Methyl 2-(3-aMinophenyl)acetate hydrochloride
- Product Name
- Methyl 2-(3-aMinophenyl)acetate hydrochloride
- CAS No.
- 150319-83-8
- Chemical Name
- Methyl 2-(3-aMinophenyl)acetate hydrochloride
- Synonyms
- Methyl 2-(3-aminophenyl);3-AMinophenylacetic acid Methyl ester HCl;Methyl 2-(3-aMinophenyl)acetate hydrochloride;3-Aminophenylacetic acid methyl ester hydrochloride;Benzeneacetic acid, 3-amino-, methyl ester, hydrochloride (1:1)
- CBNumber
- CB22616937
- Molecular Formula
- C9H12ClNO2
- Formula Weight
- 201.65008
- MOL File
- 150319-83-8.mol
Methyl 2-(3-aMinophenyl)acetate hydrochloride Property
- Melting point:
- 167-170 °C(Solv: ethanol (64-17-5); ethyl ether (60-29-7))
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- crystalline powder
- color
- Pale pink
Safety
- HS Code
- 2916391000
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M328765
- Product name
- Methyl3-aminophenylacetatehydrochloride
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- W3284
- Product name
- Methyl2-(3-aminophenyl)acetatehydrochloride
- Packaging
- 1g
- Price
- $101
- Updated
- 2021/12/16
- Product number
- P000022804
- Product name
- Methyl 2-(3-aminophenyl)acetate hydrochloride
- Purity
- 95+%
- Packaging
- 5g
- Price
- $107
- Updated
- 2021/12/16
- Product number
- OR59469
- Product name
- Methyl3-aminophenylacetatehydrochloride
- Packaging
- 5g
- Price
- $124
- Updated
- 2021/12/16
- Product number
- 4758-5-X2
- Product name
- Methyl 3-aminophenylacetate hydrochloride
- Packaging
- 5G
- Price
- $136
- Updated
- 2021/12/16
Methyl 2-(3-aMinophenyl)acetate hydrochloride Chemical Properties,Usage,Production
Synthesis
14338-36-4
150319-83-8
A. Synthesis of methyl 3-aminophenylacetate hydrochloride Thionyl chloride (19.4 g, 165 mmol) was added slowly and dropwise to a methanolic (50 ml) suspension of 3-aminophenylacetic acid (5.0 g, 33 mmol) at 0°C and under argon protection. After the dropwise addition, the reaction mixture was gradually warmed up to room temperature and stirred continuously for 16 hours. After completion of the reaction, the solvent was removed by evaporation under reduced pressure and the resulting residue was ground with ether to give methyl 3-aminophenylacetate hydrochloride (5.3 g, 96.8% yield) as a colorless solid. 1H NMR (CDCl3) δ: 10.6 (s, 2H), 7.42 (m, 4H), 3.68 (s, 3H), 3.66 (s, 2H). 13C NMR (CDCl3) δ: 172.5, 137.3, 133.1, 131.2, 130.8, 125.9, 123.7, 53.5, 41.5.
References
[1] Patent: US5276168, 1994, A
Methyl 2-(3-aMinophenyl)acetate hydrochloride Preparation Products And Raw materials
Raw materials
Preparation Products
Methyl 2-(3-aMinophenyl)acetate hydrochloride Suppliers
- Tel
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- Fax
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- sales@apolloscientific.co.uk
- Country
- United Kingdom
- ProdList
- 6084
- Advantage
- 88
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- enquiries@fluorochem.co.uk
- Country
- United Kingdom
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View Lastest Price from Methyl 2-(3-aMinophenyl)acetate hydrochloride manufacturers
- Product
- Methyl 2-(3-aMinophenyl)acetate hydrochloride 150319-83-8
- Price
- US $1.30/g
- Min. Order
- 1g
- Purity
- 98%
- Supply Ability
- 1kg,10kg,100kg
- Release date
- 2020-10-28
- Product
- Methyl 2-(3-aMinophenyl)acetate hydrochloride 150319-83-8
- Price
- US $85.00-850.00/kg
- Min. Order
- 10kg
- Purity
- 0.99
- Supply Ability
- 20tons
- Release date
- 2023-11-09