Octahydro-pyrrolo[3,2-c]pyridine-1-carboxylic acid tert-butyl ester
- Product Name
- Octahydro-pyrrolo[3,2-c]pyridine-1-carboxylic acid tert-butyl ester
- CAS No.
- 1147422-00-1
- Chemical Name
- Octahydro-pyrrolo[3,2-c]pyridine-1-carboxylic acid tert-butyl ester
- Synonyms
- 1-Boc-1H-octahydropyrrolo[3,2-c]pyridine;Octahydro-pyrrolo[3,2-c]pyridine-1-carboxylic acid tert-butyl ester;tert-butyl 2,3,3a,4,5,6,7,7a-octahydropyrrolo[3,2-c]pyridine-1-carboxylate;1H-Pyrrolo[3,2-c]pyridine-1-carboxylic acid, octahydro-, 1,1-diMethylethyl ester;tert-butyl octahydro-1H-pyrrolo[3,2-c]pyridine-1-carboxylate, Mixture of diastereomers
- CBNumber
- CB22491675
- Molecular Formula
- C12H22N2O2
- Formula Weight
- 226.32
- MOL File
- 1147422-00-1.mol
Octahydro-pyrrolo[3,2-c]pyridine-1-carboxylic acid tert-butyl ester Property
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- Appearance
- White to yellow Solid-Liquid Mixture
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
N-Bromosuccinimide Price
- Product number
- B7881
- Product name
- 1-Boc-octahydropyrrolo[3,2-c]pyridine
- Purity
- 97.0%
- Packaging
- 500mg
- Price
- $95
- Updated
- 2026/05/06
- Product number
- B7881
- Product name
- 1-Boc-octahydropyrrolo[3,2-c]pyridine
- Purity
- 97.0%
- Packaging
- 1g
- Price
- $250
- Updated
- 2026/05/06
- Product number
- B7881
- Product name
- 1-Boc-octahydropyrrolo[3,2-c]pyridine
- Purity
- 97.0%
- Packaging
- 5g
- Price
- $1160
- Updated
- 2026/05/06
- Product number
- L21842
- Product name
- tert-Butyl octahydro-1H-pyrrolo[3,2-c]pyridine-1-carboxylate
- Purity
- 97%
- Packaging
- 1G
- Price
- $180
- Updated
- 2026/05/27
- Product number
- L21842
- Product name
- tert-Butyl octahydro-1H-pyrrolo[3,2-c]pyridine-1-carboxylate
- Purity
- 97%
- Packaging
- 5G
- Price
- $910
- Updated
- 2026/05/27
Octahydro-pyrrolo[3,2-c]pyridine-1-carboxylic acid tert-butyl ester Chemical Properties,Usage,Production
Synthesis
148760-75-2
1147422-00-1
The general procedure for the synthesis of 1-Boc-1H-octahydropyrrolo[3,2-c]pyridine from 1-Boc-1H-pyrrolo[3,2-c]pyridine was as follows: 1H-pyrrolo[3,2-c]pyridine-1-carboxylic acid tert-butyl ester (2.55 g) was dissolved in a mixed solvent of ethylene glycol monomethyl ether (40 mL) and acetic acid (1 mL), and catalytic amounts of palladium hydroxide/ carbon (Pd(OH)2/C). The reaction suspension was heated at 70 °C for 24 h under hydrogen (2.0 MPa) atmosphere. Upon completion of the reaction, the catalyst was removed by filtration and the filtrate was concentrated under vacuum to remove the solvent. The resulting residue was purified by silica gel column chromatography with the eluent being a solvent mixture of dichloromethane and methanol (10:1, v/v) to afford the final target product 1-Boc-1H-octahydropyrrolo[3,2-c]pyridine as a viscous liquid (2.64 g, 100.00% yield).
References
[1] Patent: WO2013/71697, 2013, A1. Location in patent: Paragraph 00276
[2] Patent: US2014/228361, 2014, A1. Location in patent: Paragraph 0418-0419
Octahydro-pyrrolo[3,2-c]pyridine-1-carboxylic acid tert-butyl ester Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Octahydro-pyrrolo[3,2-c]pyridine-1-carboxylic acid tert-butyl ester manufacturers
- Product
- Octahydro-pyrrolo[3,2-c]pyridine-1-carboxylic acid tert-butyl ester 1147422-00-1
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 97%
- Supply Ability
- 1000kg
- Release date
- 2026-03-11
- Product
- Octahydro-pyrrolo[3,2-c]pyridine-1-carboxylic acid tert-butyl ester 1147422-00-1
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2020-01-09