(2,4-diMethylphenyl)(2-nitrophenyl)sulfane
- Product Name
- (2,4-diMethylphenyl)(2-nitrophenyl)sulfane
- CAS No.
- 1610527-49-5
- Chemical Name
- (2,4-diMethylphenyl)(2-nitrophenyl)sulfane
- Synonyms
- VOR-IM A;Vortioxetine Impurity 32;(2,4-diMethylphenyl)(2-nitrophenyl)sulfane;(2,4-Dimethyiphenyl)(2-Nitrophenyl)Sulfane;2,4-Dimethyl-1-[(2-nitrophenyl)thio]benzene;Benzene, 2,4-dimethyl-1-[(2-nitrophenyl)thio]-;2,4-Dimethyl-1-[(2-nitrophenyl)sulfanyl]benzene
- CBNumber
- CB22730763
- Molecular Formula
- C14H13NO2S
- Formula Weight
- 259.32
- MOL File
- 1610527-49-5.mol
(2,4-diMethylphenyl)(2-nitrophenyl)sulfane Property
- Boiling point:
- 353.9±30.0 °C(Predicted)
- Density
- 1.24±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Light yellow to yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D480865
- Product name
- (2,4-Dimethylphenyl)(2-nitrophenyl)sulfane
- Packaging
- 1g
- Price
- $85
- Updated
- 2021/12/16
- Product number
- 3806EA
- Product name
- (2,4-Dimethylphenyl)(2-nitrophenyl)sulfane
- Packaging
- 25g
- Price
- $169
- Updated
- 2021/12/16
- Product number
- CM249930
- Product name
- (2,4-Dimethylphenyl)(2-nitrophenyl)sulfane
- Purity
- 95+%
- Packaging
- 25g
- Price
- $299
- Updated
- 2021/12/16
- Product number
- CD12136600
- Product name
- (2,4-Dimethylphenyl)(2-nitrophenyl)sulfane
- Purity
- 97%
- Packaging
- 25g
- Price
- $317
- Updated
- 2021/12/16
- Product number
- 1610527495
- Product name
- (2,4-Dimethylphenyl)(2-nitrophenyl)sulfane
- Packaging
- 25g
- Price
- $400
- Updated
- 2021/12/16
(2,4-diMethylphenyl)(2-nitrophenyl)sulfane Chemical Properties,Usage,Production
Uses
(2,4-Dimethylphenyl)(2-nitrophenyl)sulfane is a reacatnat in studying generic industry approach to efficient purification of potential mutagenic impurities in the synthesis of drug substances.
Synthesis
Dissolve 50.00 g (0.36 mol) of 2,4- dimethylbenzenethiol (5) in 300 mL of DMF, add 30.44 g () of potassium hydroxide and stir at room temperature. 0.5425mol) of potassium hydroxide, stir at room temperature, add a total of 56.99 g (0.3617 mol) of o-chloronitrobenzene (6) in 3 batches, and react at 50 . The reaction was carried out at 50 for 5 h. The reaction was monitored by thin-layer chromatography (TLC), and the unfolding reagent was [ ethyl acetate: petroleum ether (AR bp: 60 ~90 )=1:5] . The reaction was monitored by TLC. After the reaction was completed and cooled to room temperature, 900 mL of distilled water was added with thorough stirring, a large amount of solid was precipitated, and the filter cake was filtered and recrystallized with ethanol to obtain 89.10 g of compound 4. Yield 95%, mp: 98.0%. 95%, mp: 98 ~100 , MS: C 14 H 13 NO 2 S [M+Na] + 282.0563 .
(2,4-diMethylphenyl)(2-nitrophenyl)sulfane Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from (2,4-diMethylphenyl)(2-nitrophenyl)sulfane manufacturers
- Product
- (2,4-Dimethylphenyl)(2-nitrophenyl)sulfane 1610527-49-5
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 1
- Release date
- 2025-08-26
- Product
- (2,4-diMethylphenyl)(2-nitrophenyl)sulfane 1610527-49-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2019-12-19