[6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid

Product Name: [6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid
CAS No.: 446299-81-6
Chemical Name: [6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid
Synonyms: Ozenoxacin Impurity 7;Ozenoxacin Impurity 15;5-Methyl-6-(phenacylamino)pyridin-3-yl]boronic acid;(5-methyl-6-(N-methylbenzamido)pyridin-3-yl)boronic acid;[6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid;[6- [benzoyl (methyl) amino] -5-methyl-3-pyridinyl] boric acid;Boronic acid, [6-(benzoylmethylamino)-5-methyl-3-pyridinyl]- (9CI);(S) - 6-chloro-3,4-dihydro-2h-thieno [3,2-e] - 1,2-thiazine-4-alcohol 1,1-dioxide;（ethyl 7-chloro-8-methyl-4-oxo-1,4-dihydroquinoline-3-carboxylate），[6-[benzoyl(methyl)amino]-5-methyl-3- pyridyl]boronic acid
CBNumber: CB23370678
Molecular Formula: C14H15BN2O3
Formula Weight: 270.09
MOL File: 446299-81-6.mol

More

Less

[6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid Property

Boiling point:: 513.7±60.0 °C(Predicted)
Density: 1.27±0.1 g/cm3(Predicted)
vapor pressure: 0Pa at 25℃
pka: 4.12±0.18(Predicted)
form: Solid:particulate/powder
LogP: 2.87

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H317May cause an allergic skin reaction

H411Toxic to aquatic life with long lasting effects

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P272Contaminated work clothing should not be allowed out of the workplace.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P321Specific treatment (see … on this label).

P333+P313IF SKIN irritation or rash occurs: Get medical advice/attention.

P363Wash contaminated clothing before reuse.

P501Dispose of contents/container to..…

More

Less

[6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid Chemical Properties,Usage,Production

Uses

[6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.

Synthesis

Under a nitrogen atmosphere, N-(5-bromo-3-methyl-2-pyridinyl)-N-methylbenzamide 30.0 g was dissolved in 150 mL of tetrahydrofuran, triisopropyl borate 22.0 g was added. The reaction mixture was colled to-60 .DEGREE CELSIUS., n-butyl lithium (1.56 mol/L n-hexane solution) 69 mL was added dropwise required to between 20 minutes, and the mixture was stirred for 15 minutes at the same temperature.After raising the temperature of the reaction mixture at-20 .DEGREE CELSIUS., 390 mL of water was added dropwise, it was stirred for 30 min at room temperature,the aqueous layer was separated. The aqueous layer was fractionated and HCl 1 mol/L was added to adjust the pH at 4.5,the precipitate was collected by filtration, 6-[benzoyl(methyl)amino]-5-methyl-3-pyridinylboric acid 18.5 g was obtained as colorless solid.

[6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

[6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid Suppliers

China 64 India 1 Global 65

Chemipanda Bio-Tech Co., Ltd.

Tel: +86-571-85224801; 13588483690
Fax: 0571-85241599
Email: chemipanda2010@163.com
Country: China
ProdList: 107
Advantage: 62

Jinan Chenghui Shuangda biological Co., LTD

Tel: 0531-58897003 15550412551
Fax: 0531-58897003
Email: market@jnchsd.com
Country: China
ProdList: 210
Advantage: 62

Wuhan DKY Technology Co.,Ltd.

Tel: 27-81302488 18007166089
Fax: 027-81302088
Email: info@dkybpc.com
Country: China
ProdList: 2024
Advantage: 58

ChemStrong Scientific Co.,Ltd

Tel: 0755-0755-66853366 13670046396
Fax: 0755-28363542
Email: sales@chem-strong.com
Country: China
ProdList: 17982
Advantage: 56

Shanghai Kewel Chemical Co., Ltd.

Tel: 021-64609169 18901607656
Fax: 021-64609160
Email: greensnown@163.com
Country: China
ProdList: 9911
Advantage: 50

Watson Biotechnology Co.,Ltd

Tel: 027-027-59207879 18140587686
Fax: QQ：1972026995
Email: kf@3600chem.com
Country: China
ProdList: 4699
Advantage: 55

Shanghai Synchem Pharma Co., ltd

Tel: 021-61984905-1 18016477331
Email: synchempharma@aliyun.com
Country: China
ProdList: 6454
Advantage: 55

CHENGHUI PHARMACEUTICAL GROUP LTD

Tel: 0531-58897070 15254140813
Fax: 0531-58897046
Email: market@jnchsd.com
Country: China
ProdList: 210
Advantage: 58

Aikon International Limited

Tel: 025-66028182 18112977050
Fax: (3)02557626880
Email: cfzhang@aikonchem.com
Country: China
ProdList: 15820
Advantage: 58

Jinan Chenghui Shuangda Chemical Co., Ltd.

Tel: 0531-58897066 13605407322
Fax: 0531-58897093
Email: shenyun@jnchsd.com
Country: China
ProdList: 202
Advantage: 58

More

Less

View Lastest Price from [6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid manufacturers

PNP Biotech Co. Ltd

Product: [6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid 446299-81-6
Price: US $0.00/kg
Min. Order: 25kg
Purity: 98%
Supply Ability: Inquiry
Release date: 2022-10-21

Hebei Xinsheng New Material Technology Co., LTD.

Product: [6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid 446299-81-6
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 99.9%
Supply Ability: 20 tons
Release date: 2023-09-15

Hebei Xinsheng New Material Technology Co., LTD.

Product: [6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid 446299-81-6
Price: US $35.00-25.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 20 Ton
Release date: 2023-10-16

446299-81-6, [6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acidRelated Search:

5-broMo-N,3-diMethylpyridin-2-aMine N,3-diMethyl-5-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-aMine 2-Chloro-3-methyl-5-bromopyridine Ozenoxacin intermediate 7-Chloro-1-cyclopropyl-1,4-dihydro-8-Methyl-4-oxo-3-quinolinecarboxylic Acid Benzamide, N-methyl-N-(3-methyl-2-pyridinyl)-

(5-methyl-6-(N-methylbenzamido)pyridin-3-yl)boronic acid

[6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid

5-Methyl-6-(phenacylamino)pyridin-3-yl]boronic acid

Boronic acid, [6-(benzoylmethylamino)-5-methyl-3-pyridinyl]- (9CI)

[6- [benzoyl (methyl) amino] -5-methyl-3-pyridinyl] boric acid

（ethyl 7-chloro-8-methyl-4-oxo-1,4-dihydroquinoline-3-carboxylate），[6-[benzoyl(methyl)amino]-5-methyl-3- pyridyl]boronic acid

(S) - 6-chloro-3,4-dihydro-2h-thieno [3,2-e] - 1,2-thiazine-4-alcohol 1,1-dioxide

Ozenoxacin Impurity 7

Ozenoxacin Impurity 15

446299-81-6

C14H15BN2O3

446299-81-6