3-AMINO-2-CYCLOHEXEN-1-ONE
- Product Name
- 3-AMINO-2-CYCLOHEXEN-1-ONE
- CAS No.
- 5220-49-5
- Chemical Name
- 3-AMINO-2-CYCLOHEXEN-1-ONE
- Synonyms
- 3-AMINOCYCLOHEX-2-EN-1-ONE;3-AMINO-CYCLOHEX-2-ENONE;AKOS 91521;Cartier impurity 10;3-aminocyclohexenone;Carteolol Impurity 25;3-Amino-2-cyclohexenone;1-Aminocyclohexene-3-one;1-Amino-1-cydohexene-3-one;3-AMINO-2-CYCLOHEXEN-1-ONE
- CBNumber
- CB2342890
- Molecular Formula
- C6H9NO
- Formula Weight
- 111.14
- MOL File
- 5220-49-5.mol
3-AMINO-2-CYCLOHEXEN-1-ONE Property
- Melting point:
- 129-133 °C (lit.)
- Boiling point:
- 212.4±30.0 °C(Predicted)
- Density
- 1.091±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Store in freezer, under -20°C
- solubility
- soluble in Methanol
- form
- powder to crystal
- pka
- 5.65±0.20(Predicted)
- color
- Light yellow to Brown to Dark green
- BRN
- 471354
- InChI
- InChI=1S/C6H9NO/c7-5-2-1-3-6(8)4-5/h4H,1-3,7H2
- InChIKey
- ZZMRPOAHZITKBV-UHFFFAOYSA-N
- SMILES
- C1(=O)CCCC(N)=C1
- CAS DataBase Reference
- 5220-49-5(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- 239372
- Product name
- 3-Amino-2-cyclohexen-1-one
- Purity
- 99%
- Packaging
- 5g
- Price
- $53.4
- Updated
- 2023/06/20
- Product number
- 239372
- Product name
- 3-Amino-2-cyclohexen-1-one
- Purity
- 99%
- Packaging
- 25g
- Price
- $157
- Updated
- 2023/06/20
- Product number
- A1936
- Product name
- 3-Amino-2-cyclohexen-1-one
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $45
- Updated
- 2025/07/31
- Product number
- A1936
- Product name
- 3-Amino-2-cyclohexen-1-one
- Purity
- >98.0%(GC)
- Packaging
- 25g
- Price
- $134
- Updated
- 2025/07/31
- Product number
- A634540
- Product name
- 1-Amino-3-oxo-1-cyclohexene
- Packaging
- 5g
- Price
- $50
- Updated
- 2021/12/16
3-AMINO-2-CYCLOHEXEN-1-ONE Chemical Properties,Usage,Production
Chemical Properties
Dark yellow crystal
Uses
3-Amino-2-cyclohexen-1-one was used in the synthesis of a series of 2-amino-5-oxo-4-phenyl-5,6,7,8-tetrahydroquinoline-3-carbonitriles.
Synthesis
504-02-9
5220-49-5
General procedure for the synthesis of 3-amino-2-cyclohexen-1-one from 1,3-cyclohexanedione: 1,3-cyclohexanedione (0.03 mol) and ammonium acetate (0.039 mol) were added to a 100 mL three-necked flask, and the mixture was thoroughly stirred. The mixture was placed in an oil bath at 110°C for 15 min of reaction. Upon completion of the reaction, the oil bath was removed and the reaction system was allowed to cool naturally, at which time the reaction solution gradually solidified. After cooling to room temperature, ethyl acetate (10 mL) was added to the reaction mixture and heated to dissolve the solid, which was subsequently cooled to 0°C to promote crystallization. The precipitated solid was collected by filtration and dried to give yellow crystals of 3-amino-2-cyclohexen-1-one in 93.6% yield.
References
[1] New Journal of Chemistry, 2005, vol. 29, # 6, p. 769 - 772
[2] Patent: CN107337639, 2017, A. Location in patent: Paragraph 0120; 0123; 0135; 0144-0146; 0157; 0168; 0179
[3] Synlett, 2009, # 5, p. 818 - 822
[4] Synthetic Communications, 1998, vol. 28, # 7, p. 1197 - 1200
[5] Tetrahedron, 2003, vol. 59, # 43, p. 8589 - 8595
3-AMINO-2-CYCLOHEXEN-1-ONE Preparation Products And Raw materials
Raw materials
Preparation Products
3-AMINO-2-CYCLOHEXEN-1-ONE Suppliers
- Tel
- 03-36680489
- Fax
- 03-3668-0520
- Sales-JP@TCIchemicals.com
- Country
- Japan
- ProdList
- 28387
- Advantage
- 80
- Tel
- --
- Fax
- --
- labchem-tec@wako-chem.co.jp
- Country
- Japan
- ProdList
- 6819
- Advantage
- 80
View Lastest Price from 3-AMINO-2-CYCLOHEXEN-1-ONE manufacturers
- Product
- 3-Aminocyclohex-2-en-1-one 5220-49-5
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-09-29
- Product
- 3-Aminocyclohex-2-enone 5220-49-5
- Price
- US $590.00/Kg
- Min. Order
- 1Kg
- Purity
- 98
- Supply Ability
- 500 Kg
- Release date
- 2024-04-11
- Product
- 3-aminocyclohex-2-enone 5220-49-5
- Price
- US $0.00-0.00/KG
- Min. Order
- 1g
- Purity
- 98%min
- Supply Ability
- 100kgs/month
- Release date
- 2021-11-22