ChemicalBook > CAS DataBase List > 3-Bromo-7,12-diphenylbenzo[k]fluoranthene

3-Bromo-7,12-diphenylbenzo[k]fluoranthene

Product Name: 3-Bromo-7,12-diphenylbenzo[k]fluoranthene
CAS No.: 187086-32-4
Chemical Name: 3-Bromo-7,12-diphenylbenzo[k]fluoranthene
Synonyms: 3-Bromo-7,12-diphenylbenzo[k]fluoranthene;3-Bromo-7,12-diphenylbenzo[k]fluoranthrene;Benzo[k]fluoranthene, 3-bromo-7,12-diphenyl
CBNumber: CB22485049
Molecular Formula: C32H19Br
Formula Weight: 483.4
MOL File: 187086-32-4.mol

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3-Bromo-7,12-diphenylbenzo[k]fluoranthene Property

Boiling point:: 649.4±24.0 °C(Predicted)
Density: 1.409
storage temp.: Sealed in dry,Room Temperature
form: solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: HCH0364643
Product name: 3-BROMO-7,12-DIPHENYLBENZO[K]FLUORANTHENE
Purity: 95.00%
Packaging: 5MG
Price: $503.83
Updated: 2021/12/16

Arctom

Product number: AS023013
Product name: 3-Bromo-7,12-diphenylbenzo[k]fluoranthene
Purity: 97%
Packaging: 1g
Price: $97
Updated: 2021/12/16

Crysdot

Product number: CD43000604
Product name: 3-Bromo-7,12-diphenylbenzo[k]fluoranthene
Purity: 97%
Packaging: 1g
Price: $99
Updated: 2021/12/16

Crysdot

Product number: CD43000604
Product name: 3-Bromo-7,12-diphenylbenzo[k]fluoranthene
Purity: 97%
Packaging: 5g
Price: $297
Updated: 2021/12/16

Arctom

Product number: AS023013
Product name: 3-Bromo-7,12-diphenylbenzo[k]fluoranthene
Purity: 97%
Packaging: 5g
Price: $322
Updated: 2021/12/16

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3-Bromo-7,12-diphenylbenzo[k]fluoranthene Chemical Properties,Usage,Production

Synthesis

16391-62-1

187086-32-4

Example 1. Synthesis of 3-bromo-7,12-diphenylbenzo[k]fluoranthene To a solvent mixture of 50 mL of N-methylpyrrolidone (NMP) and 500 mL of dichloromethane were added 10.0 g (25 mmol) of 7,12-diphenylbenzo[k]fluoranthene (see WO2010/031833 for preparation) and 6.45 g (36 mmol) of N-bromosuccinimide (NBS). The reaction mixture was stirred at room temperature for 20 hours. Upon completion of the reaction, the dichloromethane was evaporated under reduced pressure and the product was subsequently precipitated by addition of water. The precipitate was collected by filtration and dried to give 12.1 g (quantitative yield) of the title compound as a beige solid. Thin layer chromatography (TLC) analysis showed an Rf value of 0.9 (unfolding agent ratio petroleum ether:toluene = 2:1).

References

[1] Patent: WO2012/123888, 2012, A1. Location in patent: Page/Page column 60-61
[2] Patent: US2016/284947, 2016, A1. Location in patent: Paragraph 0296; 0297; 0298
[3] Patent: CN107778199, 2018, A. Location in patent: Paragraph 0060; 0066; 0072
[4] Patent: EP2907803, 2015, A1. Location in patent: Page/Page column 137
[5] Patent: TWI558705, 2016, B. Location in patent: Paragraph 0140; 0147

3-Bromo-7,12-diphenylbenzo[k]fluoranthene Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-Bromo-7,12-diphenylbenzo[k]fluoranthene manufacturers

Career Henan Chemical Co

Product: 3-Bromo-7,12-diphenylbenzo[k]fluoranthene 187086-32-4
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2019-07-05

187086-32-4, 3-Bromo-7,12-diphenylbenzo[k]fluorantheneRelated Search:

3-Bromo-7,12-diphenylbenzo[k]fluoranthene

Benzo[k]fluoranthene, 3-bromo-7,12-diphenyl

3-Bromo-7,12-diphenylbenzo[k]fluoranthrene

187086-32-4

C32H19Br