ChemicalBook > CAS DataBase List > 4-DIETHYLAMINO-2-METHOXY-BENZALDEHYDE

4-DIETHYLAMINO-2-METHOXY-BENZALDEHYDE

Product Name: 4-DIETHYLAMINO-2-METHOXY-BENZALDEHYDE
CAS No.: 55586-68-0
Chemical Name: 4-DIETHYLAMINO-2-METHOXY-BENZALDEHYDE
Synonyms: TIMTEC-BB SBB011177;4-DIETHYLAMINO-2-METHOXY-BENZALDEHYDE;2-Methoxy-4-(diethylamino)benzaldehyde;Benzaldehyde, 4-(diethylamino)-2-methoxy-;4-Diethylamino-2-methoxy-benzaldehyde in stock Factory;5-(Diethylamino)-2-formylanisole, N,N-Diethyl-4-formyl-3-methoxyaniline
CBNumber: CB2350233
Molecular Formula: C12H17NO2
Formula Weight: 207.27
MOL File: 55586-68-0.mol

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4-DIETHYLAMINO-2-METHOXY-BENZALDEHYDE Property

Melting point:: 73-76 °C
Boiling point:: 334.8±27.0 °C(Predicted)
Density: 1.056±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 2.94±0.42(Predicted)
Appearance: Light yellow to brown Solid

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Safety

Hazard Codes: Xi,T
Risk Statements: 25
Safety Statements: 45
HazardClass: IRRITANT
HS Code: 2922390090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: D442130
Product name: 4-Diethylamino-2-methoxy-benzaldehyde
Packaging: 1g
Price: $75
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD70103
Product name: 4-Diethylamino-2-methoxybenzaldehyde
Packaging: 10g
Price: $100
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD70103
Product name: 4-Diethylamino-2-methoxybenzaldehyde
Packaging: 5G
Price: $60
Updated: 2021/12/16

AK Scientific

Product number: A859
Product name: 4-Diethylamino-2-methoxybenzaldehyde
Packaging: 5g
Price: $71
Updated: 2021/12/16

Matrix Scientific

Product number: 010377
Product name: 4-Diethylamino-2-methoxy-benzaldehyde
Packaging: 500mg
Price: $15
Updated: 2021/12/16

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4-DIETHYLAMINO-2-METHOXY-BENZALDEHYDE Chemical Properties,Usage,Production

Synthesis

17754-90-4

74-88-4

55586-68-0

The general procedure for the synthesis of 4-diethylamino-2-methoxy-benzaldehyde from 4-(diethylamino)salicylaldehyde and iodomethane was as follows: 4-diethylamino-2-hydroxybenzaldehyde (5.8 g, 30 mmol), potassium hydroxide (2 g, 35 mmol), and potassium carbonate (8.3 g, 60 mmol) were dissolved in acetonitrile (30 mL), and heated and stirred at 80 °C for for 10 min. Subsequently, iodomethane (3.5 mL, 56 mmol) was slowly added to the reaction system, and the reaction continued to be stirred at 80 °C for 2 hours. After completion of the reaction, the mixture was cooled to room temperature and filtered to remove insoluble impurities. The filtrate was concentrated under reduced pressure and purified by silica gel column chromatography (sieve size 120-200 mesh) with the eluent ethyl acetate/hexane (1:3, v/v) to afford the target product 4-diethylamino-2-methoxy-benzaldehyde as a yellow solid in 85% yield. The structure of the product was confirmed by 1H NMR and 13C NMR: 1H NMR (500 MHz, CDCl3) δ 10.11 (s, 1H), 7.68 (dd, J = 8.9, 2.8 Hz, 1H), 6.26 (d, J = 8.8 Hz, 1H), 6.02 (s, 1H), 3.87 (s, 3H), 3.41 (dd, J = 6.9, 2.7 Hz, 4H), 1.21 (t, J = 5.4 Hz, 6H); 13C NMR (125 MHz, CDCl3) δ 187.1, 164.1, 153.8, 130.7, 114.2, 104.2, 92.4, 55.2, 44.7, 12.5.

References

[1] Journal of Physical Chemistry A, 2004, vol. 108, # 31, p. 6452 - 6454
[2] Dyes and Pigments, 2018, vol. 148, p. 474 - 491
[3] RSC Advances, 2013, vol. 3, # 46, p. 24021 - 24024
[4] Patent: US2017/320846, 2017, A1. Location in patent: Sheet 16

4-DIETHYLAMINO-2-METHOXY-BENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 4-DIETHYLAMINO-2-METHOXY-BENZALDEHYDE manufacturers

Chemwill Asia Co.,Ltd.

Product: 4-Diethylamino-2-methoxy-benzaldehyde in stock Factory 55586-68-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: TOP 3 Factory in China
Supply Ability: Top 3 largest production capacity Factory
Release date: 2019-04-03

55586-68-0, 4-DIETHYLAMINO-2-METHOXY-BENZALDEHYDERelated Search:

Nedocromil 4-DIETHYLAMINO-2-METHOXY-BENZALDEHYDE 2-ETHOXY-4-MORPHOLIN-4-YL-BENZALDEHYDE 2-ETHOXY-4-PYRROLIDIN-1-YL-BENZALDEHYDE 2-METHOXY-4-PIPERIDIN-1-YL-BENZALDEHYDE NEDOCROMIL SODIUM 2-METHOXY-4-PYRROLIDIN-1-YL-BENZALDEHYDE 2-METHOXY-4-MORPHOLIN-4-YL-BENZALDEHYDE 4-DIETHYLAMINO-2-ETHOXY-BENZALDEHYDE 2,5-DIMETHOXY-4-MORPHOLIN-4-YL-BENZALDEHYDE 2-ETHOXY-4-PIPERIDIN-1-YL-BENZALDEHYDE 5-CHLORO-4-(1,3-DIOXO-1,3-DIHYDRO-ISOINDOL-2-YL)-2-METHOXY-BENZOIC ACID 5-chloro-2-methoxy-4-(2-oxopyrrolidin-1-yl)benzoic acid 2,5-DIMETHOXY-4-PYRROLIDIN-1-YL-BENZALDEHYDE 2,5-DIMETHOXY-4-PIPERIDIN-1-YL-BENZALDEHYDE 8-METHOXY-2,3,6,7-TETRAHYDRO-1H,5H-PYRIDO[3,2,1-IJ]QUINOLINE-9-CARBALDEHYDE AURORA KA-3423

4-DIETHYLAMINO-2-METHOXY-BENZALDEHYDE

TIMTEC-BB SBB011177

5-(Diethylamino)-2-formylanisole, N,N-Diethyl-4-formyl-3-methoxyaniline

Benzaldehyde, 4-(diethylamino)-2-methoxy-

2-Methoxy-4-(diethylamino)benzaldehyde

4-Diethylamino-2-methoxy-benzaldehyde in stock Factory

55586-68-0