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1H-Indazole, 6-bromo-1,3-dimethyl-

Product Name
1H-Indazole, 6-bromo-1,3-dimethyl-
CAS No.
1095539-84-6
Chemical Name
1H-Indazole, 6-bromo-1,3-dimethyl-
Synonyms
6-BroMo-1,3-diMethyl-1H-i...;6-Bromo-1,3-dimethyl-indazole;1H-Indazole, 6-bromo-1,3-dimethyl-;6-Bromo-1,3-dimethyl-1H-indazole 95+%
CBNumber
CB22632016
Molecular Formula
C9H9BrN2
Formula Weight
225.09
MOL File
1095539-84-6.mol
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1H-Indazole, 6-bromo-1,3-dimethyl- Property

Boiling point:
310.9±22.0 °C(Predicted)
Density 
1.53±0.1 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
1.38±0.50(Predicted)
Appearance
White to off-white Solid
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Safety

HS Code 
2933998090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
B997845
Product name
6-Bromo-1,3-dimethyl-1H-indazole
Packaging
100mg
Price
$90
Updated
2021/12/16
SynQuest Laboratories
Product number
3H32-9-4N
Product name
6-Bromo-1,3-dimethyl-1H-indazole
Packaging
5G
Price
$1188
Updated
2021/12/16
Matrix Scientific
Product number
112338
Product name
6-Bromo-1,3-dimethyl-1H-indazole
Packaging
5g
Price
$1210
Updated
2021/12/16
Apolloscientific
Product number
OR40130
Product name
6-Bromo-1,3-dimethyl-1H-indazole
Purity
95+%
Packaging
250mg
Price
$118
Updated
2021/12/16
SynQuest Laboratories
Product number
3H32-9-4N
Product name
6-Bromo-1,3-dimethyl-1H-indazole
Packaging
250mg
Price
$119
Updated
2021/12/16
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1H-Indazole, 6-bromo-1,3-dimethyl- Chemical Properties,Usage,Production

Synthesis

865156-82-7

60-34-4

1095539-84-6

1. 2-Acetyl-5-bromophenyl methanesulfonate was prepared according to the method described in International Application Publication No. WO 2005/090305 (Example 40a). 2. 2-acetyl-5-bromophenyl methanesulfonate was mixed with methylhydrazine and ammonium acetate and reacted under reflux conditions for 6 days to obtain 6-bromo-1,3-dimethyl-1H-indazole in 60% yield. 3. 6-Bromo-1,3-dimethyl-1H-indazole was dissolved in THF and treated with n-BuLi, followed by the passage of carbon dioxide gas, and the reaction afforded the target compound in a yield of 1.23 g in 60% yield.

References

[1] Patent: WO2008/65508, 2008, A1. Location in patent: Page/Page column 34

1H-Indazole, 6-bromo-1,3-dimethyl- Preparation Products And Raw materials

Raw materials

Preparation Products

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1H-Indazole, 6-bromo-1,3-dimethyl- Suppliers

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