HONGHUI-MED 480010000000

Product Name: HONGHUI-MED 480010000000
CAS No.: 118129-60-5
Chemical Name: HONGHUI-MED 480010000000
Synonyms: M8390;HONGHUI-MED 480010000000;1,7-Dibromo-3,4,9,10-Tetracarboxylic Acid Dianhydride;1,7-dibromoperylene-3,4,9,10-tetracarboxylicdianhydride;1,7-DibroMo-3,4,9,10-perylenetetracarboxylic dianhydride;1,7-Dibromo-3,4,9,10-perylenetetracarboxylic Dianhydride >1,7-dibromo-3,4:9,10-perylenetetracarboxylic acid dianhydride;Perylo[3,4-cd:9,10-c,d]dipyran-1,3,8,10-tetrone, 5,12-dibromo-;1,7-dibromoperylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride;5,12-Dibromoanthra[2,1,9-def:6,5,10-d'e'f']diisochromene-1,3,8,10-tetraone
CBNumber: CB22465230
Molecular Formula: C24H6Br2O6
Formula Weight: 550.11
MOL File: 118129-60-5.mol

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HONGHUI-MED 480010000000 Property

Melting point:: 360°C(lit.)
Boiling point:: 840.2±65.0 °C(Predicted)
Density: 2.159±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
form: powder
color: Orange to Brown to Dark red
λmax: 524nm(DMSO)(lit.)
InChI: InChI=1S/C24H6Br2O6/c25-13-5-12-16-10(22(28)32-24(12)30)4-2-8-18-14(26)6-11-15-9(21(27)31-23(11)29)3-1-7(19(15)18)17(13)20(8)16/h1-6H
InChIKey: WPBVUAVIGWNDGT-UHFFFAOYSA-N
SMILES: C1(=O)OC(=O)C2=CC(Br)=C3C4=C2C1=CC=C4C1=C2C4=C(C=C1Br)C(=O)OC(=O)C4=CC=C32

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Safety

WGK Germany: WGK 3
HS Code: 2932990090
Storage Class: 11 - Combustible Solids
Hazard Classifications: Eye Irrit. 2
Skin Irrit. 2
STOT SE 3

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 900186
Product name: 1,7-Dibromo-3,4,9,10-tetracarboxylic acid dianhydride
Packaging: 1g
Price: $233
Updated: 2023/06/20

TCI Chemical

Product number: D3871
Product name: 1,7-Dibromo-3,4,9,10-perylenetetracarboxylic Dianhydride
Purity: >98.0%(HPLC)
Packaging: 1g
Price: $464
Updated: 2026/03/19

TCI Chemical

Product number: D3871
Product name: 1,7-Dibromo-3,4,9,10-perylenetetracarboxylic Dianhydride
Purity: >98.0%(HPLC)
Packaging: 5g
Price: $1607
Updated: 2026/03/19

TRC

Product number: D423505
Product name: 5,12-Dibromoanthra[2,1,9-def:6,5,10-d''e''f'']diisochromene-1,3,8,10-tetraone
Packaging: 10mg
Price: $45
Updated: 2021/12/16

TRC

Product number: D423505
Product name: 5,12-Dibromoanthra[2,1,9-def:6,5,10-d''e''f'']diisochromene-1,3,8,10-tetraone
Packaging: 50mg
Price: $60
Updated: 2021/12/16

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HONGHUI-MED 480010000000 Chemical Properties,Usage,Production

Uses

Synthetic building block of high-mobility air-stable n-type semiconductors (electron-transport small organic molecules and polymers).

Synthesis

128-69-8

118129-60-5

Example 1: 292.5 g (0.75 mol) of 3,4,9,10-tetracarboxylic dianhydride of >98% purity was stirred with 4420 g of 100% by weight sulfuric acid for 12 hours at room temperature. Subsequently 7 g of iodine was added and the mixture was heated to 85°C. 262.5 g (1.64 mol) of bromine was added slowly and dropwise over 8 hours. Upon completion of the reaction, the mixture was cooled to room temperature and purged with nitrogen to remove excess bromine. Next, the sulfuric acid concentration was diluted to 86 wt% by adding a total of 670 g of water in batches over a period of 1 hour. During this process, the reaction mixture was again heated to 85°C. After cooling, the precipitated product was filtered through a G4 glass filter and washed with 3 kg of 86 wt% sulfuric acid. The product was stirred in 5 liters of water and then filtered again, washed to neutrality and dried under reduced pressure at 120°C. 370 g of 1,7-dibromo-3,4,9,10-perylenetetracarboxylic acid dianhydride in the form of a bright red fine crystalline powder was finally obtained, with a melting point >360 °C, a purity of >98% and a yield of 90%. Analytical data: Elemental analysis (calculated value/measured value, wt%): C: 52.4/52.1; H: 1.1/1.1; O: 17.45/17.4; Br: 29.1/29.4. IR (KBr): ν=1782+1770 (strong, C=O), 1735+1723 (strong, C=O) cm^-1; UV/VIS ( H2SO4): λmax (ε) = 408 (10309), 520 (29410), 554 (43141) nm.

References

[1] Angewandte Chemie - International Edition, 1998, vol. 37, # 10, p. 1434 - 1437
[2] Journal of Materials Chemistry, 2010, vol. 20, # 12, p. 2362 - 2368
[3] Asian Journal of Chemistry, 2010, vol. 22, # 9, p. 7135 - 7144
[4] Patent: US6063181, 2000, A
[5] Patent: US6143905, 2000, A

HONGHUI-MED 480010000000 Preparation Products And Raw materials

Raw materials

Preparation Products

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HONGHUI-MED 480010000000 Suppliers

Americas 1 China 109 Europe 1 India 2 Japan 1 United Kingdom 2 United States 6 Global 122

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View Lastest Price from HONGHUI-MED 480010000000 manufacturers

Career Henan Chemical Co

Product: 1,7-Dibromo-3,4,9,10-tetracarboxylic acid dianhydride 118129-60-5
Price: US $10000.00/KG
Min. Order: 10G
Purity: 99%
Supply Ability: 100KG
Release date: 2018-08-03

118129-60-5, HONGHUI-MED 480010000000Related Search:

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M8390

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118129-60-5