METHYL 3,4,5-TRIFLUOROBENZENECARBOXYLATE

Product Name: METHYL 3,4,5-TRIFLUOROBENZENECARBOXYLATE
CAS No.: 773873-72-6
Chemical Name: METHYL 3,4,5-TRIFLUOROBENZENECARBOXYLATE
Synonyms: Methyl 3;5-trifluorobenzoate;RARECHEM AL BF 0343;3,4,5-fluorobenzoate;Methyl 3,4,5-trifluorobenzoate;3,4,5-trifluoroMethyl benzoate;Methyl3,4,5-trifluorobenzoate99%;3,4,5-Trifluorobenzoic acid methyl ester;METHYL 3,4,5-TRIFLUOROBENZENECARBOXYLATE;Benzoic acid, 3,4,5-trifluoro-, methyl ester
CBNumber: CB2252137
Molecular Formula: C8H5F3O2
Formula Weight: 190.12
MOL File: Mol file

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METHYL 3,4,5-TRIFLUOROBENZENECARBOXYLATE Property

Boiling point:: 211.1±40.0 °C(Predicted)
Density: 1.358±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
form: liquid
color: Clear, colourless

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Safety

Hazard Codes: Xi
HazardClass: IRRITANT
HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC

Product number: M332058
Product name: Methyl3,4,5-trifluorobenzenecarboxylate
Packaging: 250mg
Price: $55
Updated: 2021/12/16

TRC

Product number: M332058
Product name: Methyl3,4,5-trifluorobenzenecarboxylate
Packaging: 1g
Price: $75
Updated: 2021/12/16

Usbiological

Product number: 455049
Product name: Methyl 3-
Packaging: 100mg
Price: $305
Updated: 2021/12/16

Usbiological

Product number: 455061
Product name: Methyl 3-
Packaging: 1g
Price: $305
Updated: 2021/12/16

Usbiological

Product number: 455069
Product name: Methyl 3-
Packaging: 100mg
Price: $305
Updated: 2021/12/16

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METHYL 3,4,5-TRIFLUOROBENZENECARBOXYLATE Chemical Properties,Usage,Production

Synthesis

67-56-1

121602-93-5

773873-72-6

Thionyl chloride (0.61 mL) was slowly added to methanol (20 mL) and the reaction mixture was stirred for 5 minutes under ice bath cooling. Subsequently, 3,4,5-trifluorobenzoic acid (1.00 g) was added in batches under the same cooling conditions, and the temperature was gradually raised to 60 °C after the addition was completed. The reaction was kept at this temperature with continuous stirring for 5 hours. Upon completion of the reaction, the mixture was cooled to room temperature and subsequently concentrated under reduced pressure to remove the solvent. The resulting residue was purified by silica gel column chromatography (eluent: ethyl acetate/hexane mixed solvent) to afford the target product methyl 3,4,5-trifluorobenzoate (712 mg) as a colorless oil.

References

[1] Patent: WO2018/140809, 2018, A1. Location in patent: Paragraph 00463
[2] Patent: JP2016/141632, 2016, A. Location in patent: Paragraph 0516; 0518

METHYL 3,4,5-TRIFLUOROBENZENECARBOXYLATE Preparation Products And Raw materials

Raw materials

Preparation Products

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METHYL 3,4,5-TRIFLUOROBENZENECARBOXYLATE Suppliers

China 47 Germany 2 India 1 United Kingdom 3 United States 10 Global 63

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773873-72-6, METHYL 3,4,5-TRIFLUOROBENZENECARBOXYLATERelated Search:

Methyl Oleate

RARECHEM AL BF 0343

METHYL 3,4,5-TRIFLUOROBENZENECARBOXYLATE

Methyl 3,4,5-trifluorobenzoate

5-trifluorobenzoate

Methyl 3

3,4,5-trifluoroMethyl benzoate

3,4,5-Trifluorobenzoic acid methyl ester

Methyl3,4,5-trifluorobenzoate99%

3,4,5-fluorobenzoate

Benzoic acid, 3,4,5-trifluoro-, methyl ester

773873-72-6