1-broMo-4-fluoro-2-Methoxy-5-nitrobenzene

Product Name: 1-broMo-4-fluoro-2-Methoxy-5-nitrobenzene
CAS No.: 935288-20-3
Chemical Name: 1-broMo-4-fluoro-2-Methoxy-5-nitrobenzene
Synonyms: 110853;2-Bromo-5-fluoro-4-nitroanisole;1-broMo-4-fluoro-2-Methoxy-5-nitrobenzene;Benzene, 1-bromo-4-fluoro-2-methoxy-5-nitro-
CBNumber: CB22718334
Molecular Formula: C7H5BrFNO3
Formula Weight: 250.02
MOL File: 935288-20-3.mol

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1-broMo-4-fluoro-2-Methoxy-5-nitrobenzene Property

Melting point:: 74-75°
Boiling point:: 299.7±35.0 °C(Predicted)
Density: 1.716±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
Appearance: Off-white to yellow Solid
InChI: InChI=1S/C7H5BrFNO3/c1-13-7-3-5(9)6(10(11)12)2-4(7)8/h2-3H,1H3
InChIKey: GTIYDLQTZFEZEA-UHFFFAOYSA-N
SMILES: C1(Br)=CC([N+]([O-])=O)=C(F)C=C1OC

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Safety

Risk Statements: 36/37/38
Safety Statements: 26-36/37/39
HS Code: 29049090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B701075
Product name: 1-Bromo-4-fluoro-2-methoxy-5-nitrobenzene
Packaging: 100mg
Price: $60
Updated: 2021/12/16

Oakwood

Product number: 097605
Product name: 1-Bromo-4-fluoro-2-methoxy-5-nitrobenzene
Purity: 98%
Packaging: 250mg
Price: $30
Updated: 2021/12/16

AK Scientific

Product number: 9036DT
Product name: 1-Bromo-4-fluoro-2-methoxy-5-nitrobenzene
Packaging: 1g
Price: $192
Updated: 2021/12/16

Matrix Scientific

Product number: 120644
Product name: 1-Bromo-4-fluoro-2-methoxy-5-nitrobenzene
Purity: 97%
Packaging: 1g
Price: $900
Updated: 2021/12/16

Matrix Scientific

Product number: 120644
Product name: 1-Bromo-4-fluoro-2-methoxy-5-nitrobenzene
Purity: 97%
Packaging: 5g
Price: $1797
Updated: 2021/12/16

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1-broMo-4-fluoro-2-Methoxy-5-nitrobenzene Chemical Properties,Usage,Production

Synthesis

1075705-01-9

935288-20-3

Under nitrogen protection, copper bromide (3.568 g, 16 mmol, 1.5 eq.) was dissolved with tert-butyl nitrite (3.399 g, 33 mmol, 3 eq.) in acetonitrile (250 mL), heated to 50 °C and stirred. Subsequently, a solution of 4-fluoro-2-methoxy-5-nitroaniline (2 g, 11 mmol, 1 eq.) dissolved in acetonitrile (20 mL) was slowly added dropwise to the reaction system, and the reaction was continued with stirring for 2.5 hours. After completion of the reaction, the reaction mixture was cooled to room temperature and separated by extraction with ethyl acetate and water. The organic phase was washed with water and saturated saline in turn, dried over anhydrous sodium sulfate, and concentrated under reduced pressure to obtain a brown oily crude product. The crude product was purified by silica gel column chromatography (eluent: petroleum ether/ethyl acetate=10/1) to afford the target compound 1-bromo-4-fluoro-2-methoxy-5-nitrobenzene as yellow solid (1.87 g, yield 69.57%).

References

[1] Patent: EP3345900, 2018, A1. Location in patent: Paragraph 0044

1-broMo-4-fluoro-2-Methoxy-5-nitrobenzene Preparation Products And Raw materials

Raw materials

Preparation Products

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1-broMo-4-fluoro-2-Methoxy-5-nitrobenzene Suppliers

China 69 India 1 United States 6 Global 76

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View Lastest Price from 1-broMo-4-fluoro-2-Methoxy-5-nitrobenzene manufacturers

Career Henan Chemical Co

Product: 1-broMo-4-fluoro-2-Methoxy-5-nitrobenzene 935288-20-3
Price: US $6.68/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg-1000kg
Release date: 2020-01-08

935288-20-3, 1-broMo-4-fluoro-2-Methoxy-5-nitrobenzeneRelated Search:

1-broMo-4-fluoro-2-Methoxy-5-nitrobenzene

110853

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2-Bromo-5-fluoro-4-nitroanisole

935288-20-3