ChemicalBook > CAS DataBase List > 3-Ethyl-3-oxetanemethanol

3-Ethyl-3-oxetanemethanol

Product Name
3-Ethyl-3-oxetanemethanol
CAS No.
3047-32-3
Chemical Name
3-Ethyl-3-oxetanemethanol
Synonyms
(3-Ethyloxetan-3-yl)Methanol;3-ethyl;3-ETHYL-3-HYDROXYMETHYLOXETANE;EOX;EHMO;EOXA;OXA (oxet;YF-FM EHMO;Monomer-EHMO;Eternacoll EHO
CBNumber
CB2354190
Molecular Formula
C6H12O2
Formula Weight
116.16
MOL File
3047-32-3.mol
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3-Ethyl-3-oxetanemethanol Property

Boiling point:
96 °C/4 mmHg (lit.)
Density 
1.019 g/mL at 25 °C (lit.)
vapor pressure 
3.1Pa at 25℃
refractive index 
n20/D 1.453(lit.)
Flash point:
227 °F
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
form 
Liquid
pka
14.58±0.10(Predicted)
color 
Clear colorless
Water Solubility 
Miscible in water.
InChI
InChI=1S/C6H12O2/c1-2-6(3-7)4-8-5-6/h7H,2-5H2,1H3
InChIKey
UNMJLQGKEDTEKJ-UHFFFAOYSA-N
SMILES
O1CC(CC)(CO)C1
LogP
0.6 at 25℃
CAS DataBase Reference
3047-32-3(CAS DataBase Reference)
EPA Substance Registry System
3-Oxetanemethanol, 3-ethyl- (3047-32-3)
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Safety

Hazard Codes 
Xn
Risk Statements 
36/37/38-22
Safety Statements 
37/39-26-24/25
WGK Germany 
3
TSCA 
Yes
HS Code 
29329990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H319Causes serious eye irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
444197
Product name
3-Ethyl-3-oxetanemethanol
Purity
96%
Packaging
10g
Price
$79.3
Updated
2024/03/01
TCI Chemical
Product number
E0546
Product name
3-Ethyl-3-oxetanemethanol
Purity
>96.0%(GC)
Packaging
25g
Price
$36
Updated
2024/03/01
TCI Chemical
Product number
E0546
Product name
3-Ethyl-3-oxetanemethanol
Purity
>96.0%(GC)
Packaging
100g
Price
$106
Updated
2024/03/01
Alfa Aesar
Product number
H53497
Product name
3-Ethyl-3-oxetanemethanol, 97%
Packaging
5g
Price
$56.4
Updated
2023/06/20
Alfa Aesar
Product number
H53497
Product name
3-Ethyl-3-oxetanemethanol, 97%
Packaging
25g
Price
$216
Updated
2023/06/20
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3-Ethyl-3-oxetanemethanol Chemical Properties,Usage,Production

Chemical Properties

clear colorless liquid

Uses

3-Ethyl-3-oxetanemethanol is used as pharmaceutical intermediate.

Application

Poly(3-ethyl-3-oxetanemethanol) could be used as a core to synthesize amphiphilic hyperbranched polyethers (AHPs), which have multiple linear poly-(ethylene glycol) arms. The AHPs owned good dispersion performance for coating pigment particles. Among AHP's products, AHP47 with 0.47 DB had good potential in coating applications. can also be used to synthesize azobenzene-focused hyperbranched poly(3- ethyl-3-oxetanemethanol)[1-2].

Synthesis Reference(s)

Journal of the American Chemical Society, 79, p. 3455, 1957 DOI: 10.1021/ja01570a038

Synthesis

3-Ethyl-3-oxetanemethanol was prepared by a modified procedure described in the literature. A mixture of trimethylopropane (1, 26.8 g, 0.2 mol), diethyl carbonate (23.6 g, 0.2 mol) and potassium hydroxide (0.1 g, 1.8 mmol) in 2 ml absolute ethyl alcohol was refluxed in oil bath at 110?C for 1 h. Then, the mixture was distilled at 110?C for 1 h. Distillation was continued until the temperature of oil bath reached 140?C. After the distillation, the vacuum was supplied for 1 h to remove the excess solvent. On heating above 185?C, the distilled materials were collected in a cold trap under vacuum and obtained >85% of the theoretical yield. 1H-NMR (CDCl3, δ, ppm): 0.80–0.83 (t, 3H, –CH2CH3), 1.61–1.66 (q, 2H, –CH2CH3), 3.62 (s, 2H, –CH2OH), 3.66 (s, 1H, –CH2OH), 4.31–4.32 and 4.38–4.39 (d, 4H, –CH2O).

References

[1] Q. Xu. “Synthesis and properties of amphiphilic hyperbranched polyethers as pigment dispersant.” IOP Conference Series: Materials Science and Engineering 216 1 (2018).
[2] Xu, Youqian et al. “Hierarchical self-assembly of protoporphyrin IX-bridged Janus particles into photoresponsive vesicles?.” RSC Advances 37 (2016): 31053–31058.

3-Ethyl-3-oxetanemethanol Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Ethyl-3-oxetanemethanol Suppliers

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View Lastest Price from 3-Ethyl-3-oxetanemethanol manufacturers

Hebei Zhuanglai Chemical Trading Co.,Ltd
Product
3-Ethyl-3-oxetanemethanol 3047-32-3
Price
US $60.00/KG
Min. Order
1KG
Purity
99
Supply Ability
5000
Release date
2024-05-07
Hebei Weibang Biotechnology Co., Ltd
Product
3-ETHYL-3-OXETANEMETHANOL 3047-32-3
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20 mt
Release date
2024-11-26
Hebei Chuanghai Biotechnology Co,.LTD
Product
3-ETHYL-3-OXETANEMETHANOL 3047-32-3
Price
US $5.60/KG
Min. Order
1KG
Purity
99%
Supply Ability
5000kg
Release date
2024-08-21

3047-32-3, 3-Ethyl-3-oxetanemethanol Related Search:

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  • Oxetanes
  • Simple 4-Membered Ring Compounds
  • ALCOHOL
  • Organic Building Blocks
  • Oxygen Compounds
  • Building Blocks
  • Alcohols
  • C2 to C6
  • Asymmetric Synthesis
  • Building Blocks
  • C2 to C6
  • Chemical Synthesis
  • Chiral Building Blocks
  • Heterocyclic Building Blocks
  • Organic Building Blocks
  • Oxygen Compounds
  • Oxetanes
  • Simple 4-Membered Ring Compounds
  • Alcohols
  • C2 to C6
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