6-broMo-N-Methyl-1,3-benzothiazol-2-aMine
- Product Name
- 6-broMo-N-Methyl-1,3-benzothiazol-2-aMine
- CAS No.
- 75104-92-6
- Chemical Name
- 6-broMo-N-Methyl-1,3-benzothiazol-2-aMine
- Synonyms
- 2-Benzothiazolamine, 6-bromo-N-methyl-;6-BroMo-N-Methylbenzo[d]thiazol-2-aMine;(6-Bromo-benzothiazol-2-yl)-methyl-amine;6-broMo-N-Methyl-1,3-benzothiazol-2-aMine
- CBNumber
- CB22727855
- Molecular Formula
- C8H7BrN2S
- Formula Weight
- 243.12
- MOL File
- 75104-92-6.mol
6-broMo-N-Methyl-1,3-benzothiazol-2-aMine Property
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- Appearance
- White to off-white Solid
N-Bromosuccinimide Price
- Product number
- 1681AC
- Product name
- 6-Bromo-N-methylbenzo[d]thiazol-2-amine
- Packaging
- 100mg
- Price
- $76
- Updated
- 2021/12/16
- Product number
- HCH0367846
- Product name
- 6-BROMO-N-METHYLBENZO[D]THIAZOL-2-AMINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $501.84
- Updated
- 2021/12/16
- Product number
- 137891
- Product name
- 6-Bromo-N-methyl-1,3-benzothiazol-2-amine
- Purity
- 95%+
- Packaging
- 1g
- Price
- $524
- Updated
- 2021/12/16
- Product number
- 137891
- Product name
- 6-Bromo-N-methyl-1,3-benzothiazol-2-amine
- Purity
- 95%+
- Packaging
- 2.500g
- Price
- $1144
- Updated
- 2021/12/16
- Product number
- 137891
- Product name
- 6-Bromo-N-methyl-1,3-benzothiazol-2-amine
- Purity
- 95%+
- Packaging
- 5g
- Price
- $1728
- Updated
- 2021/12/16
6-broMo-N-Methyl-1,3-benzothiazol-2-aMine Chemical Properties,Usage,Production
Synthesis
80945-86-4
74-89-5
75104-92-6
In a sealed reaction tube, 6-bromo-2-chlorobenzo[d]thiazole (701) (0.5 g, 2.0 mmol) was dissolved in methylamine solution (20 mL), and the resulting mixture was stirred and reacted at 60 °C overnight. Upon completion of the reaction, the mixture was cooled to room temperature, concentrated under reduced pressure to remove the solvent and quenched by the addition of water (20 mL). The precipitated solid was collected by filtration to afford the target product 6-bromo-N-methylbenzo[d]thiazol-2-amine (702) (0.43 g, 87.9% yield). The product was analyzed by ESI-MS and showed (M + H)+ m/z: 242.8.
References
[1] Patent: US2015/225407, 2015, A1. Location in patent: Paragraph 0416
[2] Recueil des Travaux Chimiques des Pays-Bas, 1934, vol. 53, p. 1
[3] Patent: WO2017/46739, 2017, A1. Location in patent: Page/Page column 50
6-broMo-N-Methyl-1,3-benzothiazol-2-aMine Preparation Products And Raw materials
Raw materials
Preparation Products
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