ChemicalBook > CAS DataBase List > Pyridine, 2-chloro-6-Methoxy-4-Methyl-
Pyridine, 2-chloro-6-Methoxy-4-Methyl-
- Product Name
- Pyridine, 2-chloro-6-Methoxy-4-Methyl-
- CAS No.
- 25297-52-3
- Chemical Name
- Pyridine, 2-chloro-6-Methoxy-4-Methyl-
- Synonyms
- 2-Chloro-6-Methoxy-4-Methylpyridine;Pyridine, 2-chloro-6-Methoxy-4-Methyl-
- CBNumber
- CB22640222
- Molecular Formula
- C7H8ClNO
- Formula Weight
- 157.6
- MOL File
- 25297-52-3.mol
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Pyridine, 2-chloro-6-Methoxy-4-Methyl- Property
- storage temp.
- Inert atmosphere,Room Temperature
- Appearance
- Colorless to light yellow Liquid
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N-Bromosuccinimide Price
AK Scientific
- Product number
- 7955DN
- Product name
- 2-Chloro-6-methoxy-4-methylpyridine
- Packaging
- 5g
- Price
- $566
- Updated
- 2021/12/16
AK Scientific
- Product number
- 7955DN
- Product name
- 2-Chloro-6-methoxy-4-methylpyridine
- Packaging
- 250mg
- Price
- $104
- Updated
- 2021/12/16
Crysdot
- Product number
- CD11158514
- Product name
- 2-Chloro-6-methoxy-4-methylpyridine
- Purity
- 97%
- Packaging
- 5g
- Price
- $356
- Updated
- 2021/12/16
Ambeed
- Product number
- A213553
- Product name
- 2-Chloro-6-methoxy-4-methylpyridine
- Purity
- 97%
- Packaging
- 5g
- Price
- $375
- Updated
- 2021/12/16
Chemenu
- Product number
- CM171409
- Product name
- 2-chloro-6-methoxy-4-methylpyridine
- Purity
- 97%
- Packaging
- 1g
- Price
- $386
- Updated
- 2021/12/16
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Pyridine, 2-chloro-6-Methoxy-4-Methyl- Chemical Properties,Usage,Production
Synthesis
67-56-1
39621-00-6
25297-52-3
The general procedure for synthesizing 2-chloro-6-methoxy-4-methylpyridine from methanol and 2,6-dichloro-4-methylpyridine is as follows: referring to the method of Example 53; 2,6-dichloro-4-methylpyridine (250 mg, 1.5 mmol) was dissolved in methanol (2 mL), and this solution was then added to a pre-prepared sodium methanol solution (prepared by the reaction of sodium (71 mg, 3.0 mmol ) was prepared by reacting with anhydrous methanol in a total volume of about 20 mL). Subsequently, the reaction mixture was heated to reflux for 48 hours. Upon completion of the reaction, the solvent was removed by evaporation and the residue was extracted by partitioning with water and dichloromethane. The organic layer was separated, washed sequentially with water and brine, and then dried over anhydrous sodium sulfate. Finally, the dried organic phase was concentrated to afford the target product 2-chloro-6-methoxy-4-methylpyridine (150 mg, 61% yield) as a light orange oily liquid.
References
[1] Inorganic Chemistry, 2017, vol. 56, # 13, p. 7519 - 7532
[2] Patent: US2011/9390, 2011, A1. Location in patent: Page/Page column 19-20
Pyridine, 2-chloro-6-Methoxy-4-Methyl- Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Pyridine, 2-chloro-6-Methoxy-4-Methyl- manufacturers
Nanjing jinheyou Trading Co., Ltd.
- Product
- Pyridine, 2-chloro-6-Methoxy-4-Methyl- 25297-52-3
- Price
- US $0.00/g
- Min. Order
- 1g
- Purity
- 95%min
- Supply Ability
- 20kg/month
- Release date
- 2019-12-19