2-(BROMOACETYL)PYRIDINE HYDROBROMIDE
- Product Name
- 2-(BROMOACETYL)PYRIDINE HYDROBROMIDE
- CAS No.
- 17570-98-8
- Chemical Name
- 2-(BROMOACETYL)PYRIDINE HYDROBROMIDE
- Synonyms
- BUTTPARK 32\08-51;TIMTEC-BB SBB005581;2-(BROMOACETYL)PYRIDINE HBR;2-(Bromoacetyl)pyrdine hydrobromide;2-(BROMOACETYL)PYRIDINE HYDROBROMIDE;2-Bromo-1-(2-pyridinyl)-1-ethanone*HBr;2-(2-BROMOACETYL)PYRIDINE HYDROBROMIDE;2-(Bromoacetyl)pyridine hydrobromide ,97%;Bromomethyl 2-pyridyl ketone hydrobromide;2-Bromo-1-(2-pyridinyl)ethanone hydrobromide
- CBNumber
- CB2396888
- Molecular Formula
- C7H7Br2NO
- Formula Weight
- 280.94
- MOL File
- 17570-98-8.mol
2-(BROMOACETYL)PYRIDINE HYDROBROMIDE Property
- Melting point:
- 205 °C
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- powder
- color
- light brown
- InChI
- InChI=1S/C7H6BrNO.BrH/c8-5-7(10)6-3-1-2-4-9-6;/h1-4H,5H2;1H
- InChIKey
- BYKVUGZUYJUSKD-UHFFFAOYSA-N
- SMILES
- C1(N=CC=CC=1)C(=O)CBr.Br
- CAS DataBase Reference
- 17570-98-8(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi,Xn
- Risk Statements
- 36/37/38-36-22
- Safety Statements
- 26-36/37/39
- Hazard Note
- Irritant
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B679373
- Product name
- 2-(Bromoacetyl)pyridinehydrobromide
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- OR1299
- Product name
- 2-(Bromoacetyl)pyridinehydrobromide
- Purity
- 98%
- Packaging
- 1g
- Price
- $27
- Updated
- 2021/12/16
- Product number
- FB32828
- Product name
- 2-(Bromoacetyl)pyridine hydrobromide
- Packaging
- 1g
- Price
- $63
- Updated
- 2021/12/16
- Product number
- 081085
- Product name
- 2-Bromo-1-(2-pyridinyl)-1-ethanone hydrobromide
- Purity
- 95%
- Packaging
- 5g
- Price
- $65
- Updated
- 2021/12/16
- Product number
- OR1299
- Product name
- 2-(Bromoacetyl)pyridinehydrobromide
- Purity
- 98%
- Packaging
- 5g
- Price
- $76
- Updated
- 2021/12/16
2-(BROMOACETYL)PYRIDINE HYDROBROMIDE Chemical Properties,Usage,Production
Synthesis
1122-62-9
17570-98-8
The general procedure for the synthesis of 2-bromo-1-(2-pyridyl)-1-acetone hydrobromide from 2-acetylpyridine was as follows: bromine (1.52 mL, 9.72 mmol) was slowly added dropwise to a 30% hydrobromide/acetic acid (12 mL) solution containing 2-acetylpyridine (3 g, 24.8 mmol) at 15 °C. After the dropwise addition was completed, the reaction mixture was warmed to 40 °C and kept stirring for 1 h. Subsequently, it was continued to be warmed to 75 °C and stirred for 1 h. The reaction mixture was then heated up to 40 °C and kept stirring for 1 h. Upon completion of the reaction, the reaction solution was cooled to 20 °C, ether (30 mL) was added and stirred at this temperature for 30 minutes. The resulting yellow precipitate was collected by filtration, and the precipitate was washed with ether (10 mL) and dried to afford the target product 2-bromo-1-(2-pyridyl)-1-acetone hydrobromide (6.81 g, 97.8% yield).
References
[1] Patent: CN105524056, 2016, A. Location in patent: Paragraph 0048; 0049; 0050
[2] Patent: WO2008/4117, 2008, A1. Location in patent: Page/Page column 85
[3] PLoS ONE, 2016, vol. 11, # 5,
[4] Patent: WO2017/17631, 2017, A2. Location in patent: Paragraph 00330
[5] Journal of Medicinal Chemistry, 2010, vol. 53, # 2, p. 787 - 797
2-(BROMOACETYL)PYRIDINE HYDROBROMIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-(BROMOACETYL)PYRIDINE HYDROBROMIDE manufacturers
- Product
- 2-(BROMOACETYL)PYRIDINE HYDROBROMIDE 17570-98-8
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-10-28
- Product
- 2-(BROMOACETYL)PYRIDINE HYDROBROMIDE 17570-98-8
- Price
- US $1.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 100KG
- Release date
- 2018-12-22