Methyl 8-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate

Product Name: Methyl 8-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate
CAS No.: 116047-26-8
Chemical Name: Methyl 8-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate
Synonyms: 7-methoxycarbonyl-1,2,3,4-tetrahydronaphthalene-1-one;methyl 8-oxo-6,7-dihydro-5H-naphthalene-2-carboxylate;methyl 8-oxo-5,6,7,8-tetrahydronaphthalene-1-carboxylate;Methyl 8-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate;2-Naphthalenecarboxylic acid, 5,6,7,8-tetrahydro-8-oxo-, methyl ester
CBNumber: CB22724364
Molecular Formula: C12H12O3
Formula Weight: 204.22
MOL File: 116047-26-8.mol

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Methyl 8-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate Property

storage temp.: Sealed in dry,Room Temperature
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: CHM0393385
Product name: METHYL-8-OXO-5,6,7,8-TETRAHYDRONAPHTHALENE-2-CARBOXYLATE
Purity: 95.00%
Packaging: 5MG
Price: $502.96
Updated: 2021/12/16

AK Scientific

Product number: 2640AA
Product name: Methyl8-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate
Packaging: 2.5g
Price: $1906
Updated: 2021/12/16

AK Scientific

Product number: 2640AA
Product name: Methyl8-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate
Packaging: 10g
Price: $4584
Updated: 2021/12/16

Chemenu

Product number: CM141049
Product name: Methyl8-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate
Purity: 95+%
Packaging: 1g
Price: $688
Updated: 2021/12/16

Alichem

Product number: 116047268
Product name: Methyl8-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate
Packaging: 1g
Price: $720.3
Updated: 2021/12/16

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Methyl 8-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate Chemical Properties,Usage,Production

Synthesis

67-56-1

89781-52-2

116047-26-8

Intermediate VIII: Steps for the synthesis of methyl 8-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate: Step a) Preparation of methyl 8-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate: to a methanolic solution of 8-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylic acid (16 g, 0.084 mol) was added sulfoxide chloride (23 g, 0.2 mol). The reaction mixture was stirred at room temperature for 12 hours. After completion of the reaction, the solvent was removed by distillation under reduced pressure. The residue was dissolved in ethyl acetate (200 mL), the organic layer was washed with 10% aqueous sodium bicarbonate, dried over anhydrous magnesium sulfate, and concentrated under reduced pressure to give methyl 8-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate 16 g (94% yield) as a liquid. Thin layer chromatography (TLC) conditions: chloroform/methanol (9/1, v/v), Rf = 0.9.

References

[1] Patent: WO2005/12280, 2005, A1. Location in patent: Page/Page column 55
[2] Helvetica Chimica Acta, 1993, vol. 76, # 4, p. 1539 - 1563

Methyl 8-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate Preparation Products And Raw materials

Raw materials

Preparation Products

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Methyl 8-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate Suppliers

China 28 India 1 United States 1 Global 30

Shanghai Hanhong Scientific Co.,Ltd.

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Career Henan Chemica Co

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116047-26-8, Methyl 8-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylateRelated Search:

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116047-26-8