ChemicalBook > CAS DataBase List > 14-HydroxyMyristic acid

14-HydroxyMyristic acid

Product Name: 14-HydroxyMyristic acid
CAS No.: 17278-74-9
Chemical Name: 14-HydroxyMyristic acid
Synonyms: 14-HydroxyMyristic acid;Tetradecanoic acid, 14-hydroxy-;14-Hydroxytetradecanoic acid, 98 +%;14-Hydroxytetradecanoic acid - [H72227]
CBNumber: CB22549701
Molecular Formula: C14H28O3
Formula Weight: 244.37
MOL File: 17278-74-9.mol

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14-HydroxyMyristic acid Property

Melting point:: 86-87 °C(Solv: acetone (67-64-1))
Boiling point:: 387.1±15.0 °C(Predicted)
Density: 0.970±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 4.78±0.10(Predicted)
Appearance: Off-white to light yellow Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: 6904CJ
Product name: 14-Hydroxytetradecanoicacid
Packaging: 100mg
Price: $208
Updated: 2021/12/16

AK Scientific

Product number: 6904CJ
Product name: 14-Hydroxytetradecanoicacid
Packaging: 1g
Price: $575
Updated: 2021/12/16

Ambeed

Product number: A209054
Product name: 14-Hydroxytetradecanoicacid
Purity: 95%
Packaging: 1g
Price: $382
Updated: 2021/12/16

Crysdot

Product number: CD13020556
Product name: 14-Hydroxytetradecanoicacid
Purity: 95+%
Packaging: 1g
Price: $396
Updated: 2021/12/16

Ambeed

Product number: A209054
Product name: 14-Hydroxytetradecanoicacid
Purity: 95%
Packaging: 50mg
Price: $85
Updated: 2021/12/16

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14-HydroxyMyristic acid Chemical Properties,Usage,Production

Definition

ChEBI: A long-chain fatty acid that is myristic (tetradecanoic) acid substituted at position 14 by a hydroxy group.

Synthesis

1147745-12-7

17278-74-9

The general procedure for the synthesis of 14-hydroxytetradecanoic acid from the compound (CAS: 1147745-12-7) as a starting material is as follows: a solution of potassium hydroxide (8.60 g, 153 mmol) in water (100 mL) was added to a solution of the above ester (9.20 g, 30.6 mmol) in methanol (100 mL), and the reaction mixture was heated and reacted for 2 days at 60 °C. . After completion of the reaction, the mixture was cooled to room temperature and subsequently washed with hexane (2 x 70 mL) and concentrated under vacuum. Then, concentrated hydrochloric acid (32%, 20 mL, 0.65 mol) was added dropwise and the mixture was extracted with ethyl acetate (2 × 150 mL). The organic layers were combined, dried over anhydrous magnesium sulfate and evaporated to dryness to give 14-hydroxytetradecanoic acid as a white solid. Yield: 7.10 g (95%). Thin layer chromatography (TLC) analysis (silica gel plate, chloroform:methanol = 85:15): rf = 0.50. 1H NMR spectrum (300 MHz, CDCl3, δH): 3.66 (t, J = 6.6 Hz, 2H); 2.36 (t, J = 7.4 Hz, 2H); 1.72-1.52 (m, 4H); 1.29 (bs, 18H).

References

[1] Patent: US2016/289283, 2016, A1. Location in patent: Paragraph 0254; 0255; 0256; 0257

14-HydroxyMyristic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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17278-74-9, 14-HydroxyMyristic acidRelated Search:

Tetradecanic acid (myristic acid)

14-Hydroxytetradecanoic acid, 98 +%

14-HydroxyMyristic acid

Tetradecanoic acid, 14-hydroxy-

14-Hydroxytetradecanoic acid - [H72227]

17278-74-9