ChemicalBook > CAS DataBase List > 6-Chloro-N,N-dimethyl-3-pyridinecarboxamide
6-Chloro-N,N-dimethyl-3-pyridinecarboxamide
- Product Name
- 6-Chloro-N,N-dimethyl-3-pyridinecarboxamide
- CAS No.
- 54864-83-4
- Chemical Name
- 6-Chloro-N,N-dimethyl-3-pyridinecarboxamide
- Synonyms
- 2-Propyl-8-hydroxyquinoline;6-Chloro-N,N-dimethylnicotinamide;N,N-dimethyl-6-chloro-nicotinamide;6-Chloro-N,N-dimethyl-3-pyridinecarboxamide;3-Pyridinecarboxamide, 6-chloro-N,N-dimethyl-;6-chloro-N,N-dimethylnicotinamide(SALTDATA: FREE)
- CBNumber
- CB22462138
- Molecular Formula
- C8H9ClN2O
- Formula Weight
- 184.62
- MOL File
- 54864-83-4.mol
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6-Chloro-N,N-dimethyl-3-pyridinecarboxamide Property
- Boiling point:
- 330.9±27.0 °C(Predicted)
- Density
- 1.231
- storage temp.
- 2-8°C(protect from light)
- form
- solid
- pka
- -1.49±0.10(Predicted)
- Appearance
- Light brown to off-white Solid
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
Sigma-Aldrich
- Product number
- CBR00393
- Product name
- 6-Chloro-N,N-dimethylnicotinamide
- Purity
- Aldrich
- Packaging
- 1g
- Price
- $128
- Updated
- 2025/07/31
TRC
- Product number
- C368698
- Product name
- 6-Chloro-N,N-dimethylnicotinamide
- Packaging
- 1g
- Price
- $330
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FC150624
- Product name
- 6-Chloro-N,N-dimethylnicotinamide
- Packaging
- 50mg
- Price
- $66
- Updated
- 2021/12/16
AK Scientific
- Product number
- CS-W016976
- Product name
- 6-Chloro-N,N-dimethylnicotinamide
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FC150624
- Product name
- 6-Chloro-N,N-dimethylnicotinamide
- Packaging
- 100mg
- Price
- $114
- Updated
- 2021/12/16
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6-Chloro-N,N-dimethyl-3-pyridinecarboxamide Chemical Properties,Usage,Production
Synthesis
5326-23-8
124-40-3
54864-83-4
Scheme 32: Synthesis of 6-chloro-N,N-dimethylnicotinamide [198] 6-Chloronicotinic acid [197] (3.0 g, 19.0 mmol) was dissolved in tetrahydrofuran (THF, 100 ml) in an oven-dried 250 ml two-necked round-bottomed flask. The reaction system was degassed with nitrogen. To this clarified solution 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride (EDC.HCl, 4.02 g, 20.9 mmol) and N-methylmorpholine (NMM, 2.3 ml, 20.9 mmol) were added sequentially. The reaction mixture was stirred for 10 min at room temperature under nitrogen protection. Subsequently, dimethylamine solution (Me2NH, 13.06 ml, 2N, 25.5 mmol) was slowly added dropwise and the reaction was continued to be stirred for 16 h at room temperature. The progress of the reaction was monitored by thin layer chromatography (TLC). After completion of the reaction, the reaction mixture was quenched with water and extracted with ethyl acetate (3 x 100 ml). The organic phases were combined, washed with saturated saline and dried over anhydrous sodium sulfate. The organic layer was concentrated under reduced pressure to obtain the crude product, which was purified by column chromatography (silica gel 100-200 mesh, 2% methanol/dichloromethane) to afford the target compound [198] (2.62 g, 75%) as a white solid. Electrospray mass spectrometry (ESTMS): 185 (M++1).
References
[1] Patent: WO2014/16849, 2014, A2. Location in patent: Page/Page column 141
[2] Patent: EP1354882, 2003, A1. Location in patent: Page/Page column 70
6-Chloro-N,N-dimethyl-3-pyridinecarboxamide Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 6-Chloro-N,N-dimethyl-3-pyridinecarboxamide manufacturers
Career Henan Chemical Co
- Product
- 6-Chloro-N,N-dimethyl-3-pyridinecarboxamide 54864-83-4
- Price
- US $9.80/KG
- Min. Order
- 1g
- Purity
- ≥99%
- Supply Ability
- 100kg
- Release date
- 2020-01-11