1-Phenyl-1H-imidazole-4-carboxylic acid
- Product Name
- 1-Phenyl-1H-imidazole-4-carboxylic acid
- CAS No.
- 18075-64-4
- Chemical Name
- 1-Phenyl-1H-imidazole-4-carboxylic acid
- Synonyms
- 1-Phenyl-1H-imidazole-4-carboxylic acid;1H-Imidazole-4-carboxylic acid, 1-phenyl-;1-Phenyl-1H-imidazole-4-carboxylic acid 97%
- CBNumber
- CB22500443
- Molecular Formula
- C10H8N2O2
- Formula Weight
- 188.18
- MOL File
- 18075-64-4.mol
1-Phenyl-1H-imidazole-4-carboxylic acid Property
- Boiling point:
- 424.5±18.0 °C(Predicted)
- Density
- 1.28±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 1.48±0.10(Predicted)
- Appearance
- White to off-white Solid
Safety
- HS Code
- 2933299090
N-Bromosuccinimide Price
- Product number
- P335275
- Product name
- 1-Phenyl-1H-imidazole-4-carboxylicAcid
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- P335275
- Product name
- 1-Phenyl-1H-imidazole-4-carboxylicAcid
- Packaging
- 500mg
- Price
- $200
- Updated
- 2021/12/16
- Product number
- W3926
- Product name
- 1-Phenyl-1H-imidazole-4-carboxylicacid
- Packaging
- 1g
- Price
- $204
- Updated
- 2021/12/16
- Product number
- 073779
- Product name
- 1-Phenyl-1H-imidazole-4-carboxylic acid
- Purity
- 95+%
- Packaging
- 500mg
- Price
- $150
- Updated
- 2021/12/16
- Product number
- 4H58-1-FC
- Product name
- 1-Phenyl-1H-imidazole-4-carboxylic acid
- Packaging
- 1g
- Price
- $176
- Updated
- 2021/12/16
1-Phenyl-1H-imidazole-4-carboxylic acid Chemical Properties,Usage,Production
Synthesis
116343-89-6
18075-64-4
General procedure for the synthesis of 1-phenyl-1H-imidazole-4-carboxylic acid from methyl 1-phenyl-1H-imidazole-4-carboxylate: LiOH-H2O (143 mg, 3.4 mmol) was added to a stirred methyl 1-phenyl-1H-imidazole-4-carboxylic acid (231 mg, 1.1 mmol) solution in a mixture of THF (3 mL), MeOH (1 mL), and H2O ( 1 mL) in mixed solvents and continued stirring for 3 hours at room temperature. After completion of the reaction, the reaction mixture was concentrated under reduced pressure. Subsequently, cold water was added and acidified with 10% aqueous HCl and the precipitated solid was collected to give 180 mg (83.7% yield) of 1-phenyl-1H-imidazole-4-carboxylic acid.
References
[1] Patent: US2009/239810, 2009, A1. Location in patent: Page/Page column 81
[2] Patent: US2010/160323, 2010, A1. Location in patent: Page/Page column 24
[3] Patent: WO2017/103614, 2017, A1. Location in patent: Page/Page column 67
1-Phenyl-1H-imidazole-4-carboxylic acid Preparation Products And Raw materials
Raw materials
Preparation Products
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