2-Phenyl-7-BroMoquinoline
- Product Name
- 2-Phenyl-7-BroMoquinoline
- CAS No.
- 1203578-65-7
- Chemical Name
- 2-Phenyl-7-BroMoquinoline
- Synonyms
- 7-broMo-2-phenylquinoline;2-Phenyl-7-BroMoquinoline;Quinoline, 7-bromo-2-phenyl-;7-Bromo-2-phenylquinoline 95+%
- CBNumber
- CB22652799
- Molecular Formula
- C15H10BrN
- Formula Weight
- 284.15
- MOL File
- 1203578-65-7.mol
2-Phenyl-7-BroMoquinoline Property
- Melting point:
- 122.0-123.5℃
- Density
- 1.433±0.06 g/cm3 (20℃ 760 Torr)
- storage temp.
- Sealed in dry,Room Temperature
Safety
- HS Code
- 2933499090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B997778
- Product name
- 7-Bromo-2-phenylquinoline
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- OR350432
- Product name
- 7-Bromo-2-phenylquinoline
- Purity
- 95+%
- Packaging
- 1g
- Price
- $242
- Updated
- 2021/12/16
- Product number
- 3H32-9-C1
- Product name
- 7-Bromo-2-phenylquinoline
- Packaging
- 1g
- Price
- $287
- Updated
- 2021/12/16
- Product number
- OR350432
- Product name
- 7-Bromo-2-phenylquinoline
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $98
- Updated
- 2021/12/16
- Product number
- 3H32-9-C1
- Product name
- 7-Bromo-2-phenylquinoline
- Packaging
- 250mg
- Price
- $116
- Updated
- 2021/12/16
2-Phenyl-7-BroMoquinoline Chemical Properties,Usage,Production
Synthesis
946122-05-0
98-86-2
1203578-65-7
General procedure for the synthesis of 2-phenyl-7-bromoquinoline from (2-amino-4-bromophenyl)methanol and acetophenone: acetophenone (144 mg, 1.2 mmol), [Cp*Ir(6,6'-(OH)2bpy)(H2O)][OTf]2 (8.3 mg, 0.01 mmol, 1 mol%), potassium hydroxide (56 mg, 1.0 mmol, 1.0 equiv), 2-amino-4-bromobenzyl alcohol (201 mg, 1.0 mmol), and water (1 mL) were added sequentially to a 5 mL round bottom flask. The reaction mixture was refluxed in air for 12 h and then cooled to room temperature. The reaction mixture was extracted with ethyl acetate, the organic solvent was removed by rotary evaporation, and then purified by column chromatography (unfolding agent: petroleum ether/ethyl acetate) to afford pure 2-phenyl-7-bromoquinoline in 94% yield.
References
[1] Patent: CN107400084, 2017, A. Location in patent: Paragraph 0141; 0142; 0143
[2] Organic Letters, 2016, vol. 18, # 15, p. 3558 - 3561
[3] Organic and Biomolecular Chemistry, 2018, vol. 16, # 2, p. 274 - 284
2-Phenyl-7-BroMoquinoline Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-Phenyl-7-BroMoquinoline manufacturers
- Product
- 2-Phenyl-7-BroMoquinoline 1203578-65-7
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- ≥98%
- Supply Ability
- g/kg/Ton
- Release date
- 2019-12-25