PiperidiniuM, 1-ethyl-1-Methyl-4-oxo-, iodide (1:1)
- Product Name
- PiperidiniuM, 1-ethyl-1-Methyl-4-oxo-, iodide (1:1)
- CAS No.
- 77542-18-8
- Chemical Name
- PiperidiniuM, 1-ethyl-1-Methyl-4-oxo-, iodide (1:1)
- Synonyms
- SKL520;EOS-60490;1-ethyl-1-methyl-piperidin-1-ium-4-one;1-methyl-1-ethyl-4-oxopiperidinium iodide;1-Ethyl-1-methyl-4-oxo-piperidinium iodide;1-ethyl-1-methylpiperidin-1-ium-4-one,iodide;PiperidiniuM, 1-ethyl-1-Methyl-4-oxo-, iodide;PiperidiniuM, 1-ethyl-1-Methyl-4-oxo-, iodide (1;PiperidiniuM, 1-ethyl-1-Methyl-4-oxo-, iodide (1:1)
- CBNumber
- CB22624820
- Molecular Formula
- C8H16INO
- Formula Weight
- 269.12321
- MOL File
- 77542-18-8.mol
PiperidiniuM, 1-ethyl-1-Methyl-4-oxo-, iodide (1:1) Property
- Melting point:
- 180-182 °C (decomp)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- Appearance
- White to light yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- P000023786
- Product name
- 1-Ethyl-1-methyl-4-oxopiperidin-1-ium iodide
- Purity
- 95+%
- Packaging
- 1g
- Price
- $109
- Updated
- 2021/12/16
- Product number
- 4354CS
- Product name
- 1-Ethyl-1-methyl-4-oxopiperidin-1-iumiodide
- Packaging
- 250mg
- Price
- $112
- Updated
- 2021/12/16
- Product number
- P000023786
- Product name
- 1-Ethyl-1-methyl-4-oxopiperidin-1-ium iodide
- Purity
- 95+%
- Packaging
- 5g
- Price
- $390
- Updated
- 2021/12/16
- Product number
- CHM0387065
- Product name
- 1-ETHYL-1-METHYL-4-OXOPIPERIDIN-1-IUM IODIDE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $502.62
- Updated
- 2021/12/16
- Product number
- 4354CS
- Product name
- 1-Ethyl-1-methyl-4-oxopiperidin-1-iumiodide
- Packaging
- 5g
- Price
- $544
- Updated
- 2021/12/16
PiperidiniuM, 1-ethyl-1-Methyl-4-oxo-, iodide (1:1) Chemical Properties,Usage,Production
Synthesis
1445-73-4
75-03-6
77542-18-8
General steps: 1. Preparation of 1-ethyl-1-methyl-4-oxopiperidine-1-iodide 1-Methylpiperidin-4-one (13.8 mL, 120 mmol) was dissolved in butan-2-one (70 mL) followed by the addition of ethyl iodide (10.6 mL, 132 mmol). The reaction mixture was stirred at room temperature for 4 days. Upon completion of the reaction, the mixture was filtered and the solid product was collected and dried under vacuum to afford the title compound as an orange solid (27.8 g, 86% yield). The product was confirmed by NMR hydrogen spectrum (300 MHz, D2O): δ 3.52-3.38 (m, 6H), 3.05 (s, 3H), 2.17-1.99 (m, 4H), 1.34 (t, J = 7.3 Hz, 3H); mass spectrum (ES+) m/z 142.2 (M + 1).
References
[1] Green Chemistry, 2017, vol. 19, # 3, p. 614 - 618
[2] ChemMedChem, 2015, vol. 10, # 7, p. 1249 - 1258
[3] Patent: WO2017/201468, 2017, A1. Location in patent: Page/Page column 163
[4] Organic Process Research and Development, 2012, vol. 16, # 1, p. 109 - 116
[5] Bioorganic and Medicinal Chemistry, 2010, vol. 18, # 21, p. 7675 - 7699
PiperidiniuM, 1-ethyl-1-Methyl-4-oxo-, iodide (1:1) Preparation Products And Raw materials
Raw materials
Preparation Products
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