Methyl 2-bromo-4-(trifluoromethyl)benzoate

Product Name: Methyl 2-bromo-4-(trifluoromethyl)benzoate
CAS No.: 1214334-90-3
Chemical Name: Methyl 2-bromo-4-(trifluoromethyl)benzoate
Synonyms: Methyl 2-bromo-4-(trifluoromethyl);2-bromo-4- (trifluoromethyl) benzoate;2-broMo-4-trifluoroMethylMethyl benzoate;Methyl 2-bromo-4-(trifluoromethyl)benzoate;2-Bromo-4-(trifluoromethyl)benzoic acid methyl ester;Benzoic acid, 2-bromo-4-(trifluoromethyl)-, methyl ester
CBNumber: CB22516574
Molecular Formula: C9H6BrF3O2
Formula Weight: 283.04
MOL File: 1214334-90-3.mol

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Methyl 2-bromo-4-(trifluoromethyl)benzoate Property

Boiling point:: 248.9±40.0 °C(Predicted)
Density: 1.598±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
form: liquid
color: Colourless to light yellow

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Safety

HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TRC

Product number: M296350
Product name: Methyl2-bromo-4-(trifluoromethyl)benzoate
Packaging: 100mg
Price: $45
Updated: 2021/12/16

TRC

Product number: M296350
Product name: Methyl2-bromo-4-(trifluoromethyl)benzoate
Packaging: 500mg
Price: $65
Updated: 2021/12/16

Apolloscientific

Product number: PC53418
Product name: Methyl2-bromo-4-(trifluoromethyl)benzoate
Packaging: 1g
Price: $38
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2823-B-10
Product name: Methyl 2-bromo-4-(trifluoromethyl)benzoate
Packaging: 1g
Price: $42
Updated: 2021/12/16

AK Scientific

Product number: J96831
Product name: 2-Bromo-4-(trifluoromethyl)benzoicacidmethylester
Packaging: 5g
Price: $160
Updated: 2021/12/16

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Methyl 2-bromo-4-(trifluoromethyl)benzoate Chemical Properties,Usage,Production

Synthesis

328-89-2

74-88-4

1214334-90-3

At room temperature and under nitrogen protection, 2 g (7.434 mmol) of 2-bromo-4-trifluoromethylbenzoic acid (CAS: 328-89-2) was dissolved in 20 ml of DMF. Subsequently, 1.13 g (8.177 mmol) of potassium carbonate and 557 μL (8.921 mmol) of iodomethane were sequentially added to this solution. The reaction mixture was stirred overnight under nitrogen atmosphere. After completion of the reaction, the mixture was poured into 300 ml of water and the aqueous layer was extracted with ethyl acetate (2 x 80 ml). The organic phases were combined, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography (eluent: heptane/ethyl acetate, gradient 0 to 10%) to give 1.75 g (83% yield) of methyl 2-bromo-4-trifluoromethylbenzoate as an orange oil.

References

[1] Synthesis (Germany), 2012, vol. 44, # 14, p. 2173 - 2180
[2] Patent: US2010/197715, 2010, A1. Location in patent: Page/Page column 28
[3] Patent: US2011/53904, 2011, A1. Location in patent: Page/Page column 15
[4] Patent: WO2011/23667, 2011, A1. Location in patent: Page/Page column 26
[5] Patent: US2011/190349, 2011, A1. Location in patent: Page/Page column 10

Methyl 2-bromo-4-(trifluoromethyl)benzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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Methyl 2-bromo-4-(trifluoromethyl)benzoate Suppliers

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View Lastest Price from Methyl 2-bromo-4-(trifluoromethyl)benzoate manufacturers

Career Henan Chemica Co

Product: Methyl 2-bromo-4-(trifluoromethyl)benzoate 1214334-90-3
Price: US $1.80/KG
Min. Order: 1g
Purity: 96%-99%
Supply Ability: 1kg/10kg/100kg
Release date: 2020-11-07

1214334-90-3, Methyl 2-bromo-4-(trifluoromethyl)benzoateRelated Search:

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2-bromo-4- (trifluoromethyl) benzoate

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2-broMo-4-trifluoroMethylMethyl benzoate

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1214334-90-3