(FMOC-CYS-OH)2
- Product Name
- (FMOC-CYS-OH)2
- CAS No.
- 135273-01-7
- Chemical Name
- (FMOC-CYS-OH)2
- Synonyms
- (FMOC-CYS)2;(FMOC-CYS-OH)2;Fmoc-L-Cystine;(Fmoc-L-Cys-OH)2;N,N'-Bis-FMoc-L-cystine;(Fmoc-Cys-OH)2 (Disulfide bond);N-ALPHA,N-ALPHA-BIS-FMOC-L-CYSTINE;Nα,Nα-Bis-Fmoc-L-cystine(Disulfide bond);((9H-Fluoren-9-yl)MethOxy]Carbonyl Cys-OH)2;N,N'-DI-9-FLUORENYLMETHOXYCARBONYL-L-CYSTINE
- CBNumber
- CB2283906
- Molecular Formula
- C36H32N2O8S2
- Formula Weight
- 684.78
- MOL File
- 135273-01-7.mol
(FMOC-CYS-OH)2 Property
- Boiling point:
- 925.8±65.0 °C(Predicted)
- Density
- 1.412
- Flash point:
- 513.7℃
- storage temp.
- Sealed in dry,2-8°C
- pka
- 3.06±0.10(Predicted)
Safety
- Safety Statements
- 24/25
- HS Code
- 29309090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 264846
- Product name
- N-alpha,N-alpha-Bis-Fmoc-L-cystine
- Packaging
- 1g
- Price
- $373
- Updated
- 2021/12/16
- Product number
- 03909
- Product name
- ,BisFmoc-L-cystine(Disulfide bond)
- Purity
- ≥ 99% (HPLC)
- Packaging
- 1G
- Price
- $25
- Updated
- 2021/12/16
- Product number
- AS88283
- Product name
- N,N'-Bis-Fmoc-L-cystine
- Purity
- 95% ee
- Packaging
- 1g
- Price
- $53
- Updated
- 2021/12/16
- Product number
- FB47873
- Product name
- N-alpha,N-alpha-Bis-Fmoc-L-cystine(Disulfide bond)
- Packaging
- 1g
- Price
- $88.5
- Updated
- 2021/12/16
- Product number
- 03909
- Product name
- ,BisFmoc-L-cystine(Disulfide bond)
- Purity
- ≥ 99% (HPLC)
- Packaging
- 5G
- Price
- $100
- Updated
- 2021/12/16
(FMOC-CYS-OH)2 Chemical Properties,Usage,Production
Chemical Properties
White to off-white powder
Synthesis
56-89-3
28920-43-6
135273-01-7
The general procedure for the synthesis of Fmoc-L-cystine from L-cystine and 9-fluorenylmethyl chloroformate was as follows: sodium carbonate (4.6 g, 43.6 mmol) and L-cystine (5.0 g, 20.8 mmol) were dissolved in deionized water (200 mL). The reaction system was cooled to 10 °C. Methyl 9-fluorenyl chloroformate (Fmoc-Cl, 11.85 g, 45.8 mmol) was dissolved in 1,4-dioxane (80 mL) and this solution was slowly added dropwise to the above aqueous L-cystine solution. The reaction mixture was stirred continuously at 10 °C for 2 h, followed by natural warming to room temperature. Upon completion of the reaction, a thick white precipitate was produced, which was drained through a sintered glass funnel. The resulting solid was washed with ether (50 mL) and ground, followed by drying under vacuum for 48 hours. The final N,N'-bis(Fmoc)-L-cystine (14.0 g, 98% yield) was obtained as a white powdery product.
References
[1] Patent: US2007/37963, 2007, A1. Location in patent: Page/Page column 11-12; Figure 4
(FMOC-CYS-OH)2 Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from (FMOC-CYS-OH)2 manufacturers
- Product
- (Fmoc-Cys-OH)2 135273-01-7
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1T
- Release date
- 2023-11-14