Ethyl 2,6-dichloro-4-Methylnicotinate
- Product Name
- Ethyl 2,6-dichloro-4-Methylnicotinate
- CAS No.
- 108130-10-5
- Chemical Name
- Ethyl 2,6-dichloro-4-Methylnicotinate
- Synonyms
- Ethyl 2,6-dichloro-4-Methylnicotinate;3-Pyridinecarboxylic acid, 2,6-dichloro-4-methyl-, ethyl ester
- CBNumber
- CB22641012
- Molecular Formula
- C9H9Cl2NO2
- Formula Weight
- 234.08
- MOL File
- 108130-10-5.mol
Ethyl 2,6-dichloro-4-Methylnicotinate Property
- Boiling point:
- 307.0±37.0 °C(Predicted)
- Density
- 1.320±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- pka
- -3.68±0.10(Predicted)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H402Harmful to aquatic life
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P273Avoid release to the environment.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- HCH0368735
- Product name
- ETHYL-2,6-DICHLORO-4-METHYLNICOTINATE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $501.14
- Updated
- 2021/12/16
- Product number
- 119583
- Product name
- Ethyl 2,6-dichloro-4-methylnicotinate
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $180
- Updated
- 2021/12/16
- Product number
- 119583
- Product name
- Ethyl 2,6-dichloro-4-methylnicotinate
- Purity
- 95+%
- Packaging
- 1g
- Price
- $450
- Updated
- 2021/12/16
- Product number
- Z3868
- Product name
- Ethyl2,6-dichloro-4-methylnicotinate
- Packaging
- 5g
- Price
- $779
- Updated
- 2021/12/16
- Product number
- 119583
- Product name
- Ethyl 2,6-dichloro-4-methylnicotinate
- Purity
- 95+%
- Packaging
- 5g
- Price
- $1404
- Updated
- 2021/12/16
Ethyl 2,6-dichloro-4-Methylnicotinate Chemical Properties,Usage,Production
Synthesis
62774-90-7
75-03-6
108130-10-5
2,6-Dichloro-4-methylpyridine-3-carboxylic acid (100 g, 485 mmol) and potassium carbonate (100 g, 728 mmol) were stirred in dimethylformamide (1.25 L) for 30 hours at room temperature. Subsequently, ethyl iodide (59.5 mL, 728 mmol) was added to the reaction system and stirring was continued for 18 hours. After completion of the reaction, water was added to the mixture and extracted with ethyl acetate (3×). The organic layers were combined, washed sequentially with water (2×) and brine (1×), dried over magnesium sulfate, and the solvent was evaporated to dryness under reduced pressure to afford ethyl 2,6-dichloro-4-methylpyridine-3-carboxylate (112 g), which was used for subsequent reactions without further purification.
References
[1] Patent: WO2013/156154, 2013, A1. Location in patent: Page/Page column 49
Ethyl 2,6-dichloro-4-Methylnicotinate Preparation Products And Raw materials
Raw materials
Preparation Products
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