ChemicalBook > CAS DataBase List > 5-Bromo-6-chloro-1H-indole

5-Bromo-6-chloro-1H-indole

Product Name
5-Bromo-6-chloro-1H-indole
CAS No.
122531-09-3
Chemical Name
5-Bromo-6-chloro-1H-indole
Synonyms
5-bromo-6-chloro-indole;5-bromo-6-chloro-1H-indole;1H-Indole, 5-broMo-6-chloro-;5-bromo-6-chloro-1H-indole(5-?Bromo-?6-?Chloroindole)
CBNumber
CB22504739
Molecular Formula
C8H5BrClN
Formula Weight
230.49
MOL File
122531-09-3.mol
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5-Bromo-6-chloro-1H-indole Property

Boiling point:
358℃
Density 
1.772
Flash point:
170℃
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
pka
15.14±0.30(Predicted)
Appearance
White to off-white Solid
InChI
InChI=1S/C8H5BrClN/c9-6-3-5-1-2-11-8(5)4-7(6)10/h1-4,11H
InChIKey
SMZUROGBNBCCPT-UHFFFAOYSA-N
SMILES
N1C2=C(C=C(Br)C(Cl)=C2)C=C1
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B682438
Product name
5-Bromo-6-chloro-1H-indole
Packaging
0.25g
Price
$55
Updated
2021/12/16
AK Scientific
Product number
J96365
Product name
5-Bromo-6-chloro-1H-indole
Packaging
100mg
Price
$10
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB29903
Product name
5-Bromo-6-chloro-1H-indole
Packaging
2g
Price
$100
Updated
2021/12/16
Matrix Scientific
Product number
091920
Product name
5-Bromo-6-chloro-1H-indole
Purity
95+%
Packaging
250mg
Price
$198
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB29903
Product name
5-Bromo-6-chloro-1H-indole
Packaging
5G
Price
$200
Updated
2021/12/16
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5-Bromo-6-chloro-1H-indole Chemical Properties,Usage,Production

Uses

5-Bromo-6-chloro-1H-indole was used in the study to prepare indole derivatives as intermediates for agrochemicals and drugs.

Synthesis

29682-39-1

1826-67-1

122531-09-3

Under nitrogen protection, 1-bromo-2-chloro-4-nitrobenzene (57.4 g, 0.243 mol) was dissolved in tetrahydrofuran (THF, 500 mL) and cooled to -40°C. At this temperature, vinylmagnesium bromide (1 M solution of THF, 728 mL, 0.728 mol) was added slowly and dropwise. After the dropwise addition was completed, the reaction mixture was kept stirred at -40°C for 1 hr. Subsequently, the reaction was quenched by addition of aqueous ammonium chloride (NH4Cl) and gradually warmed to room temperature. The reaction mixture was extracted with ethyl acetate, the organic layers were combined, dried over anhydrous magnesium sulfate (MgSO4), filtered and concentrated. The crude product was purified by column chromatography (using 5-bromo-6-chloro-1H-indole as reference) to afford the target product 5-bromo-6-chloro-1H-indole (8.40 g, 15% yield).

References

[1] Patent: KR101601357, 2016, B1. Location in patent: Paragraph 0285-0287

5-Bromo-6-chloro-1H-indole Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-Bromo-6-chloro-1H-indole manufacturers

Henan Aochuang Chemical Co.,Ltd.
Product
5-bromo-6-chloro-indole 122531-09-3
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1Ton
Release date
2022-10-13
Career Henan Chemical Co
Product
5-bromo-6-chloro-indole 122531-09-3
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
KG/T
Release date
2019-12-18

122531-09-3, 5-Bromo-6-chloro-1H-indoleRelated Search:


  • 5-bromo-6-chloro-indole
  • 1H-Indole, 5-broMo-6-chloro-
  • 5-bromo-6-chloro-1H-indole
  • 5-bromo-6-chloro-1H-indole(5-?Bromo-?6-?Chloroindole)
  • 122531-09-3