ChemicalBook > CAS DataBase List > 3-Pyridinecarboxylic acid, 5-hydroxy-6-iodo-, ethyl ester

3-Pyridinecarboxylic acid, 5-hydroxy-6-iodo-, ethyl ester

Product Name: 3-Pyridinecarboxylic acid, 5-hydroxy-6-iodo-, ethyl ester
CAS No.: 59288-40-3
Chemical Name: 3-Pyridinecarboxylic acid, 5-hydroxy-6-iodo-, ethyl ester
Synonyms: ethyl 5-hydroxy-6-iodonicotinate;5-Hydroxy-6-iodo-nicotinic acid ethyl ester;5-hydroxy-6-iodo-3-Pyridinecarboxylic acid ethyl ester;3-Pyridinecarboxylic acid, 5-hydroxy-6-iodo-, ethyl ester
CBNumber: CB22473673
Molecular Formula: C8H8INO3
Formula Weight: 293.06
MOL File: 59288-40-3.mol

Less

3-Pyridinecarboxylic acid, 5-hydroxy-6-iodo-, ethyl ester Property

storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
Appearance: White to off-white Solid

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P501Dispose of contents/container to..…

Less

N-Bromosuccinimide Price

AK Scientific

Product number: 8821AB
Product name: Ethyl5-hydroxy-6-iodonicotinate
Packaging: 250mg
Price: $273
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0368970
Product name: ETHYL-5-HYDROXY-6-IODONICOTINATE
Purity: 95.00%
Packaging: 5MG
Price: $498.67
Updated: 2021/12/16

Ambeed

Product number: A191659
Product name: Ethyl5-hydroxy-6-iodonicotinate
Purity: 98%
Packaging: 250mg
Price: $45
Updated: 2021/12/16

Ambeed

Product number: A191659
Product name: Ethyl5-hydroxy-6-iodonicotinate
Purity: 98%
Packaging: 1g
Price: $167
Updated: 2021/12/16

Alichem

Product number: 59288403
Product name: Ethyl5-hydroxy-6-iodonicotinate
Packaging: 250mg
Price: $189
Updated: 2021/12/16

Less

3-Pyridinecarboxylic acid, 5-hydroxy-6-iodo-, ethyl ester Chemical Properties,Usage,Production

Synthesis

59288-38-9

59288-40-3

General procedure for the synthesis of ethyl 5-hydroxy-6-iodo-3-pyridinecarboxylate from ethyl 5-hydroxynicotinate: a solution of ethyl 5-hydroxynicotinate was added to water (15 L), followed by sodium carbonate (733 g, 30.7 mol) and iodine (965 g, 15.3 mol). The reaction was carried out at room temperature with stirring for 2 hours. The progress of the reaction was monitored by thin layer chromatography (TLC) (unfolding agent: petroleum ether/ethyl acetate = 1/1, Rf = 0.8) and after confirming the completion of the reaction, the pH was adjusted to 7 by slowly adding 1N hydrochloric acid to the reaction solution, when a solid precipitated. The solid product was collected by filtration and dried under reduced pressure to give ethyl 5-hydroxy-6-iodo-3-pyridinecarboxylate (925 g) as a yellow solid in 82.5% yield.

References

[1] Patent: CN105418620, 2016, A. Location in patent: Paragraph 0008; 0032; 0033

3-Pyridinecarboxylic acid, 5-hydroxy-6-iodo-, ethyl ester Preparation Products And Raw materials

Raw materials

Preparation Products

Less

3-Pyridinecarboxylic acid, 5-hydroxy-6-iodo-, ethyl ester Suppliers

China 35 India 1 United States 2 Global 38

Capot Chemical Co., Ltd

Tel: +86 (0) 571 85 58 67 18
Fax: 0086-571-85864795
Country: China
ProdList: 18207
Advantage: 66

Chiba Pharmaceutical Science and technology Co, Ltd.

Tel: 0531-81313138 13066006660
Fax: QQ: 3366077777
Email: chibapharm@foxmail.com
Country: China
ProdList: 3991
Advantage: 55

SynAsst Chemical.

Tel: 021-60343070
Fax: 021-35122006
Country: China
ProdList: 12740
Advantage: 55

Shanghai CP Pharmaceutical Technology Co., Ltd.

Tel: 18221530285
Fax: -
Country: China
ProdList: 489
Advantage: 55

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Yantai ShengKailun Chemical Technology Co., Ltd.

Tel: 13356901049
Fax: QQ：1025383091
Email: 3119594100@qq.com
Country: China
ProdList: 7964
Advantage: 55

Nanijing m&m biotechnology Co. ,Ltd.

Tel: 025-87782433 18021532344
Fax: 025-87782433
Email: 1345332203@qq.com
Country: China
ProdList: 4134
Advantage: 58

Biokitchen

Tel: 021-021-021-31663258 13795219287
Fax: 021-31663258
Email: donghuanwen@126.com
Country: China
ProdList: 8816
Advantage: 58

Cochemical Ltd.

Tel: 029-86115547 17791676824
Fax: 021-51602123
Email: sales@cochemical.com
Country: China
ProdList: 4006
Advantage: 58

Capot Chemical Co.,Ltd.

Tel: +86-（0）57185586718; +8613336195806
Fax: +86-571-85864795
Email: sales@capot.com
Country: China
ProdList: 29735
Advantage: 60

Aikon International Limited

Tel: 025-66061636 18013972705
Fax: (3)02557626880
Email: qqyang@aikonchem.com
Country: China
ProdList: 15814
Advantage: 58

Shanghai Jizhi Biochemical Technology Co. Ltd.

Tel: 4009004166/18616739031 18616739031
Email: 3007523370@qq.com
Country: China
ProdList: 52687
Advantage: 58

Shanghai Sealing Biotechnology Co. Ltd..

Tel: 15721176654
Email: 1815535157@qq.com
Country: China
ProdList: 881
Advantage: 58

Labnetwork lnc.

Tel: +86-27-50766799 +8618062016861
Email: contact@labnetwork.com
Country: China
ProdList: 19987
Advantage: 58

Wuxi Kehua Biological Technology Co., Ltd.

Tel: 0510-86838766 13636419861
Email: 2258830676@qq.com
Country: China
ProdList: 5044
Advantage: 58

Block Chemical Technology (Shanghai) Co., LTD

Tel: 021-20432219 13918097649
Fax: QQ79021576
Email: li_jinfei@acblock-lab.com
Country: China
ProdList: 9673
Advantage: 58

Shanghai Kaiwei Chemical Technology Co., Ltd.

Tel: 021-58461859 15821823057
Email: service@aiviche.com
Country: China
ProdList: 49312
Advantage: 58

Neostar United (Changzhou) Industrial Co., Ltd.

Tel: +86-0519-85551759 +8613506123987
Fax: +0086-519-85557389
Email: marketing1@neostarunited.com
Country: China
ProdList: 8830
Advantage: 58

Shanghai Haohong Pharmaceutical Co., Ltd.

Tel: 400-8210725 4008210725
Email: malulu@leyan.com
Country: China
ProdList: 40000
Advantage: 58

Beijing Stronger Science Co., Ltd.

Tel: 0531-88924771 15614660963
Email: elsa.hang@strongerscience.com
Country: China
ProdList: 10623
Advantage: 58

Shaanxi Yudingzhuo Medical Technology Co., Ltd.

Tel: 18992018580 18165105898
Fax: QQ:1617857088
Email: 13608210612@163.com
Country: China
ProdList: 2984
Advantage: 58

Bide Pharmatech Ltd.

Tel: 400-6005915
Email: sales@picasso-e.com
Country: China
ProdList: 39653
Advantage: 58

Meryer (Shanghai) Chemical Technology Co., Ltd.

Tel: 18621169109
Email: market03@meryer.com
Country: China
ProdList: 27987
Advantage: 58

Yantai Sheng Kai Lun Biological Products Co. , Ltd.

Tel: 13356901049
Email: mark@sklnchem.cn
Country: China
ProdList: 7998
Advantage: 58

Beijing Solarbio Science & Tecnology Co., Ltd.

Tel: 010-50973130 17801761073
Email: Gsiyu@solarbio.com
Country: China
ProdList: 50464
Advantage: 58

Zhuhai Aobokai Biomedical Technology Co., Ltd.

Tel: 400-0628126 15697567703
Email: sales-team@aobchem.com.cn
Country: China
ProdList: 49999
Advantage: 58

Accela ChemBio Co.,Ltd.

Tel: 021-50795510 4000665055
Email: syeu@accelachem.com
Country: China
ProdList: 11015
Advantage: 58

Baoji Didu Pharmaceutical and Chemical Co., Ltd

Tel: 029-81145305 17791533577
Email: 1021@dideu.com
Country: China
ProdList: 10009
Advantage: 58

Shanghai potentpharm CO.,Ltd

Tel: 13524892556
Email: 263541193@qq.com
Country: China
ProdList: 189
Advantage: 58

Shanghai Scibiotron Pharmaceutical Co., Ltd

Tel: +86-16621589600
Email: contact@scibiotron.com
Country: China
ProdList: 5535
Advantage: 58

Cochemical Co. Ltd.

Tel: +86-029-86115547 +86-17791676824
Email: sales@cochemical.com
Country: China
ProdList: 3952
Advantage: 58

Zhengzhou Lingzhiyue Technology Co., Ltd

Tel: +86-0371-55074660 +8613523716970
Email: Lingzhiyue@aliyun.com
Country: China
ProdList: 3145
Advantage: 58

Lianyungang Kelian Chemical Co., Ltd.

Tel: --
Fax: --
Email: sales@klinechem.com
Country: CHINA
ProdList: 507
Advantage: 58

Shanghai Hao Zhun Biological Technology Co., Ltd.

Tel: --
Fax: --
Email: info@zzsrm.com
Country: CHINA
ProdList: 6650
Advantage: 58

Debye Scientific Corporation

Tel: --
Fax: --
Country: China
ProdList: 6891
Advantage: 50

59288-40-3, 3-Pyridinecarboxylic acid, 5-hydroxy-6-iodo-, ethyl esterRelated Search:

3-Pyridinecarboxylic acid, 5-hydroxy-6-iodo-, ethyl ester

ethyl 5-hydroxy-6-iodonicotinate

5-hydroxy-6-iodo-3-Pyridinecarboxylic acid ethyl ester

5-Hydroxy-6-iodo-nicotinic acid ethyl ester

59288-40-3