
- 10mg
- Price
- $50
- Updated
- 2021/12/16
- Product number
- FA145048
- Product name
- 6-Amino-4-methoxypyrazolo[3,4-d]pyrimidine
- Packaging
- 25mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- FA145048
- Product name
- 6-Amino-4-methoxypyrazolo[3,4-d]pyrimidine
- Packaging
- 50mg
- Price
- $125
- Updated
- 2021/12/16
- Product number
- FA145048
- Product name
- 6-Amino-4-methoxypyrazolo[3,4-d]pyrimidine
- Packaging
- 100mg
- Price
- $200
- Updated
- 2021/12/16
- Product number
- 0244AA
- Product name
- 4-Methoxy-1H-pyrazolo[3,4-d]pyrimidin-6-amine
- Packaging
- 100mg
- Price
- $428
- Updated
- 2021/12/16
4-METHOXY-1H-PYRAZOLO[3,4-D]PYRIMIDIN-6-AMINE Chemical Properties,Usage,Production
Synthesis
124-41-4
100644-65-3
100644-67-5
The general procedure for the synthesis of 4-methoxy-1H-pyrazolo[3,4-d]pyrimidin-6-amine from sodium methanol and 4-chloro-1H-pyrazolo[3,4-d]pyrimidin-6-amine was as follows: 4-chloro-1H-pyrazolo[3,4-d]pyrimidin-6-amine (800 mg, 4.73 mmol) was dissolved in 12.5 mL anhydrous methanol and purged with nitrogen to remove the oxygen. Subsequently, the solution was transferred to a methanol solution containing 2.3 M sodium methanol. After the reaction was refluxed at 65 °C for 2 h, 7.5 mL of acetic acid was slowly added and stirring was continued for 5 min. Upon completion of the reaction, the solvent was removed by rotary evaporation and dried under vacuum to give 745 mg of tan solid product in 95.4% yield.
References
[1] Patent: CN103804447, 2016, B. Location in patent: Paragraph 0076; 0086; 0087; 0088
[2] Helvetica Chimica Acta, 1986, vol. 69, # 7, p. 1602 - 1613
[3] Heterocycles, 1985, vol. 23, # 10, p. 2521 - 2524
4-METHOXY-1H-PYRAZOLO[3,4-D]PYRIMIDIN-6-AMINE Preparation Products And Raw materials
Raw materials
Preparation Products
4-METHOXY-1H-PYRAZOLO[3,4-D]PYRIMIDIN-6-AMINE Suppliers
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