BOC-GLY-GLY-GLY-OH
- Product Name
- BOC-GLY-GLY-GLY-OH
- CAS No.
- 28320-73-2
- Chemical Name
- BOC-GLY-GLY-GLY-OH
- Synonyms
- Boc-Gly-Gly-Gly;Boc-GGG-OH;BOC-(GLY)3-OH;BOC-GLY-GLY-GLY-OH;Tenapanor Impurity 15;N-Boc-glycylglycylglycine;Boc-Glycyl-Glycyl-Glycine;BOC-L-GLYCYL GLYCYL GLYCINE;REF DUPL: Boc-Gly-Gly-Gly-OH;Boc-Gly-Gly-Gly-OH≥ 97.5% (HPLC)
- CBNumber
- CB2318686
- Molecular Formula
- C11H19N3O6
- Formula Weight
- 289.29
- MOL File
- 28320-73-2.mol
BOC-GLY-GLY-GLY-OH Property
- Melting point:
- 205 °C
- Boiling point:
- 641.8±50.0 °C(Predicted)
- Density
- 1.263
- storage temp.
- Sealed in dry,2-8°C
- form
- Solid
- pka
- 3.33±0.10(Predicted)
- color
- White to off-white
Safety
- HS Code
- 2924297099
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B656128
- Product name
- Boc-Gly-Gly-Gly-OH
- Packaging
- 5g
- Price
- $70
- Updated
- 2021/12/16
- Product number
- FB49243
- Product name
- Boc-Gly-Gly-Gly-OH
- Packaging
- 5G
- Price
- $130.3
- Updated
- 2021/12/16
- Product number
- BP-24097
- Product name
- Boc-Gly-Gly-Gly-OH
- Purity
- 97%
- Packaging
- 2g
- Price
- $150
- Updated
- 2021/12/16
- Product number
- AS29064
- Product name
- N-Boc-glycylglycylglycine
- Purity
- 95+%
- Packaging
- 25g
- Price
- $201
- Updated
- 2021/12/16
- Product number
- 094131
- Product name
- Boc-Gly-Gly-Gly
- Purity
- 95+%
- Packaging
- 5g
- Price
- $202
- Updated
- 2021/12/16
BOC-GLY-GLY-GLY-OH Chemical Properties,Usage,Production
Chemical Properties
White to off-white powder
Uses
Boc-Gly-Gly-Gly-OH is used in synthesis method for terlipressin.
Synthesis
556-33-2
24424-99-5
28320-73-2
GENERAL METHOD: Glycyl-glycyl-glycine (1 mmol) was slowly added to a solution of ethanol (1 mL) containing guanidine hydrochloride (15 mmol) and di-tert-butyl dicarbonate (2.5-3 mmol) under stirring conditions, and the reaction temperature was maintained at 35-40°C. The reaction mixture was stirred continuously until a clarified solution was formed. Subsequently, the ethanol was removed by evaporation under vacuum. The residue was washed sequentially with distilled water (2 mL) and hexane or petroleum ether (2 mL) to obtain almost pure Boc-glycine-glycine-glycine. The crude product can be recrystallized if further improvement of product purity is required.
References
[1] European Journal of Organic Chemistry, 2017, vol. 2017, # 41, p. 6209 - 6227
[2] Carbohydrate Research, 2006, vol. 341, # 10, p. 1657 - 1668
[3] Tetrahedron Letters, 2011, vol. 52, # 12, p. 1260 - 1264
[4] Organic and Biomolecular Chemistry, 2006, vol. 4, # 19, p. 3626 - 3638
[5] Tetrahedron Letters, 2000, vol. 41, # 18, p. 3433 - 3436
BOC-GLY-GLY-GLY-OH Preparation Products And Raw materials
Raw materials
Preparation Products
BOC-GLY-GLY-GLY-OH Suppliers
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View Lastest Price from BOC-GLY-GLY-GLY-OH manufacturers
- Product
- BOC-GLY-GLY-GLY-OH 28320-73-2
- Price
- US $2.00-5.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2025-06-27
- Product
- Boc-Gly-Gly-Gly 28320-73-2
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1T+
- Release date
- 2024-01-17
- Product
- Boc-Gly-Gly-Gly-OH 28320-73-2
- Price
- US $0.00/g
- Min. Order
- 25g
- Purity
- >95.00%
- Supply Ability
- 25g
- Release date
- 2024-04-01