4,4-DIMETHYL-2-OXAZOLIDINONE
- Product Name
- 4,4-DIMETHYL-2-OXAZOLIDINONE
- CAS No.
- 26654-39-7
- Chemical Name
- 4,4-DIMETHYL-2-OXAZOLIDINONE
- Synonyms
- DMO;DMRTA1;4-Dimethyl-2-oxazolidon;4,4-Dimethyloxazolidinone;4,4-DIMETHYL-2-OXAZOLIDINONE;4,4-dimethyl-oxazolidin-2...;4,4-diMethyl-oxazolidin-2-one;2-Oxazolidinone,4,4-dimethyl-;4,4-dimethyl-oxazolidine-2-one;4,4-Dimethyl-1,3-oxazolidin-2-one
- CBNumber
- CB2436935
- Molecular Formula
- C5H9NO2
- Formula Weight
- 115.13
- MOL File
- 26654-39-7.mol
4,4-DIMETHYL-2-OXAZOLIDINONE Property
- Melting point:
- 55-56 °C(Solv: ethanol (64-17-5); ligroine (8032-32-4))
- Boiling point:
- 152-154 °C(Press: 10 Torr)
- Density
- 1.039±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- solid
- pka
- 12.91±0.40(Predicted)
- color
- White to off-white
- EPA Substance Registry System
- 2-Oxazolidinone, 4,4-dimethyl- (26654-39-7)
Safety
- WGK Germany
- 3
- HS Code
- 2934999090
N-Bromosuccinimide Price
- Product number
- CBR01583
- Product name
- 4,4-Dimethyl-1,3-oxazolidin-2-one
- Purity
- Aldrich
- Packaging
- 1g
- Price
- $179
- Updated
- 2025/07/31
- Product number
- FD126904
- Product name
- 4,4-Dimethyl-1,3-oxazolidin-2-one
- Packaging
- 500mg
- Price
- $150
- Updated
- 2021/12/16
- Product number
- FD126904
- Product name
- 4,4-Dimethyl-1,3-oxazolidin-2-one
- Packaging
- 250mg
- Price
- $85
- Updated
- 2021/12/16
- Product number
- 8803AD
- Product name
- 4,4-Dimethyl-oxazolidin-2-one
- Packaging
- 1g
- Price
- $120
- Updated
- 2021/12/16
- Product number
- 068859
- Product name
- 4,4-Dimethyl-oxazolidin-2-one
- Purity
- >95%
- Packaging
- 1g
- Price
- $255
- Updated
- 2021/12/16
4,4-DIMETHYL-2-OXAZOLIDINONE Chemical Properties,Usage,Production
Synthesis
124-68-5
57-13-6
26654-39-7
4,4-Dimethyloxazolidin-2-one (DMO) was synthesized as follows: 2-amino-2-methyl-1-propanol (10.0 g, 112 mmol) was mixed with urea (13.5 g, 224 mmol), and the mixture was heated and reacted for 1 hour at 170-180 °C, followed by heating up to 210-220 °C and continued heating for 1 hour. After completion of the reaction, it was cooled to room temperature and the reaction mixture was dissolved in water (50 mL). Dichloromethane (DCM, 5 x 50 mL) extraction was performed with the aqueous solution. The organic phases were combined, dried with anhydrous sodium sulfate (Na2SO4), filtered and concentrated under reduced pressure to afford 4,4-dimethyloxazolidin-2-one 10.3 g in 80% yield. The product was identified by 1H NMR (CDCl3): δ 6.13 (br s, 1H, NH), 4.07 (s, 2H, CH2), 1.32 (s, 6H, 2 CH3) ppm; 13C NMR (CDCl3) δ 159.4,77.1,55.4,27.7 ppm.
References
[1] Asian Journal of Chemistry, 2011, vol. 23, # 2, p. 929 - 930
[2] Patent: WO2015/68159, 2015, A2. Location in patent: Paragraph 00121-00122
4,4-DIMETHYL-2-OXAZOLIDINONE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4,4-DIMETHYL-2-OXAZOLIDINONE manufacturers
- Product
- 4,4-Dimethyl-1,3-oxazolidin-2-one 26654-39-7
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98.3%
- Supply Ability
- 100 tons
- Release date
- 2022-01-14