4-AMINO-5-IODO-2-METHYLPYRIDINE

Product Name: 4-AMINO-5-IODO-2-METHYLPYRIDINE
CAS No.: 849353-19-1
Chemical Name: 4-AMINO-5-IODO-2-METHYLPYRIDINE
Synonyms: 5-Iodo-2-methyl-4-pyridinamine;5-iodo-2-Methylpyridin-4-aMine;4-AMINO-5-IODO-2-METHYLPYRIDINE;2-Methyl-4-amino-5-iodopyridine;5-Iodo-2-methylpyridin-4-ylamine;4-PyridinaMine, 5-iodo-2-Methyl-
CBNumber: CB22455277
Molecular Formula: C6H7IN2
Formula Weight: 234.04
MOL File: 849353-19-1.mol

More

Less

4-AMINO-5-IODO-2-METHYLPYRIDINE Property

storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
Appearance: White to off-white Solid
InChI: InChI=1S/C6H7IN2/c1-4-2-6(8)5(7)3-9-4/h2-3H,1H3,(H2,8,9)
InChIKey: UJDOLPPZRSZZAS-UHFFFAOYSA-N
SMILES: C1(C)=NC=C(I)C(N)=C1

More

Less

Hazard and Precautionary Statements (GHS)

More

Less

N-Bromosuccinimide Price

AK Scientific

Product number: X5596
Product name: 5-Iodo-2-methyl-4-pyridinamine
Packaging: 100mg
Price: $158
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0361217
Product name: 4-AMINO-5-IODO-2-METHYLPYRIDINE
Purity: 95.00%
Packaging: 5MG
Price: $500.12
Updated: 2021/12/16

Ambeed

Product number: A173674
Product name: 5-Iodo-2-methylpyridin-4-amine
Purity: 95+%
Packaging: 250mg
Price: $86
Updated: 2021/12/16

Ambeed

Product number: A173674
Product name: 5-Iodo-2-methylpyridin-4-amine
Purity: 95+%
Packaging: 1g
Price: $134
Updated: 2021/12/16

Chemenu

Product number: CM132492
Product name: 5-iodo-2-methylpyridin-4-amine
Purity: 95%
Packaging: 1g
Price: $297
Updated: 2021/12/16

More

Less

4-AMINO-5-IODO-2-METHYLPYRIDINE Chemical Properties,Usage,Production

Synthesis

18437-58-6

849353-19-1

General procedure for the synthesis of 5-iodo-2-methylpyridin-4-amine (i55) from 2-methylpyridin-4-amine: to a solution of 2-methylpyridin-4-amine (5 g, 46 mmol) in water (25 mL) was added sodium carbonate (Na2CO3, 3.4 g, 32 mmol) and the reaction mixture was heated to reflux. Subsequently, potassium iodide (KI, 9.8 g, 59 mmol) and iodine (I2, 9.3 g, 36 mmol, dissolved in 50 mL of water) were added and the reaction was continued at reflux for 7 hours. Upon completion of the reaction, the reaction was quenched with sodium thiosulfate solution followed by extraction of the target compound with dichloromethane (DCM). The organic layer was separated, dried with anhydrous sodium sulfate and concentrated under reduced pressure to remove the solvent. The resulting residue was purified by column chromatography on silica gel (100-200 mesh) using a hexane solution of 25% ethyl acetate as eluent to give the final target product 5-iodo-2-methylpyridin-4-amine (i55) (0.85 g, 8% yield). The product was characterized by 1H NMR (400 MHz, DMSO-d6): δ 2.20 (s, 3H), 6.00 (s, 2H), 6.49 (s, 1H), 8.22 (s, 1H). Mass spectrum (ESI) showed m/e(M + 1)+: 235.

References

[1] Patent: WO2016/124508, 2016, A1. Location in patent: Page/Page column 68; 69

4-AMINO-5-IODO-2-METHYLPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

4-AMINO-5-IODO-2-METHYLPYRIDINE Suppliers

China 22 Germany 1 India 1 United States 4 Global 28

Jiangsu Yaoheng Pharmaceutical Technology Co., Ltd.

Tel: 13524761129
Email: 2183470029@qq.com
Country: China
ProdList: 864
Advantage: 58

Wuhan ariel chemical Co., LTD.

Tel: 18986259541
Fax: 027-87840182
Email: sales@3stc.com
Country: China
ProdList: 3764
Advantage: 58

Hangzhou Sage Chemical Co., Ltd.

Tel: +86057186818502 13588463833
Fax: Pls mail us for more information!
Email: info@sagechem.com
Country: China
ProdList: 10266
Advantage: 58

Shanghai Devinchem Ltd

Tel: 027-65318838 13646286950
Email: sales@devinchem.com
Country: China
ProdList: 2953
Advantage: 58

Synchem OHG

Tel: +49 5662 408730
Fax: +49 5662 4087320
Email: info@synchem.de
Country: Germany
ProdList: 4705
Advantage: 70

Zhengzhou Alfachem Co., Ltd.

Tel: 0371-53765687 18937137882
Fax: QQ:2885373884
Email: 2853979813@qq.com
Country: China
ProdList: 7992
Advantage: 55

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Aikon International Limited

Tel: 025-66061636 18013972705
Fax: (3)02557626880
Email: qqyang@aikonchem.com
Country: China
ProdList: 15814
Advantage: 58

Shanghai Jizhi Biochemical Technology Co. Ltd.

Tel: 4009004166/18616739031 18616739031
Email: 3007523370@qq.com
Country: China
ProdList: 52687
Advantage: 58

Shanghai Kaiwei Chemical Technology Co., Ltd.

Tel: 021-58461859 15821823057
Email: service@aiviche.com
Country: China
ProdList: 49312
Advantage: 58

849353-19-1, 4-AMINO-5-IODO-2-METHYLPYRIDINERelated Search:

3-IODO-4-AMINO-2,6-DIMETHYLPYRIDINE 2-METHYL-5-IODOPYRIDINE 4-AMINO-5-IODO-2-METHYLPYRIDINE 3-Iodo-4-aminopyridine 4-Amino-5-iodo-2-phenylpyridine

4-AMINO-5-IODO-2-METHYLPYRIDINE

5-iodo-2-Methylpyridin-4-aMine

4-PyridinaMine, 5-iodo-2-Methyl-

5-Iodo-2-methyl-4-pyridinamine

5-Iodo-2-methylpyridin-4-ylamine

2-Methyl-4-amino-5-iodopyridine

849353-19-1