1-(2-Methoxyethyl)-4-nitro-1H-pyrazole

Product Name: 1-(2-Methoxyethyl)-4-nitro-1H-pyrazole
CAS No.: 948570-75-0
Chemical Name: 1-(2-Methoxyethyl)-4-nitro-1H-pyrazole
Synonyms: 1-(2-Methoxyethyl)-4-nitropyrazole;1-(2-Methoxyethyl)-4-nitro-1H-pyrazole;1H-Pyrazole, 1-(2-methoxyethyl)-4-nitro-
CBNumber: CB22599216
Molecular Formula: C6H9N3O3
Formula Weight: 171.15
MOL File: 948570-75-0.mol

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1-(2-Methoxyethyl)-4-nitro-1H-pyrazole Property

Boiling point:: 290.1±20.0 °C(Predicted)
Density: 1.34±0.1 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: -2.29±0.10(Predicted)
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H320Causes eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B486310
Product name: 1-(2-Methoxyethyl)-4-nitro-1H-pyrazole
Packaging: 100mg
Price: $75
Updated: 2021/12/16

AK Scientific

Product number: V9483
Product name: 1-(2-Methoxyethyl)-4-nitropyrazole
Packaging: 1g
Price: $117
Updated: 2021/12/16

AK Scientific

Product number: V9483
Product name: 1-(2-Methoxyethyl)-4-nitropyrazole
Packaging: 25g
Price: $477
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0295126
Product name: 1-(2-METHOXYETHYL)-4-NITRO-1H-PYRAZOLE
Purity: 95.00%
Packaging: 5MG
Price: $500.3
Updated: 2021/12/16

Ambeed

Product number: A219038
Product name: 1-(2-Methoxyethyl)-4-nitro-1H-pyrazole
Purity: 97%
Packaging: 250mg
Price: $23
Updated: 2021/12/16

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1-(2-Methoxyethyl)-4-nitro-1H-pyrazole Chemical Properties,Usage,Production

Synthesis

2075-46-9

6482-24-2

948570-75-0

To a solution of 4-nitro-1H-pyrazole (113 mg, 1 mmol, 1.0 eq.) in acetonitrile (5 mL) was added 2-bromoethyl methyl ether (138 mg, 1 mmol, 1.0 eq.) and potassium carbonate (276 mg, 2 mmol, 2.0 eq.) in that order. The reaction mixture was stirred at 80 °C for 4 hours. After completion of the reaction, the reaction mixture was diluted with ethyl acetate (100 mL) and washed with water (50 mL × 2). The organic layers were combined, concentrated and purified by silica gel column chromatography (petroleum ether/ethyl acetate = 10:1) to afford 1-(2-methoxyethyl)-4-nitro-1H-pyrazole (170 mg, yield: 100%) as a colorless oil.ESI-MS (M + H): 172.1.1 1H NMR (400 MHz, CDCl3) δ: 8.23 (s, 1H) , 8.07 (s, 1H), 4.31 (t, J = 5.2 Hz, 2H), 3.74 (t, J = 5.2 Hz, 2H), 3.35 (s, 3H).

References

[1] Patent: WO2015/89337, 2015, A1. Location in patent: Paragraph 0223
[2] Patent: WO2015/25197, 2015, A1. Location in patent: Paragraph 00078
[3] Patent: US2014/200206, 2014, A1. Location in patent: Paragraph 0339
[4] Patent: WO2007/99326, 2007, A1. Location in patent: Page/Page column 104

1-(2-Methoxyethyl)-4-nitro-1H-pyrazole Preparation Products And Raw materials

Raw materials

Preparation Products

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1-(2-Methoxyethyl)-4-nitro-1H-pyrazole Suppliers

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948570-75-0