ChemicalBook > CAS DataBase List > 2-CHLORO-5-NITROBENZENESULFONAMIDE

2-CHLORO-5-NITROBENZENESULFONAMIDE

Product Name
2-CHLORO-5-NITROBENZENESULFONAMIDE
CAS No.
96-72-0
Chemical Name
2-CHLORO-5-NITROBENZENESULFONAMIDE
Synonyms
NSC 105711;2-CHLORO-5-NITROBENZ;2-CHLORO-5-NITROBENZENESULFONAMIDE;4-NITROCHLOROBENZENE-2-SULFONAMIDE;2-chloro-5-nitrobenzenesulphonamide;2-chloro-5-nitrobenzene-1-sulfonaMid;2-chloro-5-nitrobenzene-1-sulfonaMide;Benzenesulfonamide, 2-chloro-5-nitro-;2-CHLORO-5-NITROBENZENESULFONAMIDE 98%;2,5-bis(1-naphthalenyl)-1,3,4-oxadiazole
CBNumber
CB2346287
Molecular Formula
C6H5ClN2O4S
Formula Weight
236.63
MOL File
96-72-0.mol
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2-CHLORO-5-NITROBENZENESULFONAMIDE Property

Melting point:
180-183°C
storage temp. 
Sealed in dry,Room Temperature
solubility 
Dichloromethane, Ethyl Acetate, Methanol
form 
Solid
color 
White
InChIKey
ZAJALNCZCSSGJC-UHFFFAOYSA-N
CAS DataBase Reference
96-72-0(CAS DataBase Reference)
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H317May cause an allergic skin reaction

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
S371319
Product name
2-CHLORO-5-NITROBENZENESULFONAMIDE
Purity
Aldrich<sup>CPR</sup>
Packaging
1 unit
Price
$113
Updated
2025/07/31
Sigma-Aldrich
Product number
S371319
Product name
2-CHLORO-5-NITROBENZENESULFONAMIDE
Purity
Aldrich
Packaging
250mg
Price
$110
Updated
2024/03/01
TRC
Product number
C373880
Product name
2-Chloro-5-nitrobenzenesulfonamide
Packaging
100mg
Price
$70
Updated
2021/12/16
TRC
Product number
C373880
Product name
2-Chloro-5-nitrobenzenesulfonamide
Packaging
500mg
Price
$185
Updated
2021/12/16
AK Scientific
Product number
J51399
Product name
2-Chloro-5-nitrobenzenesulfonamide
Packaging
10g
Price
$49
Updated
2021/12/16
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2-CHLORO-5-NITROBENZENESULFONAMIDE Chemical Properties,Usage,Production

Chemical Properties

White Solid

Uses

2-Chloro-5-nitrobenzenesulfonamide (cas# 96-72-0) is a compound useful in organic synthesis.

Synthesis

4533-95-3

96-72-0

Example 17A-1 Synthesis of 2-chloro-5-nitrobenzenesulfonamide: 2-chloro-5-nitrobenzenesulfonic acid (104 g, 437.6 mmol) was dissolved in thionyl chloride (240 mL), followed by the addition of N,N-dimethylformamide (2 mL) as a catalyst. The reaction mixture was heated to reflux and maintained for 4 hours to complete the reaction. Upon completion of the reaction, the mixture was carefully poured into water for quenching and the product was subsequently isolated by filtration. The resulting 2-chloro-5-nitrobenzenesulfonyl chloride was dissolved in toluene and slowly added to a pre-mixed solution of NH4OH (520 mL) and tetrahydrofuran (520 mL) at -10 °C. The reaction mixture was stirred at this temperature for 1 h. The reaction was quenched with 6 M hydrochloric acid solution and the final pH was adjusted to 4. After separating the aqueous and organic layers, the organic layer was concentrated to dryness to give a powdery product. To this powdered product pentane was added and the target compound was isolated by filtration and dried to give 2-chloro-5-nitrobenzenesulfonamide (82.6 g, 80% yield).

References

[1] European Journal of Medicinal Chemistry, 2012, vol. 50, p. 18 - 26
[2] Patent: US2011/152246, 2011, A1. Location in patent: Page/Page column 293
[3] Patent: US2005/107364, 2005, A1. Location in patent: Page/Page column 75
[4] Patent: WO2005/19191, 2005, A2. Location in patent: Page/Page column 151
[5] Journal of Pharmacy and Pharmacology, 2001, vol. 53, # 5, p. 669 - 680

2-CHLORO-5-NITROBENZENESULFONAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-CHLORO-5-NITROBENZENESULFONAMIDE Suppliers

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View Lastest Price from 2-CHLORO-5-NITROBENZENESULFONAMIDE manufacturers

Henan Fengda Chemical Co., Ltd
Product
2-CHLORO-5-NITROBENZENESULFONAMIDE 96-72-0
Price
US $100.00-1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2023-12-26
Shaanxi Dideu Medichem Co. Ltd
Product
2-Chloro-5-nitrobenzenesulfonamide 96-72-0
Price
US $0.00-0.00/Kg
Min. Order
1KG
Purity
99.0%
Supply Ability
100 tons
Release date
2020-01-10
Career Henan Chemical Co
Product
2-CHLORO-5-NITROBENZENESULFONAMIDE 96-72-0
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
1kg-1000kg
Release date
2020-01-02

96-72-0, 2-CHLORO-5-NITROBENZENESULFONAMIDERelated Search:

2-CHLORO-5-NITROBENZENESULFONAMIDE 4-CHLORO-3-NITROBENZENESULFONAMIDE Benzenesulfonamide N-butyl-4-chloro-3-nitrobenzenesulfonamide 1-(2-CHLORO-5-NITRO-BENZENESULFONYL)-PYRROLIDINE 2-CHLORO-N,N-DIETHYL-5-NITRO-BENZENESULFONAMIDE 2-chloro-4-nitrobenzenesulfonamide N-(TERT-BUTYL)-4-CHLORO-3-NITROBENZENESULFONAMIDE 2-chloro-5-nitrobenzene-1-sulfonohydrazide 5-(2-CHLORO-5-NITRO-BENZENESULFONYLAMINO)-2-HYDROXY-BENZOIC ACID 4-(2-CHLORO-5-NITRO-BENZENESULFONYL)-MORPHOLINE 2-CHLORO-N-(4-CHLORO-PHENYL)-5-NITRO-BENZENESULFONAMIDE 2-(2-CHLORO-5-NITRO-BENZENESULFONYLAMINO)-BENZOIC ACID 2-CHLORO-N-(2-CHLORO-PHENYL)-5-NITRO-BENZENESULFONAMIDE 4-(2-CHLORO-5-NITRO-BENZENESULFONYLAMINO)-BENZOIC ACID N-(3-aminopropyl)-2-chloro-5-nitrobenzene-1-sulfonamide 2-CHLORO-N-(2-FLUORO-PHENYL)-5-NITRO-BENZENESULFONAMIDE 2-chloro-N-methyl-5-nitrobenzene-1-sulfonamide

  • NSC 105711
  • 2-CHLORO-5-NITROBENZENESULFONAMIDE
  • 2-chloro-5-nitrobenzenesulphonamide
  • 2-CHLORO-5-NITROBENZENESULFONAMIDE 98%
  • 4-NITROCHLOROBENZENE-2-SULFONAMIDE
  • 2-CHLORO-5-NITROBENZ
  • 2-chloro-5-nitrobenzene-1-sulfonaMide
  • 2-chloro-5-nitrobenzene-1-sulfonaMid
  • 2,5-bis(1-naphthalenyl)-1,3,4-oxadiazole
  • Benzenesulfonamide, 2-chloro-5-nitro-
  • 2-CHLORO-5-NITROBENZENESULFONAMIDE ISO 9001：2015 REACH
  • 96-72-0
  • C6H5N2O4ClS
  • Aromatics
  • Heterocycles
  • Benzene derivates