N-BENZYL-2-NITROANILINE
- Product Name
- N-BENZYL-2-NITROANILINE
- CAS No.
- 5729-06-6
- Chemical Name
- N-BENZYL-2-NITROANILINE
- Synonyms
- BENZYL-2-NITROANILINE;N-BENZYL-2-NITROANILINE;N-Benezyl-2-nitroaniline;N-benzyl-2-nitrobenzenamine;Benzylamine, n-(o-nitrophenyl)-;2-nitro-N-(phenylmethyl)aniline;BenzeneMethanaMine, N-(2-nitrophenyl)-
- CBNumber
- CB2485458
- Molecular Formula
- C13H12N2O2
- Formula Weight
- 228.25
- MOL File
- 5729-06-6.mol
N-BENZYL-2-NITROANILINE Property
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- Appearance
- Light yellow to orange Solid
Safety
- Hazard Codes
- Xi
- Hazard Note
- Irritant
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- R415553
- Product name
- BENZYL-(2-NITRO-PHENYL)-AMINE
- Purity
- AldrichCPR
- Packaging
- 50MG
- Price
- $30.7
- Updated
- 2025/07/31
- Product number
- CS-M2851
- Product name
- Benzyl(2-nitrophenyl)amine
- Purity
- 99.78%
- Packaging
- 25g
- Price
- $1172
- Updated
- 2021/12/16
- Product number
- CHM0004075
- Product name
- N-BENZYL-2-NITRO ANILINE
- Purity
- 95.00%
- Packaging
- 5G
- Price
- $1752.43
- Updated
- 2021/12/16
- Product number
- CS-M2851
- Product name
- Benzyl(2-nitrophenyl)amine
- Purity
- 99.78%
- Packaging
- 1g
- Price
- $100
- Updated
- 2021/12/16
- Product number
- FB132546
- Product name
- N-Benzyl-2-nitroaniline
- Packaging
- 500mg
- Price
- $100
- Updated
- 2021/12/16
N-BENZYL-2-NITROANILINE Chemical Properties,Usage,Production
Synthesis
100-39-0
88-74-4
5729-06-6
Synthesis of N-benzyl-2-nitroaniline (Step 1): 2-nitroaniline (5.0 g, 36.2 mmol) was dissolved in 100 mL of tetrahydrofuran (THF) under nitrogen protection, cooled to 0 °C and then 60% sodium hydride (NaH, 1.7 g, 43.4 mmol) was slowly added. The reaction mixture was stirred at room temperature for 30 min. Subsequently, benzyl bromide (7.4 g, 43.4 mmol) was added dropwise at 0 °C and the reaction system was warmed to 80 °C and stirred overnight. Upon completion of the reaction, the solvent was removed by distillation under reduced pressure and the residue was purified by fast column chromatography (petroleum ether: ethyl acetate = 2:1) to afford N-benzyl-2-nitroaniline (2.92 g, 36% yield) as a yellow solid. The structure of the product was confirmed by 1H NMR (300 MHz, CD3OD): δ 4.65 (d, J = 6 Hz, 2H), 6.69 (t, J = 7.2 Hz, 1H), 6.94 (d, J = 9 Hz, 1H), 7.25-7.50 (m, 5H), 8.09 (d, J = 8.4 Hz, 1H), 8.62-8.68 (m, 1H ).
References
[1] Green Chemistry, 2012, vol. 14, # 12, p. 3329 - 3335
[2] Molecules, 2016, vol. 21, # 4,
[3] Patent: WO2012/151512, 2012, A2. Location in patent: Page/Page column 115
[4] ACS Medicinal Chemistry Letters, 2016, vol. 7, # 2, p. 145 - 150
[5] European Journal of Medicinal Chemistry, 2014, vol. 84, p. 395 - 403
N-BENZYL-2-NITROANILINE Preparation Products And Raw materials
Raw materials
Preparation Products
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