2-DIMETHYLAMINO-PYRIMIDINE-5-CARBALDEHYDE
- Product Name
- 2-DIMETHYLAMINO-PYRIMIDINE-5-CARBALDEHYDE
- CAS No.
- 55551-49-0
- Chemical Name
- 2-DIMETHYLAMINO-PYRIMIDINE-5-CARBALDEHYDE
- Synonyms
- ASISCHEM C63425;TIMTEC-BB SBB010324;CHEMBRDG-BB 4010270;2-DIMETHYLAMINO-PYRIMIDINE-5-CARBALDEHYDE;5-Pyrimidinecarboxaldehyde, 2-(dimethylamino)-;2-(N,N-DiMethylaMino)pyriMidine-5-carboxaldehyde;2-(dimethylamino)pyrimidine-5-carbaldehyde(SALTDATA: FREE);2-DIMETHYLAMINO-PYRIMIDINE-5-CARBALDEHYDE ISO 9001:2015 REACH
- CBNumber
- CB2490335
- Molecular Formula
- C7H9N3O
- Formula Weight
- 151.17
- MOL File
- 55551-49-0.mol
2-DIMETHYLAMINO-PYRIMIDINE-5-CARBALDEHYDE Property
- Melting point:
- 122-124 °C
- Boiling point:
- 289.6±32.0 °C(Predicted)
- Density
- 1.204±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- solid
- pka
- 2.27±0.10(Predicted)
- Appearance
- White to off-white Solid
- InChI
- InChI=1S/C7H9N3O/c1-10(2)7-8-3-6(5-11)4-9-7/h3-5H,1-2H3
- InChIKey
- XBYXYDVSCMMJDT-UHFFFAOYSA-N
- SMILES
- C1(N(C)C)=NC=C(C=O)C=N1
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- CBR00347
- Product name
- 2-(Dimethylamino)pyrimidine-5-carbaldehyde
- Purity
- Aldrich
- Packaging
- 1g
- Price
- $320
- Updated
- 2024/03/01
- Product number
- Z0688
- Product name
- 2-Dimethylamino-pyrimidine-5-carbaldehyde
- Packaging
- 1g
- Price
- $184
- Updated
- 2021/12/16
- Product number
- OR954195
- Product name
- 2-(Dimethylamino)pyrimidine-5-carbaldehyde
- Purity
- 95%
- Packaging
- 1g
- Price
- $185
- Updated
- 2021/12/16
- Product number
- D10420
- Product name
- 2-(N,N-Dimethylamino)pyrimidine-5-carboxaldehyde
- Purity
- 98%
- Packaging
- 5g
- Price
- $225
- Updated
- 2021/12/16
- Product number
- D10420
- Product name
- 2-(N,N-Dimethylamino)pyrimidine-5-carboxaldehyde
- Purity
- 98%
- Packaging
- 1g
- Price
- $60
- Updated
- 2021/12/16
2-DIMETHYLAMINO-PYRIMIDINE-5-CARBALDEHYDE Chemical Properties,Usage,Production
Synthesis
933702-55-7
55551-49-0
General procedure for the synthesis of 2-dimethylaminopyrimidine-5-carbaldehyde from 2-chloropyrimidine-5-carbaldehyde: 2-chloropyrimidine-5-carbaldehyde (412 mg, 2.89 mmol) and triethylamine (Et3N, 482 μL, 3.47 mmol) were dissolved in dioxane (20 mL), followed by the addition of a solution of dimethylamine (Me2NH) in tetrahydrofuran (THF) (1.59 mL, 2.0 M, 3.18 mmol). The reaction mixture was stirred at room temperature for 1 h. After completion of the reaction, the reaction solution was filtered and the solid was washed with dioxane (5 mL). The filtrate was concentrated under vacuum to give 2-dimethylaminopyrimidine-5-carbaldehyde (427 mg, 97.7% yield) as a yellow solid. The product was analyzed by LC-MS (ES+) and showed a molecular ion peak [MH]+ of 152.2. HPLC analysis showed a retention time (Rt) of 4.14 min and a purity of 97.9%.
References
[1] Patent: US2015/258101, 2015, A1
2-DIMETHYLAMINO-PYRIMIDINE-5-CARBALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-DIMETHYLAMINO-PYRIMIDINE-5-CARBALDEHYDE manufacturers
- Product
- 2-DIMETHYLAMINO-PYRIMIDINE-5-CARBALDEHYDE 55551-49-0
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-12-13
- Product
- 2-DIMETHYLAMINO-PYRIMIDINE-5-CARBALDEHYDE 55551-49-0
- Price
- US $9.80/KG
- Min. Order
- 1g
- Purity
- ≥99%
- Supply Ability
- 100kg
- Release date
- 2020-01-08