3-(Benzyloxy)cyclobutanol

Product Name: 3-(Benzyloxy)cyclobutanol
CAS No.: 100058-61-5
Chemical Name: 3-(Benzyloxy)cyclobutanol
Synonyms: 3-(Benzyloxy)cyclobutanol;3-(benzyloxy)cyclobutan-1-ol;3-(Benzyloxy)cyclobutanol 97%;3-(phenylmethoxy)cyclobutan-1-ol;Cyclobutanol, 3-(phenylmethoxy)-
CBNumber: CB22631958
Molecular Formula: C11H14O2
Formula Weight: 178.23
MOL File: 100058-61-5.mol

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3-(Benzyloxy)cyclobutanol Property

Boiling point:: 145 °C(Press: 4 Torr)
Density: 1.0773 g/cm3(Temp: 25 °C)
storage temp.: Sealed in dry,Room Temperature
form: liquid
pka: 14.78±0.40(Predicted)
color: Colourless
InChI: InChI=1S/C11H14O2/c12-10-6-11(7-10)13-8-9-4-2-1-3-5-9/h1-5,10-12H,6-8H2
InChIKey: ZGSDRBWWICYJBU-UHFFFAOYSA-N
SMILES: C1(O)CC(OCC2=CC=CC=C2)C1

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Safety

HS Code: 2906190090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B700438
Product name: 3-(Benzyloxy)cyclobutanol
Packaging: 100mg
Price: $65
Updated: 2021/12/16

TRC

Product number: B700438
Product name: 3-(Benzyloxy)cyclobutanol
Packaging: 1g
Price: $330
Updated: 2021/12/16

Apolloscientific

Product number: OR317118
Product name: 3-(Benzyloxy)cyclobutanol
Packaging: 250mg
Price: $126
Updated: 2021/12/16

AK Scientific

Product number: 0077AA
Product name: 3-Hydroxycyclobutanone
Packaging: 250mg
Price: $144
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2607-1-15
Product name: 3-(Benzyloxy)cyclobutanol
Purity: 98%
Packaging: 250mg
Price: $149
Updated: 2021/12/16

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3-(Benzyloxy)cyclobutanol Chemical Properties,Usage,Production

Synthesis

30830-27-4

100058-61-5

Step 1. 3-(Benzyloxy)cyclobutanone (2.00 g, 11.4 mmol), tetrahydrofuran (20 mL), and methanol (1 mL) were added to a 100 mL round-bottomed flask, and the reaction system was cooled to 0 °C. The reaction system was then cooled to 0 °C. The reaction mixture was then stirred for 30 minutes at room temperature. Subsequently, sodium borohydride (0.475 g, 12.5 mmol) was added in batches, and after addition, the reaction mixture was stirred at room temperature for 30 minutes. After completion of the reaction, the mixture was poured into water (30 mL) and extracted with ethyl acetate (2 x 30 mL). The organic layers were combined, dried over anhydrous sodium sulfate, filtered and concentrated to give 3-(benzyloxy)cyclobutanol (1.83 g, 90%) as a yellow oil.MS (ESI, cationic) m/z 179 [M + H]+.

References

[1] Patent: WO2014/43272, 2014, A1. Location in patent: Paragraph 0298; 0304; 0305; 0306
[2] Patent: WO2018/137573, 2018, A1. Location in patent: Page/Page column 98
[3] Patent: US6579875, 2003, B1
[4] Patent: WO2015/74064, 2015, A2. Location in patent: Paragraph 0640
[5] ACS Medicinal Chemistry Letters, 2016, vol. 7, # 7, p. 666 - 670

3-(Benzyloxy)cyclobutanol Preparation Products And Raw materials

Raw materials

Preparation Products

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3-(Benzyloxy)cyclobutanol Suppliers

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100058-61-5, 3-(Benzyloxy)cyclobutanolRelated Search:

3-(Benzyloxy)cyclobutanol

3-(Benzyloxy)cyclobutanol 97%

3-(benzyloxy)cyclobutan-1-ol

Cyclobutanol, 3-(phenylmethoxy)-

3-(phenylmethoxy)cyclobutan-1-ol

100058-61-5