3-(Boc-amino)-2-piperidone

Product Name: 3-(Boc-amino)-2-piperidone
CAS No.: 99780-98-0
Chemical Name: 3-(Boc-amino)-2-piperidone
Synonyms: 3-Boc-aMino-2-piperidinone;3-(Boc-amino)-2-piperidone;_x000D_3-(Boc-amino)-2-piperidone;tert-Butyl (2-oxopiperidin-3-yl)carbaMate;tert-butyl N-(2-oxopiperidin-3-yl)carbamate;(+/-)-3-<(tert-butoxycarbonyl)amino>-2-piperidone;1,1-Dimethylethyl?N-(2-oxo-3-piperidinyl)carbamate;Carbamic acid, N-(2-oxo-3-piperidinyl)-, 1,1-dimethylethyl ester
CBNumber: CB22500771
Molecular Formula: C10H18N2O3
Formula Weight: 214.26
MOL File: 99780-98-0.mol

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3-(Boc-amino)-2-piperidone Property

Boiling point:: 405.6±34.0 °C(Predicted)
Density: 1.11±0.1 g/cm3(Predicted)
storage temp.: 2-8°C
pka: 11.05±0.20(Predicted)
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: B621138
Product name: 3-(Boc-amino)-2-piperidone
Packaging: 500mg
Price: $90
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0299986
Product name: 3-(BOC-AMINO)-2-PIPERIDONE
Purity: 95.00%
Packaging: 5MG
Price: $496.39
Updated: 2021/12/16

AK Scientific

Product number: 7000AC
Product name: tert-Butyl(2-oxopiperidin-3-yl)carbamate
Packaging: 1g
Price: $144
Updated: 2021/12/16

Crysdot

Product number: CD11000199
Product name: tert-Butyl(2-oxopiperidin-3-yl)carbamate
Purity: 95+%
Packaging: 5g
Price: $211
Updated: 2021/12/16

Chemenu

Product number: CM179771
Product name: tert-Butyl(2-oxopiperidin-3-yl)carbamate
Purity: 95%
Packaging: 5g
Price: $224
Updated: 2021/12/16

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3-(Boc-amino)-2-piperidone Chemical Properties,Usage,Production

Synthesis

1892-22-4

24424-99-5

99780-98-0

General procedure for the synthesis of 3-(Boc-amino)-2-piperidinone from 3-aminopiperidin-2-one and di-tert-butyl dicarbonate: To a 500 mL round-bottomed flask were added 3-aminopiperidin-2-one (10 g, 87.61 mmol, 1.00 equiv), methanol (200 g, 6.24 mol, 71.25 equiv), and triethylamine (20 mL). A solution of di-tert-butyl dicarbonate (20 g, 91.64 mmol, 1.05 equiv) in methanol (100 mL) was added slowly and dropwise with stirring at 0 °C. The reaction mixture was stirred at room temperature overnight. After completion of the reaction, the mixture was concentrated under vacuum. The crude product was purified by column chromatography to afford 16 g (85% yield) of 3-(Boc-amino)-2-piperidone as a white solid.

References

[1] Patent: WO2017/75056, 2017, A1. Location in patent: Paragraph 0410
[2] Journal of Medicinal Chemistry, 1986, vol. 29, # 2, p. 251 - 260
[3] Farmaco, 2004, vol. 59, # 4, p. 271 - 277
[4] Patent: WO2004/98589, 2004, A1. Location in patent: Page 163

3-(Boc-amino)-2-piperidone Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-(Boc-amino)-2-piperidone manufacturers

Career Henan Chemical Co

Product: 3-(Boc-amino)-2-piperidone 99780-98-0
Price: US $0.01/KG
Min. Order: 1KG
Purity: 98%; 99%
Supply Ability: 1kg; 10kg; 25kg
Release date: 2020-01-07

99780-98-0, 3-(Boc-amino)-2-piperidoneRelated Search:

3-(Boc-amino)-2-piperidone

tert-Butyl (2-oxopiperidin-3-yl)carbaMate

3-Boc-aMino-2-piperidinone

(+/-)-3-<(tert-butoxycarbonyl)amino>-2-piperidone

tert-butyl N-(2-oxopiperidin-3-yl)carbamate

Carbamic acid, N-(2-oxo-3-piperidinyl)-, 1,1-dimethylethyl ester

_x000D_3-(Boc-amino)-2-piperidone

1,1-Dimethylethyl?N-(2-oxo-3-piperidinyl)carbamate

99780-98-0