ChemicalBook > CAS DataBase List > 4,4-DIMETHYL-2-OXAZOLIDINONE

4,4-DIMETHYL-2-OXAZOLIDINONE

Product Name
4,4-DIMETHYL-2-OXAZOLIDINONE
CAS No.
26654-39-7
Chemical Name
4,4-DIMETHYL-2-OXAZOLIDINONE
Synonyms
DMO;DMRTA1;4-Dimethyl-2-oxazolidon;4,4-Dimethyloxazolidinone;4,4-DIMETHYL-2-OXAZOLIDINONE;4,4-dimethyl-oxazolidin-2...;4,4-diMethyl-oxazolidin-2-one;2-Oxazolidinone,4,4-dimethyl-;4,4-dimethyl-oxazolidine-2-one;4,4-Dimethyl-1,3-oxazolidin-2-one
CBNumber
CB2436935
Molecular Formula
C5H9NO2
Formula Weight
115.13
MOL File
26654-39-7.mol
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4,4-DIMETHYL-2-OXAZOLIDINONE Property

Melting point:
55-56 °C(Solv: ethanol (64-17-5); ligroine (8032-32-4))
Boiling point:
152-154 °C(Press: 10 Torr)
Density 
1.039±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
form 
solid
pka
12.91±0.40(Predicted)
color 
White to off-white
EPA Substance Registry System
2-Oxazolidinone, 4,4-dimethyl- (26654-39-7)
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Safety

WGK Germany 
3
HS Code 
2934999090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H317May cause an allergic skin reaction

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
CBR01583
Product name
4,4-Dimethyl-1,3-oxazolidin-2-one
Purity
Aldrich
Packaging
1g
Price
$179
Updated
2025/07/31
Biosynth Carbosynth
Product number
FD126904
Product name
4,4-Dimethyl-1,3-oxazolidin-2-one
Packaging
500mg
Price
$150
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD126904
Product name
4,4-Dimethyl-1,3-oxazolidin-2-one
Packaging
250mg
Price
$85
Updated
2021/12/16
AK Scientific
Product number
8803AD
Product name
4,4-Dimethyl-oxazolidin-2-one
Packaging
1g
Price
$120
Updated
2021/12/16
Matrix Scientific
Product number
068859
Product name
4,4-Dimethyl-oxazolidin-2-one
Purity
>95%
Packaging
1g
Price
$255
Updated
2021/12/16
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4,4-DIMETHYL-2-OXAZOLIDINONE Chemical Properties,Usage,Production

Synthesis

124-68-5

57-13-6

26654-39-7

4,4-Dimethyloxazolidin-2-one (DMO) was synthesized as follows: 2-amino-2-methyl-1-propanol (10.0 g, 112 mmol) was mixed with urea (13.5 g, 224 mmol), and the mixture was heated and reacted for 1 hour at 170-180 °C, followed by heating up to 210-220 °C and continued heating for 1 hour. After completion of the reaction, it was cooled to room temperature and the reaction mixture was dissolved in water (50 mL). Dichloromethane (DCM, 5 x 50 mL) extraction was performed with the aqueous solution. The organic phases were combined, dried with anhydrous sodium sulfate (Na2SO4), filtered and concentrated under reduced pressure to afford 4,4-dimethyloxazolidin-2-one 10.3 g in 80% yield. The product was identified by 1H NMR (CDCl3): δ 6.13 (br s, 1H, NH), 4.07 (s, 2H, CH2), 1.32 (s, 6H, 2 CH3) ppm; 13C NMR (CDCl3) δ 159.4,77.1,55.4,27.7 ppm.

References

[1] Asian Journal of Chemistry, 2011, vol. 23, # 2, p. 929 - 930
[2] Patent: WO2015/68159, 2015, A2. Location in patent: Paragraph 00121-00122

4,4-DIMETHYL-2-OXAZOLIDINONE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 4,4-DIMETHYL-2-OXAZOLIDINONE manufacturers

Honest Joy Holdings Limited
Product
4,4-Dimethyl-1,3-oxazolidin-2-one 26654-39-7
Price
US $0.00/KG
Min. Order
1KG
Purity
98.3%
Supply Ability
100 tons
Release date
2022-01-14