5-phenylMorpholin-3-one

Product Name: 5-phenylMorpholin-3-one
CAS No.: 1260672-03-4
Chemical Name: 5-phenylMorpholin-3-one
Synonyms: 5-phenyl-3-morpholinone;3-Morpholinone, 5-phenyl-
CBNumber: CB22678186
Molecular Formula: C10H11NO2
Formula Weight: 177.2
MOL File: 1260672-03-4.mol

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5-phenylMorpholin-3-one Property

Boiling point:: 401.9±45.0 °C(Predicted)
Density: 1.149±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 13.66±0.40(Predicted)
Appearance: Light brown to brown Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: B401325
Product name: 5-phenylmorpholin-3-one
Packaging: 25mg
Price: $45
Updated: 2021/12/16

Matrix Scientific

Product number: 132455
Product name: 5-Phenylmorpholin-3-one
Purity: 97%
Packaging: 1g
Price: $666
Updated: 2021/12/16

Matrix Scientific

Product number: 132455
Product name: 5-Phenylmorpholin-3-one
Purity: 97%
Packaging: 5g
Price: $1980
Updated: 2021/12/16

Chemenu

Product number: CM119999
Product name: 5-Phenylmorpholin-3-one
Purity: 95%
Packaging: 5g
Price: $678
Updated: 2021/12/16

Ambeed

Product number: A174835
Product name: 5-Phenylmorpholin-3-one
Purity: 95+%
Packaging: 5g
Price: $688
Updated: 2021/12/16

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5-phenylMorpholin-3-one Chemical Properties,Usage,Production

Synthesis

94193-77-8

1260672-03-4

General procedure for the synthesis of 5-phenylmorpholin-3-one from the compound (CAS:94193-77-8): crude 2-chloro-N-(2-hydroxy-1-phenylethyl)acetamide (3 g, 14.04 mmol) was dissolved in anhydrous tetrahydrofuran (THF, 40 mL) and the reaction mixture was cooled to 0 °C. Sodium hydride (NaH, 0.842 g, 35.1 mmol) was added in two portions, followed by slow warming of the reaction mixture to room temperature. Upon completion of the reaction, the reaction was quenched by slow addition of 50% THF/water solution followed by dilution with ethyl acetate (EtOAc). The organic layer was washed sequentially with aqueous sodium bicarbonate (NaHCO3), water and brine. The organic phases were combined and purified by fast column chromatography (eluent: 30-100% EtOAc/heptane gradient) to afford the target product 5-phenylmorpholin-3-one (2.25 g, 90% yield). Liquid chromatography-mass spectrometry (LC/MS) analysis showed the following results: retention time (Rt) = 0.39 min (Table 1, method f); mass spectrum (MS) m/z: 219 ([M+H+MeCN]+).

References

[1] Patent: WO2016/168641, 2016, A1. Location in patent: Page/Page column 145; 146

5-phenylMorpholin-3-one Preparation Products And Raw materials

Raw materials

Preparation Products

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5-phenylMorpholin-3-one Suppliers

China 27 India 1 United States 4 Global 32

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1260672-03-4