ChemicalBook > CAS DataBase List > (4-CHLORO-BENZOYLAMINO)-ACETIC ACID

(4-CHLORO-BENZOYLAMINO)-ACETIC ACID

Product Name: (4-CHLORO-BENZOYLAMINO)-ACETIC ACID
CAS No.: 13450-77-6
Chemical Name: (4-CHLORO-BENZOYLAMINO)-ACETIC ACID
Synonyms: IFLAB-BB F0345-3965;p-chloro-hippuricaci;4-chlorohippuricacid;OTAVA-BB BB7210742318;4-chlorobenzoylglycine;p-chlorobenzoylglycine;n-(p-chlorobenzoyl)glycine;n-(4-chlorobenzoyl)glycine;n-(4-chlorobenzoyl)-glycin;Glycine, N-(4-chlorobenzoyl)-
CBNumber: CB2390831
Molecular Formula: C9H8ClNO3
Formula Weight: 213.62
MOL File: 13450-77-6.mol

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(4-CHLORO-BENZOYLAMINO)-ACETIC ACID Property

Melting point:: 144-146°
Boiling point:: 457.2±30.0 °C(Predicted)
Density: 1.397±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
solubility: Dichloromethane (Slightly, Heated), Methanol (Slightly)
form: Solid
pka: 3.43±0.10(Predicted)
color: White to Off-White

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Safety

HazardClass: IRRITANT

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: C367420
Product name: 4-ChlorohippuricAcid
Packaging: 10g
Price: $1390
Updated: 2021/12/16

Matrix Scientific

Product number: 044056
Product name: 2-[(4-Chlorobenzoyl)amino]acetic acid
Purity: >95%
Packaging: 500mg
Price: $118
Updated: 2021/12/16

Matrix Scientific

Product number: 044056
Product name: 2-[(4-Chlorobenzoyl)amino]acetic acid
Purity: >95%
Packaging: 1g
Price: $151
Updated: 2021/12/16

Matrix Scientific

Product number: 044056
Product name: 2-[(4-Chlorobenzoyl)amino]acetic acid
Purity: >95%
Packaging: 5g
Price: $346
Updated: 2021/12/16

Activate Scientific

Product number: AS116901
Product name: 2-(4-Chlorobenzamido)aceticacid
Purity: 97+%
Packaging: 5G
Price: $465
Updated: 2021/12/16

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(4-CHLORO-BENZOYLAMINO)-ACETIC ACID Chemical Properties,Usage,Production

Uses

4-Chlorohippuric Acid is a derivative of Hippuric Acid (H356700) and is the major metabolite in human urine.

Synthesis

59893-99-1

13450-77-6

In a 500 mL round bottom flask, methyl 2-(4-chlorobenzoylamino)acetate (20 g, 88.1 mmol) was dissolved in a solvent mixture of THF (100 mL), methanol (100 mL) and water (100 mL) and lithium hydroxide monohydrate (18.5 g, 441 mmol) was added with stirring. The reaction mixture was stirred continuously for 12 hours at room temperature. After the completion of the reaction was monitored by TLC, the reaction mixture was concentrated under reduced pressure. The resulting residue was washed with EtOAc, subsequently diluted with cold water and acidified with 1N HCl solution to pH about 5. The solid product was collected by filtration and dried under reduced pressure to afford the target compound 2-(4-chlorobenzoylamino)acetic acid (14.21 g, 75.6% yield). The product was characterized by the following data: 1H NMR (300 MHz, DMSO-d6): δ 12.7 (brs, 1H), 8.93 (t, J = 5.7 Hz, 1H), 7.88-7.84 (m, 2H), 7.54 (d, J = 8.7 Hz, 2H), 3.90 (d, J = 6.3 Hz, 2H). lCMS (ESI+, m/ z): 214.0, 216.0 (M + H)+.

References

[1] Patent: WO2017/180818, 2017, A1. Location in patent: Page/Page column 45

(4-CHLORO-BENZOYLAMINO)-ACETIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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(4-CHLORO-BENZOYLAMINO)-ACETIC ACID Suppliers

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13450-77-6, (4-CHLORO-BENZOYLAMINO)-ACETIC ACIDRelated Search:

METHYL 3-ANILINO-2-[(2,4-DICHLOROBENZOYL)AMINO]ACRYLATE (4-CHLORO-BENZOYLAMINO)-ACETIC ACID 2-(4-CHLORO-BENZOYLAMINO)-PROPIONIC ACID 4-CHLORO-N-(2,5-DIOXO-5,6,7,8-TETRAHYDRO-2H-CHROMEN-3-YL)BENZENECARBOXAMIDE ETHYL 2-[(4-CHLOROBENZOYL)AMINO]ACETATE 4-CHLOROBENZOYL-L-TRYPTOPHAN CALCIUM SALT (3-CHLORO-BENZOYLAMINO)-ACETIC ACID ETHYL 3-[(4-CHLOROBENZOYL)AMINO]-2-OXO-6-PHENYL-2H-PYRAN-5-CARBOXYLATE 2,4-DICHLORO-N-(1,3-DIMETHYL-2,4,7-TRIOXO-1,3,4,7-TETRAHYDRO-2H-PYRANO[2,3-D]PYRIMIDIN-6-YL)BENZENECARBOXAMIDE METHYL 2-[(2,4-DICHLOROBENZOYL)AMINO]-3-(4-METHOXYANILINO)ACRYLATE BENZOTRIPT N-(5-ACETYL-6-METHYL-2-OXO-2H-PYRAN-3-YL)-4-CHLOROBENZENECARBOXAMIDE METHYL 2-[(2,4-DICHLOROBENZOYL)AMINO]-3-(METHOXYIMINO)PROPANOATE 2,4-DICHLORO-N-(7-HYDROXY-2-OXO-2H-CHROMEN-3-YL)BENZENECARBOXAMIDE N-(5-BENZOYL-6-METHYL-2-OXO-2H-PYRAN-3-YL)-4-CHLOROBENZENECARBOXAMIDE METHYL 3-[(4-CHLOROBENZOYL)AMINO]-6-METHYL-2-OXO-2H-PYRAN-5-CARBOXYLATE METHYL 3-(2,4-DICHLOROANILINO)-2-[(2,4-DICHLOROBENZOYL)AMINO]ACRYLATE METHYL 2-[(2,4-DICHLOROBENZOYL)AMINO]-3-([(2,4-DICHLOROBENZYL)OXY]IMINO)PROPANOATE

OTAVA-BB BB7210742318

4-chlorobenzoylglycine

4-chlorohippuricacid

n-(4-chlorobenzoyl)-glycin

n-(4-chlorobenzoyl)glycine

n-(p-chlorobenzoyl)glycine

p-chlorobenzoylglycine

p-chloro-hippuricaci

IFLAB-BB F0345-3965

(4-CHLORO-BENZOYLAMINO)-ACETIC ACID

2-[(4-CHLOROBENZOYL)AMINO]ACETIC ACID

N-(4-CHLOROBENZOYL)AMINOACETIC ACID

2-(4-ChlorobenzaMido)acetic acid

[(4-chlorophenyl)formamido]acetic acid

Glycine, N-(4-chlorobenzoyl)-

13450-77-6